Vessel Utama Laporan
August 7, 2018 | Author: Anonymous vUA5zHEpAH | Category: N/A
Short Description
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Description
PT. PUPUK SRIWIDJAJA
Hal 1 of 25
Bagian Ammonia P-II
Rev : 00
DEPARTEMEN OPERASI I
DAFTAR DAFTAR ISI 1. SPONGE IRON DESULFURIZER 2. GLYCOL ABSORBER GLYCOL S!RIPPER ". CO2 RE#O$AL FEED !REA!ING %. DESULFURIZER Co#o & Z'O 5. SA!URA!OR (. PRI#ARY REFOR#ER ). SECONDARY REFOR#ER 8. HIGH !E#PERA!URE SHIF! CON$ER!ER
*. LO+ !E#PERA!URE SHIF! CON$ER!ER 10. CO2 RE#O$AL #AIN BENFIELD 11. 11. #E!HANA!OR 12. A##ONI 12. A##ONIA A CON$ER CON$ER!ER !ER
PT. PUPUK SRIWIDJAJA
Hal 2 of 25
Bagian Ammonia P-II
Rev : 00
DEPARTEMEN OPERASI I
Na,a Ala!a'al o3e
SPONGE IRON DESULFURIZER 22 A/l 200% 201&D A. Kon Kondis disii Opera Operasi si 201 201 D
I'le- Baffle S/a7 R'
Cea,4 Ball
!e,/ea-e !e>a'a' /H H2S 'leH2S o-leU, !e>'6
2) = " oC 25 = 2) > ?4, 2 ).5 = .0 5 //, @,a 2 //, @6-a'3a P6 1 = 2 -a8'
S4ee'
!. Rea"si
S/o'e S/o'e Io' 4a-al76+oo3e' -a7
!a7 6//o-
Colle4-o O-le&
&
&
$ol,e ,e of 6/o' /o'e e o' o' 4a-al76- : 11"0 f- " Cea,4 Ball a. Da,e-e 1 '48 9. Be3 De/-8 152 ,, 4. $ol,e 5 f- " Ca6-4 D6-9-o a. Da,e-e % f-; 1 '48 9. P/e Da,e-e 1 '48 4. Pefoa-e3 Pefoa-e3 Da,e-e Da,e-e < '48
Fe2O".(H2O "H2S Fe2S" *H2O Rea>6 9e6fa- e>6o-e,6 3e'a' Fe 2O" 7a' -e,/e'a6 3ala, -a-al >a7 #. De Des" s"ri rips psii U$%$ U$%$
Ga6 7a' 7a' ,a6> ,a6> >e 3e6lf 3e6lfe e 201&D -ele98 3a8l -ela8 ,elal /e'7a'a' 3a' 3/a'a6>a' 3ala, a4>e- a-e //e 3e' 3e'a' a' ,e3 ,e3a a 6-ea 6-ea, , LS @".5 @".5 >?4 >?4, , 2; '-> ,e'3a/a->a' -e,/ea-e o/-,, 7a- a- 2) = " oC. !e,/ea-e ' 8a6 3aa 6-a9l >ae'a 9la -e,/ea-e a6 7a' ,a6> le98 -' 3a %0 oC; ,a>a >a'3'a' H 2O 3ala, 6/o'e o' a>a' ,e'a/; ,e'a/; 6e3a'> 6e3a'>a' a' 9la -e,/ea-e,/ea-e e o le98 e'3a8 3a 2) C; ,a>a >e4e/a-a' ea>6 a>a' 9e>a'. Se'7aa 6lf a'oa'> 8a6 38la'>a' >ae'a: Da/a Da/a-- ,ee ,ee3 3>6 >6 '8 '89 9-o -o /a3a /a3a 676-e, Be'fel3 A>a' -e9aa -e9aa ole8 a6 CO 2 6e8'a ,e6a> 4o,/e66o CO 2 3 ea /la'-. #e'a,9a8 9e9a' 102&D
DEPARTEMEN OPERASI I
PT. PUPUK SRIWIDJAJA
Hal " of 25
Bagian Ammonia P-II
Rev : 00
#e/a>a' a4' 9a >a-al6 /a3a /o6e6 6ela'-'7a. Ole8 >ae'a - >a3a 6lf 7a' >ela 3a '- ' @201&D 8a6 le98 >e4l 3a 2 //,. Se9aa >a-al6 3/a>a 6/o'e o' 7a- 6e9> >a7 7a' ,e'a'3' 6e9> 9e6. Po6e6 3e6lf6a6 8a6 -ea3 /a3a >ea3aa' e'8 a/ a 3a' 3ala, 6a6a'a 9a6a @/H ).5 = .0. Ua/ a 9ef'6 '-> ,e'a96o96 3a' ,e'>a- 4>/ la,a H 2S; 6/a7a ea>6 3e'a' 6/o'e o' 3a/a9ela'6'. Ua/ a 7a' 4>/ a 3/el>a' '-> ,e'4ea8 -ea3'7a 3e83a6 6/o'e o'. I'3>a6 9la >o'36 e'8 a3ala8 a3a'7a -e-e6a' a >ela 6/o'e o'. U'-> ,e'aa >o'36 6/o'e o' -e-a/ e'8 3a' 9a6a; ,a>a 3'e>6>a' la-a' NaOH ,elal 20%&L 3e'a' >o'6e'-a 0." = 0.5vol 3a 9aa' a-a6 201&D. Na,a Ala!a'al o3e
GL&#OL A!SOR!ER ' GL&#OL STRIPPER 22 A/l 200% 201&L
A. Kondisi Operasi 201 L
A96o9e De,6-e
S-//e B9le 4a/ -a7 @10 6-ae
! lea' l74ol P 6-//' a6 H2O lea' l74ol
Pe66 @>?4, 2 A 2) !e,/ @oC "2 Pe66 1.%2 2 @@>?4, A !e,/ @oC 20% o K ( C 3a ! o- 201&D 0.2 = 0.2 >?4, 2 0.2 -
!. Rea"si
#a LJ3 level A'- 6l Baffle
#. Des"ripsi U$%$
Pe6-a a96o96 3e83a6 a6 9e6fae>6o-e,6 7a' a-'7a ,ele/a6 /a'a6. Pa'a6 a96o96 a>a' 36ea/ ole8 a6 3a' !EG - 6e'3. I'la8 6e9a9'7a -e,/ea-e >elaa' 48 !EG 6e-a a6 7a' 63a8 M3>e'>a' ela-ve le98 /a'a6 3a >o'36 aal'7a.
DEPARTEMEN OPERASI I
PT. PUPUK SRIWIDJAJA
Hal % of 25
Bagian Ammonia P-II
Rev : 00
Pa3a 8a>e>a-'7a; /e6-a 3e83a6 9e-a' '-> ,e''>a' >a3a a 3ala, 9a3a' a6 a-a ,e''>a' --> e,9' @3e /o'- a 3 a6. Dala, 8al ' a96o9e 201&L ,e,/'7a f'6 7a' 6a,a; 6e8'a a -3a> ,e'7e9a9>a' >e9'-a' 3 -9e 20"&C /a3a /o6e6 HHC e,oval. Ba-a6 >e,a,/a' /e'7ea/a' >a'3'a' a 3 9a3a' a6 ole8 !EG 39a-a6 ole8 >e6e-,9a'a' a 3 9a3a' a6 3e'a' a 3 9a3a' !EG. !EG 7a' -ela8 e'8 3e'a' a >e,3a' 3ee'ea6 3 l74ol 6-//e 3e'a' /e,a'a6a' 8'a 20% oC 3a' 9a'-a' 6-//' 3a 'a-al a6 7a' 9e-e>a'a' 0.2 = 0.2 >?4, 2; 6e8'a a/ a 3a/a- 3/6a8>a'. Se9el, ,a6> >e a96o9e; lea' l74ol /el 33''>a' 3l 3a' 3aa 68'7a ( oC 3 a-a6 -e,/ea-e ,a6> a96o9e '-> ,e'4ea8 >o'3e'6a6 HHC 7a' ,e'7e9a9>a' foa,' 3 a96o9e 201&L. ,la8 >a'3'a' a 3 9a3a' a6 /a3a 9e9aa -e,/ea-e a3ala8 8al 7a' ,-la> 3>e-a8 3ala, ,ea'4a' a-a -o9le68oo-' l74ol 3e873a-o' 676-e,.
(Ref: Cahyo Hardo P, Sistem Dehidrasi Gas dengan Glycol, Studium General K! "a#ar, $%%&'
Na,a Ala-
#O2 REMO(AL FEED TREATING
PT. PUPUK SRIWIDJAJA
Hal 5 of 25
Bagian Ammonia P-II
Rev : 00
DEPARTEMEN OPERASI I
!a'al o3e
22 A/l 200% 201&E?202&E A. Kondisi Operasi 201 E ' 202 E De,6-'
201 & E LJ3 D6-9-o 1 Hol3 Do' Ga-e 1
Pa4>'
Ga6 'e4-o' Pla-e 1 LJ. Re36-9-
Hol3 Do' Ga-e 2
Pa4>'
Ga6 I'e4-o' Pla-e 2
#a LJ3 Level
A'- 6l Baffle
202 & E CO2 '?oPe'7ea/ S.G. @
Pe66 @>?4, 2 A 25 o !e,/ @ C 12* 2 Pe66 @@>?4, A 1." !e,/ @oC 12* ( = 10 ? 0." = 0.5 @ ,ol Be'fel3 @ 2CO"; DEA; $2O5; UCON 500 HB 1.2 = 1.25 ?44
!. Rea"si 2CO" 2CO2 H2O 2 HCO " Rea>6 >e >a'a' -ea3 3 A96o9e @201=E 3a' 9e6fa- e>6o-8e,6 6e3a'>a' >e > -ea3 3 6-//e @202=E. #. Des"ripsi U$%$ CO2 8a6 38la'>a' 3a a6 ,/a' >ae'a: #e'7e9a9>a' ea>6 ,e-8a'a6 3 3e6lfe Co#o. CO " H 2 CH% H2O /a'a6 CO2 % H2 CH% 2H2O /a'a6 Rea>6 >e6e-,9a'a' S7' Ga6 9ee6e >e > 3 101&B #e'a' Hea- Bala'4e 3 101&B @P,a7 Refo,e 6e8'a >e9-8a' NG 4>/ -'.
o,/o66 Be'fel3 1. 2CO" : /e'7ea/ @ 25 = "0- 2. DEA : a4-va-o @2 = %- ". $2O5 : 4oo6o' '89-o @0.- $-o-al : 0.) ,',al $5 : 0.% ,',al %. UCON 500 HB : a'- foa,'
PT. PUPUK SRIWIDJAJA
Hal ( of 25
Bagian Ammonia P-II
Rev : 00
DEPARTEMEN OPERASI I
#H&1
De,6-'
Seal Po#H&2 $a/o LJ I'le- D6-. Hol3 Do' G3 1
Pa4>' Ga6 I'e4Pla-e?LJ3 D6-9-o $a/o 6a,/le Hol3 Do' G3 2 Pa4>' Ga6 I'e4Pla-e 2
Daoff Pa' Re9ole e-' I,/'e, e' Baffle #H&% #a LJ3 Level
A'- Sl Baffle
eaala' ,e,e'8 3e6' CO 2 lea>ae @CO 2 lolo6 a'-aa la': S>la6 la-a' 7a' -3a> ,e'4>/ ,la8 2CO" 7a' ,e'7ea/ CO 2 3'7a-a>a' 3ala, FC. De'a' >e'a>a' a-e a6; 9ea- ,la8 CO 2 >- 'a>. A>a' -ea3 CO2 lea>ae 9la -3a> 3,9a' 3e'a' >e'a>a' 6>la6 la-a' Ree'ea6 la-a' -3a> 6e,/'a CO2 96a -e6ea/ ole8 Be'fel3 9la -e>a'a' /a6al CO2 3 3ala, a6 le98 9e6a 3a CO 2 3 3ala, la-a'. !e>a'a' CO 2 3 la-a' a3ala8 f'6 3a FC -e8a3a/ HCO "& /a3a 68 3a' >o,/o66'7a. Bla >o'6e'-a6 HCO"& -'; ,a>a -e>a'a' a/ CO 2 3 la-a' -'; a>9a-'7a ee'ea6'7a -3a> 6e,/'a. Pe'3''a' la-a' -3a> 6e,/'a !e>a'a' a/ la-a' a>a' e'3a8 9la 68 e'3a8; 6e8'a /e,'a' a6 le98 9a>; -a/ a-e /e'7ea/a''7a >e4l. o'-a> lJ3 3a' va/o -3a> 6e,/'a Se4aa ,, 36e9a9>a' ole8 36-96 lJ3 3a' a6 7a' -3a> ,ea-a; ,e3a 7a' -3a> 4>/ 3a' 9eo/ea6 /a3a a-e a8 3 9aa8 3e6'. A3a'7a 'e- 3ala, CO 2 36e9a9>a': e9o4oa' -9e 9'3le e9ole. LJ3 $o-e /a3a a96o9e Foa,' 96a -ea3 9la: A3a'7a 6ol3 /a-4le 3a' lolo6'7a HHC A'- foa,' 7a' 9ele98a'
PT. PUPUK SRIWIDJAJA
Hal ) of 25
Bagian Ammonia P-II
Rev : 00
DEPARTEMEN OPERASI I
Na,a Ala!a'al o3e
DESULFURIZER #oMo ZnO 22 A/l 200% 102&D
A. Kondisi Operasi 102 D
I'le- Baffle S/a7 R'
!e,/ O/6. '?o!e>a'a' Ra-o H2?fee3 a6 Ca-al76-
Cea,4 Ball S4ee'
U, !e>'6 Ca-.
")1 oC %1.5 >?4, 2 #' 0.% ,ol?,ol CoO " = ".5#oO * = 11 Z'O *0 10 & 15 -a8'
!. Rea"si
S/o'e Io' 4a-al76+oo3e' -a7
!a7 6//o-
Rea>6 3 Co#o 4a-al76RSR 2H2 RH RSH H 2S RSH H 2 RH H2S Rea>6 3 Z'O 4a-al76H2S Z'O Z'S H 2O S,9e H2 3a 3648ae LP 4o,/e66o 10"& a-a PGRU #. Des"ripsi U$%$
Colle4-o O-le&
&
&
$ol,e of 6/o'e o' 4a-al76- : 11"0 f- " Cea,4 Ball 3. Da,e-e 1 '48 e. Be3 De/-8 152 ,, f. $ol,e 5 f-" Ca6-4 D6-9-o a. Da,e-e % f-; 1 '48 9. P/e Da,e-e 1 '48 4. Pefoa-e3 Da,e-e < '48
De6lfe Co#o 9ef'6 6e9aa -e,/a- '-> ,e'a' >a'3'a' 6lf oa'> 7a' 9e/a ,e4a/-a' 3e'a' 4aa 3ea>6>a' 3e'a' H 2 ,e,9e'-> H2S 3a' al>a'a 3ala, >a-al6 Co#o. H2S 7a' -e9e'-> lal 38la'>a' ole8 >a-al6 Z'O 7a' ,e,9e'-> e'3a/a' Z'S 3a' H 2O. Slf 8a6 38la'>a' >ae'a ,e,/'7a a4' 9a >a-al6 /,a7 efo,e 3a' >oo6f '-> /eala-a'. Be9e3a 3e'a' P6 la'; 3 P6 II; >a-al6 Co#o 3a' Z'O 9ea3a 3ala, 1 ve66el /a4>e3 9e3 7a' -e/6a8 6e4aa 9e-'>a-
PT. PUPUK SRIWIDJAJA
Hal of 25
Bagian Ammonia P-II
Rev : 00
DEPARTEMEN OPERASI I
'ea >a-al6 Co#o&Z'O 3-a'3a 3e'a' 6lf -o-al o-le- 0.1 //, vol,e 3e'a' /e66e 3o/ 0.2 >?4, 2. D6a8a>a' ,e'4ea8 -e9e'->'7a 4o'3e'6a-e 3 /a4>e3 9e3 -e-a,a /a3a 6aa- 6-a- / ,a/' 68- 3o' '-> ,e'4ea8 8a'4'7a >a-al6 Z'O. Pengaruh Variabel Operasi 1. !e,/ea-e !e,/ea-e o-le- 10"&B 33e6' a'-aa ")1 oC. Bla le98 e'3a8 3a "00 oC; ,a>a >o've6 6lf a>a' e'3a8. Na,' 9la le98 3a %00 oC; ,a>a a>a' -ea3 -8e,al 4a4>' /a3a fee3 a6. 2. !e>a'a' De6' -e>a'a' 'le- 102&D " >?4, 2 3ala, >ea3aa' 'o,al. !e>a'a' ' 8a6 3aa /a3a 'la -e-e'- 3a' -3a> 9ole8 ,e'a3 vaa9le o/ea6 7a' 9e9a8. #a>' -' -e>a'a'; ,a>' 9a> 3e6lf6a6. Ya' /e'-' -e-a/ ,o'-o -e,/ea-e 3 9e3; P ve66el 3a' >a3a 6lf. ". Ra-o H 2 ? fee3 a6 D-e'->a' 9a8a ,ol a-o H 2 ? fee3 a6 0.% ,ol?,ol. U,,'7a >e'a>a' a-o a>a' ,e,/e9a> -'>a- 3e6lf6a6 7a' 38a6l>a'.
Na,a Ala!a'al o3e
SATURATOR 22 A/l 200% "01&E
Ga6 o-le-
A. Kondisi Operasi )01E !e,/ O/6. '?o200 & 205 oC !e>a'a' ") & " >?4, 2 Pe'a,9a8a' S?C Q 0. Flo fee3 a6?6-ea, 2*1*0 ? 2(000 >?8 #e3a /e'e'8 Sa-a-e3 S-ea,
LJ3 I'le-
Pa4>' R'
Pall
Pa4>' D648ae
Ga6 I'le$o-e Bea>e
LJ3 O-le-
!. Rea"si Pe'e'8a' fee3 a6 3e'a' a #. Des"ripsi U$%$ De6' a6l /a9> -3a> ,e,/'7a 6a-a-o; 'a,' /a3a A,,o'a O/-,a-o' Poe4@AOP ala- ' 3-a,9a8>a' '-> ,e'a' >o'6,6 6-ea, 3 /,a7 efo,e. Ga6 7a' -ela8 e'8 3e'a' a/ a lal 6a/ 3,a6>>a' >e efo,e 6e-ela8 34a,/ 3e'a' 6-ea, %2 >?4, 2 @#S.
PT. PUPUK SRIWIDJAJA
Hal * of 25
Bagian Ammonia P-II
Rev : 00
DEPARTEMEN OPERASI I
Na,a Ala!a'al o3e
PRIMAR& REFORMER 22 A/l 200% 101&B
A. Kondisi Operasi 101 !
!e,/ O/6. '?o!e,/ a3a'- 6e4-o' !e>a'a' fee3 a6 !e>a'a' a3a'- 9o Ra-o S-ea,?Ca9o' CH% lea> O2 4o'-e'- @fle a6 Pe66 3o/ U, !e>'6 Ca-. !. Rea"si
52% = 20 oC 10"" oC "( >?4, 2 ( ,,H 2O ".2 = ".% ,ol?,ol 11.( = 12."( ,ol ".2 5 >?4, 2 2 & " -a8'
DEPARTEMEN OPERASI I
PT. PUPUK SRIWIDJAJA
Hal 10 of 25
Bagian Ammonia P-II
Rev : 00
Rea>6 ,e-8a'e 3a' 6-ea, 3e'a' /ea'-aa >a-al6 N4>el CH% H2O CO "H 2 = @ea>6 e'3o-8e,; H f 20(.2 >?>,ol Rea>6 la'-a' 4a9o' ,o'o>63a CO H2O CO2 H2 @ea>6 e>6o-8e,6; H f &%1.2 >?>,ol Ya' 3''>a' a3ala8 ea>6 oveall; 7a-: CH% 2H2O CO2 %H2 = @ea>6 e'3o-8e,6 #. Des"ripsi U$%$
Paa,e-e 7a' ,e/a>a' vaa9le 3ala, ea>6 3 /,a7 efo,e a3ala8: 1. !e,/ea-e ala -e,/ea-e o-le- /,a7 efo,e 3'a>>a'; ,a>a ea>6 a>a' 9ee6e >e >a'a'; 9ea- a>a' ,e''>a' >a3a CH % 3a' CO2; 6e3a'>a' >a3a CO 3a' H 2 a>a' 'a>. Be-/' efe> 6e9al>'7a -ea3 9la -e,/ea-e 3-'>a'. 2. !e>a'a' !e>a'a' 3 3ala, 676-e, 3aa -e-a/; 3e'a' 3e,>a' -e>a'a' efo,e -3a> 3a'a/ 6e9aa vaa9le. !e-a/ 3e'a' >e'a>a' -e>a'a' a>a' ,e,9e>a' ef> 7a' 6a,a 6e/e- /e''a' 68. De6' efo,e 6elal ,e''>>a' 6a- >o,/o, 3ala, 6e e>o'o,. ". Ra-e 6-ea, S-ea, >e efo,' 8a6 4>/ aa /e,9e'->a' 4a9o' 3 >a-al6 -3a> -ea3. #e'a>>a' S?C a>a' ,e'e6e ea>6 >e >a'a'; 6e8''a ,e-8a'e 3a' CO a>a' 9e>a' 3a' ,e'a>>a' a6 CO 2 3a' H 2 3 3ala, a6 efo,'. Na,' efe> 6a,/''7a >e9-8a' fel a6 3a' 6-ea, a>a' 'a>. D 3ala, o/ea6 3e6'; 'la e>o'o,6 '-> S?C a-o a3ala8 ".2. >a -ea3 a'a' o/ea6 6e8''a -e9e'-> 3e/o6- 4a9o' 3ala, >a-al6 efo,e; ,a>a 3e/o6- - 3a/a- 38la'>a' 3e'a' ,e'a>>a' S?C 3 a-a6 'o,al 6ela,a 9e9ea/a a>- la,a'7a; 6e8'a a>-f-a6 >a-al6 'o,al >e,9al. Na,' 9la -e9e'-> 3e/o6- 7a' 6a'a- 9a'7a>; ,a>a /a9> /el 3,a->a' '-> /e'a'-a' >a-al6. !9e&-9e 3 >a-al6 /,a7 efo,e 36 3e'a' >a-al6 N4>el 3a' 3al ole8 ala' a6. P,a7 Refo,e P6 II -e3 3a 252 -9e 4a-al76- 3e'a' '4a' %2 -9e -a/ o&'7a; 3,a'a -e3a/a- -o-al ( o. Bla 6ala8 6a- -9e ,e,9e>a' /e9e3aa' -e>a'a' a6 ,a>a a>a' ,e'a>9a->a' ove 8ea-' a-a ea>6 efo,' -3a> 6e,/'a. Sfa-&6fa- >a-al6 efo,e 7a' 8a6 3/e8a->a' a'-aa la':
DEPARTEMEN OPERASI I
PT. PUPUK SRIWIDJAJA
Hal 11 of 25
Bagian Ammonia P-II
Rev : 00
1. H'3a 3a a4' >a-al6. Ra4' >a-al6 36' 9e/a : H2S H2S 7a' ,ele98 >a3a ,a>6,, 7a' 3-e'->a' @ 0.1 //,$ a>a' ,e'a' a>-f-a6 >a-al6. #e6> 3e,>a' a4' ' 9e6fa- 6e,e'-aa >ae'a 3e'a' ,e'al>a' a6 9e68 9e9a6 6lf; ,a>a o/ea6 a>a' >e,9al 6e/e- 6e3a >ala. Coo>' 3 /e,>aa' Hal ' -ea3 >ae'a /ee'>a8a' eve69le HHC 3a' 3e>o,/o66 eve69le CH %. Efe> 3a 4oo>' ' 3a/a,e'7e9a9>a' /e''a' a>-v-a6 >a-al6; 6e8'a /e66e 3o/ a>a' 'a> 3a' -ea3 8o- 6/o- 3 -9e >a-al6. I' ,e'7e9a9>a' ea>6 ,e'a3 -3a> ,ea-a. 2. a-al6 -e>, 3ala, >ea3aa' -eo>63a6; >a-al6 a>a' ,e'e9la -e,/ea-e le98 -' 3a -e,/ea-e o/ea6 'a,' /e'e-a' 3a/a- 3a9a>a'. ". H'3a ,e'3''>a' >a-al6 la,a 3e'a' a >ae'a a>a' /e4a8; >e4al >a-al6 9a. %. Bla >a-al6 3ala, >ea3aa' -ee3>6; aa aa -3a> -e>e'a l'>'a' >ae'a a>a' ,e'o>63a6 >a-al6; >e4al 9la >o'36 3aa 3e'a' 9a>. 5. !'>a' -e,/ea-e >a-al6 6a,/a 20% oC a-a le98 e'3a8 9la ,e,a->a' efo,' >a-al6 /a3a >ea3aa' a-,o6/8ee. >a Se4o'3a7 efo,e a>a' 39>a a-a 3al 3aa; >a-al6 8a6 6elal 3o>63a6 3e'a' 3aa 6e9el, ala' 6-ea, 38e'->a'. Dala, ,e'o/ea6>a' f'a4e; a6 7a' >ela 3a /,a7 efo,e 3aa -e,/ea-e'7a 00 oC 3e'a' ,e'a- -e,/ea-e 3 a3a'- 6e4-o' 6e>-a *2 oC. Fle a6 /a'a6 a>a' ,e'al >e 9aa8 a3a'- 6e4-o' 9o 3a' ,a6> >e 34- 3 la'-a f'a4e. D4- ,e/a>a' -a'66 a'-aa a3a'- 3e'a' 4o've4-o' 6e4-o' 7a' 9ef'6 '-> ,e'aa fle a6 7a' /a'a6 9e6''a' 6e4aa ef6e' 3e'a' -9e >a-al6 6e8'a ,e'8la'>a' 3aea8 6-a'a' 3 a3a'-. !e>a'a' 7a' 3/el>a' '-> ,e'al>a' fle a6 3la>>a' 3e'a' ,e''a>a' fa' 7a' -ele-a> 3 3a6a 4eo9o'. Fle a6 7a' ,a6> >e 9aa' 4o've4-o' f'a4e /a3a 68 6e>-a 1020 oC ,e,9e>a' /a'a6 6e4aa 9e-a' -e8a3a/ 4ol 9e>-: 1. Fee3 4a,/a' 2. U3aa /o6e6 3a' 6-ea, ". S-ea, /e'ea> @2 9aa' %. A /e'6 >e-el @9ole fee3 a-e 5. Co'3e'6a-e 6a-a-o (. Ga6 ala, 6e9aa 9a8a' 9a>a.
DEPARTEMEN OPERASI I
PT. PUPUK SRIWIDJAJA
Hal 12 of 25
Bagian Ammonia P-II
Rev : 00
Fle a6 7a' 33''>a' ,e''al>a' 3aea8 4o've4-o' 6e4-o' /a3a -e,/ea-e 22" oC 3>ela>a' ,elal 4eo9o' @6-a4> >e a-,o6/8ee 3e'a' ,e''a>a' M'34e3 3af- fa'. !e>a'a' 'o,al 3 a3a'- a3ala8 0.*"% ,,H @-e>a'a' 'ea-f. !e>a'a' ' a>a' ,e'a- ove'o '-> ,e'aa -e>a'a' 3ala, >o-a> /e,9a>aa'. Trouble shooting di Primary Reformer A3a 9e9ea/a 8al 7a' 3a/a- ,e'7e9a9>a' Refo,e -3a> 9e>ea 3e'a' 6e,e6-'7a; a'-aa la' :
1. o've6 7a' e'3a8 Bla >o've6 7a' 33a/a- -elal e'3a8; /el 3la>>a' -'3a>a' '-> ,e''>a' CH% lea>ae 3e'a' 4aa : a. Pe8a->a' Slf 4o'-e'-. U'-> ,e'e-a8 6e4aa /a6- a3a'7a Slf; 4e> 873o4a9o' fee3; a6 9a' /,a7 efo,e 3a' ala' a6 3a ee'ea-o 3 CO2 e,oval 676-e,. I'3>a6 le98 a8 3a >e9ea3aa' 6lf 3 fee3 6-ea, 9a8a CH% lea>ae 3a efo,e a>a' 9e9a8 6eea 6e-ela8 4a9o' 3, 7a' 9a 36ev4e. >a -e3a/a>ele98a' 6lf; ' 3a/a- 3>a' 3e'a' ,e''>a->a' fe>e'6 ee'ea6 3a 4a9o' 3, 9. !e,/ea- o/ea6 7a' le98 e'3a8 3a 3e6' 4. Ra6o S-ea,&4a9o' 7a' le98 e'3a8 3a 3e6' 3. a-al6 /e'a8 ,e'ala, ove 8ea-' a-a 3e/o6- 4a9o' 3 -9e 2. Ho- 6/o- 3 -9e efo,e a. Pe,9e'->a' Ca9o' I' a>a' -ea3 >ae'a ea>6 o>63a6 7a' -3a> 6e,/'a 3 6e>-a -9e 7a' 3-a'3a 3e'a' --> /a'a6 @8o- 6/o-. Ca9o' 7a' ,e',/l 3 >a-al6 a>a' ,e'8ala' >o'-a> a6 3e'a' N>el a>-f. Pe'a,9a8a' /a'a6 3a la; 8a'7a a>a' ,e'a>>a' -e,/ea-e 3a 3'3' -9e. La'>a8 7a' ,'>' 96a 3la>>a' a3ala8 3e'a' ,e'a,9a8 6-ea, /a3a -9e '-> 9e9ea/a a,. 9. Ala' a6 -3a> ,ea-a I' 36e9a9>a' ole8 -e--/'7a aea >a-al6; ,e',/l'7a >a-al6 a-a >e>o6o'a' >a-al6. U3aa 7a' -3a> -e>o'-ol 6e8'a >o'-a> 3e'a' >a-al6 7a' -ee3>6 3 a-a6 200 oC 3a/a,e'a>9a->a' /el,ea' >a-al6. e6ala8a' loa3' >a-al6 /' 3a/a- ,e'a>9a->a' 8al 6e/a. I' 3a/a- 3a-a6 3e'a' ,e'la' >e,9al loa3' >a-al6.
DEPARTEMEN OPERASI I
PT. PUPUK SRIWIDJAJA
Hal 1" of 25
Bagian Ammonia P-II
Rev : 00
4. !9e -e--/ 6e9aa'. ala a3a 6e9aa' -9e efo,e le98 /a'a6 3a/a3a la''7a; ' ,'>' a>a' M,e,9'>6: 7a' ,e'7e9a9>a' /l 3 9e3 >a-al6 a-a 6//o- 3. Se9a8 -9e 3a/a- -e--/ ole8 >o,/o'e' 3a 9ole a-e -ea-,e'- 3 6-ea, /o6e6 a-a ole8 3e/o6- 4a9o' 3a' /e4a8a' >a-al6 ". Pe66e 3o/ 7a' 9ele98a' . ala /e66e 3o/ 'a>; ' ,'>' 36e9a9>a' ole8 >eaala' /o6e6 7a' ,e'a>9a->a' -e9e'->'7a 9-a' 8al6 >a-al6 a-a /e,9e'->a' 4a9o'. e6ala8a' /o6e3 '-> loa3' >a-al6 >e efo,e 3a/a- a ,e'a>>a' /e66e 3o/ 3e'a' -e--/'7a 6/oo- 3 ole8 >a-al6 7a' /e4a8. Be9ea/a 8al 7a' 3a/a,e'7e9a9>a' -''7a /e66e 3o/ a'-aa la': a. A 7a' ,e'e'a >a-al6 efo,e 3 a-a6 500 oC 3a/a- ,e,e4a8 >a-al6 6e4aa 4e/a-. +ala/' >ea3a' /e4a8'7a >a-al6 9ea3a 3 9aa' a-a6 -9e; /e4a8a' /a>el a>8'7a a>a' -' ,elal -9e 3a' ,e'-/ 6e9aa' 9e3. 9. o'36 o/ea6 7a' ,e,9a- /e,9e'->a' 4a9o' /a3a >a-al6 a>a' ,e'a>>a' /e66e 3o/ 7a' -'. S-ea, /o6e6 7a' -3a> 4>/; 8a3'7a 6lf; -elal -' -e,/ea-e /e,a'a6a' aal /a3a fee3 a-a >o,/o66 a6 7a' 9e,a4a,&,a4a, a3ala8 /e'7e9a9 -a,a 8al '. 4. !elal 6e' 6-a- / 3a' 68- 3o' a>a' ,e,9a- -9e 9e>o'-a>6 3a' ,e'e,9a'. Peea>a' -9e ' a>a' ,e,4 /e4a8'7a >a-al6 3. +ala/' aa' -ea3; /l 3a/a- -ea3 3 'le- 'ole -9e. Pl le98 6e' -ea3 3 o-le- 'ole >ae'a /e4a8a' >a-al6 a-a ,a-eal a6' la''7a. Pa3a //a 'le-; 3e9 96a 9ea>,la6 7a' 8a6 39e68>a' 6ea>- 68- 3o'.
PT. PUPUK SRIWIDJAJA
Hal 1% of 25
Bagian Ammonia P-II
Rev : 00
DEPARTEMEN OPERASI I
Na,a Ala!a'al o3e
SE#ONDAR& REFORMER 22 A/l 200% 10"&D A S-ea, Pla-fo, S//oGa6 Po6e6 L'e Heao' al B4> Al,'a Ball
A. Kondisi Operasi 10) D
!e,/ O/6. '?o!e>a'a' CH% lea> ∆P !e,/ 3aa ' a-al6 N a6 NO Be'-> U, -e>'6
)*5 ? *)* oC "2 >?4, 2 A 0."1 = 0.5% ,ol 0.5 = 1.0 >?4, 2 %5* = 500 oC A-a6 Baa8 ) 10 Sl'3e % 8ole
Sl'3e % 8ole
Q 5 -a8'
Q 5 -a8'
!. Rea"si Be3 Ca-al76T1 Be3 Ca-al76T2 Al,'a Ball
Do,e B4>
Rea>-o : Pa4>e3 Be3 ID Ca6-a9le : 2)%" ,, !' : 10)") ,, Ca-al76- : $ol,e
U//e 1%( ,"
Loe 5)(.) ,"
Al,'a Ball : Da De/-8 $ol,e
U//e 1 22* ,, % f-"
Loe 2 )(2 ,, f-"
S-ea, $e'P/e6
Rea>6 3 Se4o'3a7 Refo,e : 2H2O O2 2H2O E>6o-8e,6 CH% H2O CO "H 2 = @20(.2 ?,ol CO H2O CO2 H2O @&%1.2 ?,ol CH% 2H2O CO2 %H2 = @oveall #. Des"ripsi U$%$
Se4o'3a7 Refo,e 9ef'6 6e9aa -e,/a-ea3'7a ea>6 a'-aa e>6e6 CH % 3a /,a7 efo,e 3e'a' 6-ea, ,e'a3 CO; CO 2 3a' H2. Be9e3a 3e'a' /,a7 efo,e 3,a'a >a-al6 9ea3a 3 3ala, -9e; ,a>a 3 6e4o'3a7 efo,e >a-al6 9ea3a 3 ve66el - 6e'3 Aa ea>6 o>63a6 CH % le98 6e,/'a; ,a>a 39-8>a' /a'a6 7a' 9e6a. S,9e /a'a6 33a/a- 3a /a'a6 8a6l ea>6 H 2 3e'a' O 2 3ala, 4o,96-o' o'e. O 2 33a/a- 3a 6//l7 3aa 7a' 6e>al6 6,9e N 2 '-> >e/ela' ea>6 /e,9e'->a' NH " 3 A,,o'a Co've-e. U'-> efe>-f'7a ea>6 H 2 3e'a' O 2; ,a>a 36-96 3aa 3 4o,96-o' o'e 3a- ole8 9'e -/ ? a ,e.
PT. PUPUK SRIWIDJAJA
Hal 15 of 25
Bagian Ammonia P-II
Rev : 00
DEPARTEMEN OPERASI I
Pengaruh Variable Operasi
1. !e,/ea-e ae'a ea>6 9e6fa- e'3o-8e,; >e'a>a' -e,/ea-e a>a' ,e'7e9a9>a' >e6e-,9a'a' ea>6 oveall 9ee6e >e aa8 >o,/o'e' 7a' ,e,el>a' /a'a6 @>e >a'a'. !e,/ea-e 'le-?o-le- )*5 ? *)*oC. Pe'o'-ola' -e,/ea-e 3a/a- 3la>>a' 3e'a' 4aa ,e'a- *+o, %dara -an $as%"/ e$pera%re in+e dari as proses dan e$pera%re %dara in+e . De'a' /e'a,9a8a' 3aa 7a' ,a6>; ,a>a a>a' ,e'a>>a' -e,/ea-e 3a' '-> ,e'aa >o'36 o/ea6 8a6 3>a' /e,9a>aa' 3 /,a7 efo,e. 2. !e>a'a' Pa3a 3a6a'7a; -e>a'a' 9>a'la8 vaa9le o/ea6; 'a,' 9a6a'7a 3aa 6e>-a "1 = "2 >?4, 2. Se4aa ,, 9la -e>a'a' 3'a>>a' ,a>a >e6e-,9a'a' oveall a>a' 9eea> >e ,la8 ,ole>l a- 7a' -e>e4l @>e >. ". o,/o66 I'le- 3a' o-le- CH % lea>ae ,e'e'->a' /o6e6 o>63a6 3 6e4o'3a7 efo,e. Bla CH % o-le- ,a68 -' @K0.5% ,ol; 8al ' 96a -ea3 >ae'a a3a'7a >e'a>a' 6lf 3 3ala, fee3 a6; fee3 a6 3a' 3aa 7a' -3a> 6e,9a'; 3a' la' 6e9aa'7a. %. Fee3 Ra-e ala o'36 /a3a >ea3aa' o/-,, 3a' 3/el>a' /e9a8a' /a3a ala' fee3 a6; 8a6 3la>>a' /e9a8a' 7a' 6e9a'3' /a3a ala' 3aa '-> ,e'aa /e9a'3'a' H 2 3a' N2 -e-a/ @":1; ,ol 5. Hea- Lo66 Hea- Lo66 a'-aa /,a7 3a' 6e4o'3a7 efo,e a-a 3 6e>-a 6e4o'3a7 6a'a- /e'-'. Dala, 3e6' -3a> a3a /a9> NH " 7a' -3a> ,e'ala, 8ea- lo66 a'-aa /,a7&6e4o'3a7; 6e4o'3a7 - 6e'3 a-a -a'6fe l'e 3a 6e4o'3a7 >e a6-e 8ea- 9ole. Bla 8ea- lo66 6a'a9e6a; ,a>a 3/e>a>a' CH % lea> ,a68 -' (. a-al6 No,al loa3' /a3a 66 a-a6 6e>-a 20 3a' 66 9aa8 0. De6' vol,e >a-al6 38-' 3a !H2S$ @-8eoe-4al 873oe' 6/a4e velo4-7 3e'a' vaa9le -e,/ea-e o-leEf6e'6 ,a>6,, 3a o/ea6 efo,' 6e4aa >e6el8a' 38aa/>a' 6e9a'7a> ,'>' /a3a 6aa- /e,9a>aa' /a-al. E'e /e,9a>aa' a>a' ,e'a' 9a8a' 9a>a '-> 3a/ /,a7 efo,e. Na,' ,la8 3aa 7a' ,a6> >e 6e4o'3a7 efo,e 3-e'->a' ole8 >e9-8a' N 2. a3 3a >e6el8a' ea>6 3 efo,e a>a' 3a- ole8 vaa6 68 3 /,a7 efo,e.
PT. PUPUK SRIWIDJAJA
Hal 1( of 25
Bagian Ammonia P-II
Rev : 00
DEPARTEMEN OPERASI I
Na,a Ala!a'al o3e
IG TEMPERATURE SIFT #ON(ERTER 22 A/l 200% 10%&D A. Kondisi Operasi 10 D
Ra648' R' !8e,oell Ca-al76-
!e,/ '?o!e>a'a' a-al6 CO lea> ∆P U, -e>'6
"%" ? %"2 oC "1&"5 >?4, 2 Fe 2O"; /o,o-e3 -8 C 2O" ".0" ,ol 0.2 >?4, 2 Q % & 5 -a8'
!. Rea"si
Rea>6 3 H!S : CO H2O CO2 H2 @&*.)( 4al?,ol #. Des"ripsi U$%$
Al,'a Ball
ID 68ell : "505 ,, S-a8- 63e : 510( ,, Ca-al76De/-8 %2() ,, $ol,e %1.1 ," Ra68' R' De/-8 $ol,e Al,'a Ball De/-8 $ol,e
152 ,, 51.)5 f-"
152 ,, 51.)5 f-"
CO -ele98 3a8l 8a6 39a8 ,e'a3 CO 2 ,elal ea>6 68f- 3 68f- 4o've-e aa 36ea/ ole8 la-a' 9e'fel3 6e-a ,e'a,9a8 /o3>6 a6 H 2. Rea>6 68f- 3la>6a'a>a' 3ala, 2 -a8a/; 7a- -e,/ea-e -' 3a' e'3a8. Rea>6 -e6e9- ,e/a>a' ea>6 eve69le 3a' e>6o-8e,6. Pa3a >ea3aa' ,e'3e>a- >e6e-,9a'a'; /e''a' -e,/ea- a>a' ,e'a>>a' >o've6 3a' 6e9al>'7a >e'a>a' -e,/ea- a>a' ,e''>a' >o've6. !e-a/ /a3a -e,/ea- e'3a8; >e4e/a-a' ea>6 a>a' -' >ae'a >e4e/a-a' ea>6 f'6 3a -e,/ea-. Ole8 >ae'a - /a3a >ea3aa' a8 3a >e6e-,9a'a' @CO ,a68 -'; ea>6 3la>>a' /a3a -e,/ea- -'. e,3a' /a3a >ea3aa' ,e'3e>a- >e6e,9a'a' @CO 63a8 e'3a8; ea>6 3la>6a'a>a' /a3a -e,/ea- 7a' le98 e'3a8 3 L!S '-> ,e,a'faa->a' >e6e-,9a'a' 3,a'a 34a/a >o've6 7a' le98 -'. B6a 3l8a3 af> .1 '-> /e'ela6a' 3 a-a6.
PT. PUPUK SRIWIDJAJA
Hal 1) of 25
Bagian Ammonia P-II
Rev : 00
DEPARTEMEN OPERASI I
ae'a CO 3a/a- a -e3e>o,/o66 ,e'a3 9e'-> >a9o' a-a -e83oe'a6 ,e'a3 CH %; ,la8 6-ea, 7a' 4>/ 6e>-a 20 8a6 a3a '-> ,e'4ea8 8al -e6e9-. Hal ' 36e9a9>a' /a3a -e,/ea- 3 a-a6 121 oC; a>a' -ea3 /e9a8a' 6->- >a-al6 a-a 3e83a6 9la >e9ea3aa' 6-ea, -3a> a3a. Ba6a'7a ala' 6-ea, >e efo,e ,e'a,' 6-ea, ,',, >e 68f4o've-e; a3 -3a> ,e',9l>a' ,a6ala8. %;5 %
3 $o+ #O +ea" 4s Te$p
" ";5 a e " + O 2;5 # + 2 o $1;5 3 1 0;5 0 100
200
"00
%00
500
Gra*i" 5.1
(00
)00
Te$ p 6o#7
Pengaruh Variabel Operasi CO lea> 3a H!SC -ea'-' /a3a >o,/o66 ,/a'; -e,/ea-; -e>a'a'; 6/a4e velo4-7 3a' 6-ea, a6 a6o. Se,a vaa9le ' 6al' 9e89'a' ,elal ea>6 >'e-> ,a/' >e6e-,9a'a'. !e,/ea-e ,e,a'>a' /ea' /e'-' >ae'a 6a'a- 9e/e'a8 >e/a3a a>-f-a6 >a-al6 3a' >o've6.
1. o,/o66 Fee3 Ga6 o'6e'-a6 CO; CO 2 3a' H2 3 3ala, fee3 6a'a- ,e,/e'a8 3ala, ,e'3e6a' H!SC 7a' 9e89'a' 3e'a' >e9-8a' 6-ea,; ,la8 9e3 >a-al6 7a' 39-8>a' 3a' -e,/ea- o/ea6 '-> ,e'3a/a->a' >o've6 7a' 3''>a'. e8a3a' 6lf 3ala, fee3 a6 a>a' 9e/e'a8 /a3a >a' H!SC; 3,a'a 8a6 39a- aa -3a> ,e,/e'a8 a>-f-a6 >a-al6 2. !e,/ea-e !e,/ea- o/ea6 a3ala8 8al 7a' /al' 6e' 3a- 3ala, >o,e6al CO 4o've-e. Efe> 3a -' a-a e'3a8'7a -e,/ea-e 6al' 9elaa'a' f'6 3ala, ea>6 68f- 4o've-e. +ala/' -e,/ea- e'3a8 ,e''>a->a' >e6e,9a'a' /a3a CO lea>ae 7a' e'3a8; !e,/ea- -' a>a' ,e''>a->a' a>-v-a6 >a-al6 7a' 6e9al>'7a ,e''>a->a' >e4e/a-a' ea>6 3a' ,e'3e>a- >o've6 >e6e,9a'a'. Ole8 >ae'a - 3e'a' >o,/o66 'le-; -e>a'a'; 6/a4e velo4-7 3a' S?G a-o 7a' -e-a/ '-> 6/e6f> vol,e 3a >a-al6; a>a' ,e'3e>a- -e,/ea- o/ea6 o/-,,.
PT. PUPUK SRIWIDJAJA
Hal 1 of 25
Bagian Ammonia P-II
Rev : 00
DEPARTEMEN OPERASI I
Na,a Ala!a'al o3e
LO8 TEMPERATURE SIFT #ON(ERTER 22 A/l 200% 10&D A. Kondisi Operasi 105 D
Ra648' R' Ca-al76- Be3
#a' Hole
!e,/ O/6 ,'?,a !e>a'a' CO lea> ∆P a-al6 CO @ - Z'O @ - C68. 6-e'-8
20( ? 2(0 oC "1&"2 >?4, 2 0." ,ol 0." = 0.5 >?4, 2 A-a6 Baa8 1% " = %2 2% 20 & 2% 100 > @aal
5.%% > @aal
Al,'a Ball
!. Rea"si !8e,oell
Rea>6 3 L!S : CO H2O CO2 H2 @&*.)( 4al?,ol Al,'a Ball
ID 68ell : "10 ,, S-a8- 63e : (%01 ,, Ca-al76- : De/-8 $ol,e
U//e **0 ,, %00 f-"
Ra68' R' De/-8 $ol,e Al,'a Ball De/-8 $ol,e
Loe %%)0 ,, 100 f-"
152 ,, (0 f-"
%5) ,, 10 f-"
#. Des"ripsi U$%$
L!S 3ala, o/ea6 'o,al -e,/ea- 3aa /a3a 21( oC. #e6>/' 3e,>a' 3'>a' 9eo/ea6 /a3a -e,/ea- le98 e'3a8 a6al ,a68 3 a-a6 3e /o'- @K ± 10 = 20 oC 3a 4a,/a' a6 3a' 6-ea,. Bla -ea3 >o'3e'6a6; ,a>a la-a' a,,o', 4a9o'a-e a>a' ,ela->a' C 2 a>-f. !e,/ea- o/ea6 3a/a- 3'a>>a' 8'a 2(0 oC; 9la , >a-al6 63a8 -a. o've6 CO 3 L!S ,e,/'7a /e'a8 7a' 6a,a 6e/e- H!S 3ala, /e9a8a' -e,/ea-; a6o 6-ea,&4a9o' 3a' >o,/o66 a6 7a' ,a6>.
Paa,e-e o/ea6 7a' 3''>a' '-> ,e'3a/a->a' CO lea> 7a' >e4l: 1. Ra6o S-ea,&Ga6 6e-' ,'>' +ala/' a6o ' 63a8 -3a> 9e9a8 3a ,la8 6-ea, 7a' ,a6> >e efo,e; a6o 96a 3,o3f>a6 3e'a' Je'48 a'-aa 88 3a' lo -e,/ea-e 6-ae a-a 6-ea, 7a' la'6' ,a6>. Se4aa -eo; ' 3a/a- ,e''>a' CO lea>; 'a,' 6e4aa /a>-> 3a/a,e''>a' , >a-al6. Pa3a '36- 9e6a 8al ' 3,o3f>a6 3e'a' ,e''a>a' '3e4- 4ool' a'-aa H!S 3a' L!S
PT. PUPUK SRIWIDJAJA
Hal 1* of 25
Bagian Ammonia P-II
Rev : 00
DEPARTEMEN OPERASI I
2. !e,/ea- ,a6> 6ee'3a8 ,'>' #',, -e,/ea- ,a6> 39a-a6 ole8 3e /o'- 3a 6-ea, /a3a a6 /o6e6. U'-> ala6a' '; 'le- -e,/ea- 3aa 6e>-a 10 = 20 oC 3 a-a6 3e /o'-. Pa3a /a>->'7a; '-> ,e'4a/a , >a-al6 ,a>6,al 3a' ,',, CO o-le-; -e,/ea- 'le- 3aa 6ela,a ,'>' /a3a /o66 -e,/ea- -ee'3a8 7a' ,a68 ,'>'. >a CO o-le- 'a>; 'le- -e,/ea- 6e8a6'7a 3'a>>a' 2&" oC '-> ,eea>-f>a' >a-al6. Na,a Ala!a'al o3e
METANATOR 22 A/l 200% 10(&D
Al,'a Ball
!8e,oell
Ca-al76-
Al,'a Ball
ID 68ell : 2%" ,, S-a8- 63e : "12 ,, Ca-al76- : De/-8 "151 ,, $ol,e 15.%% ,"
A. Kondisi Operasi 109 D !e,/ O/6 ,'?,a 2(0 ? %5% oC !e,/ '?o"00 = "2 oC !e>a'a' 25 = 2 >?4, 2 a-al6 N : 20 - ,' CO ' "100 //, ?? CO 2 ' 1000 //, CO CO2 o 10 //, @3e6a' 0.5 >?4, 2 ∆P U, -e>'6 Q 10 & 11 -a8' !. Rea"si Rea>6 3 #e-8a'a-o : CO "H2 CH% H2O @&%*." 4al?,ol CO2 %H2 CH% 2H2O @&"*.5 4al?,ol #. Des"ripsi U$%$ CO 3a' CO 2 8a6 39a8 ,e'a3 CH % >ae'a /a3a >o'36 o/ea6 3a' >o'6e'-a6 -e-e'-; >a 9eea>6 3e'a' NH " 3 3aea8 67'-8e6a loo/ 3a/a- ,e'a3 A,,o', Ca9a,a-e 7a' 9e6fa- >oo6f; a4' 9a >a-al6 A,,o'a Co've-e 3a' 3a/a- ,e6a> 63&63 -9' 4o,/e66o 10"&. 1 CO 3 a6 'le- a>a' ,e'a>>a' -e,/ea-e 9e3 )2 oC 1 CO2 3 a6 'le- a>a' ,e'a>>a' -e,/ea-e 9e3 (1 oC
DEPARTEMEN OPERASI I
PT. PUPUK SRIWIDJAJA
Hal 20 of 25
Bagian Ammonia P-II
Rev : 00
Se8'a 9la "100 //, CO 3a' 1000 //, CO 2 a>a' ,e,9e >e'a>a' -e,/ea- 6e9e6a 2.% oC. Pe'o'-ola' -e,/ea-e 'le- 3e'a' ,e'a- 97 /a66 flo a66 /o6e6 o-le- 68ell 10%&C. Pengaruh Variabel Operasi 1. !e,/ea- ae'a ea>6 3e,>a' -' eo-8e,6'7a; ,a>a /a3a ,e-8a'a-o 3/o-e>6 3e'a' 'le- valve '-> ,e'-/ 3a' ve'- a6 9la -e,/ea- 'a> 6e3e,>a' 4e/a-. Hal ' 3la>>a' '-> ,el'3' >a-al6 ,e-8a'a-o 3a' ,e'4ea8 ,a6>'7a CO 3a' CO 2 >e 3ala, 67'-8e6a loo/. e6a>a' >a-al6 /e,a'e' 3a/a- -ea3 ,elal o/ea6 7a' >o'-'7 /a3a -e,/ea- 6e>-a 510 oC
2. !e>a'a' !e>a'a' ,e-8a'a-o 3aa -e-a/ 3a' 9>a' ,e/a>a' vaa9el 3o,'a'. Na,' a'a' ,e''>a' -e>a'a' ,e-8a'a-o 3 9aa8 -e>a'a' 'o,al >a /a3a / 6-ea, ,a68 9e-e>a'a' 'o,al; 6e9el, 7a>' >e3a valve 'le- -e--/ a/a- 3a' ve'- 3a'-aa'7a 39>a. >a -3a>; /e''a' -e>a'a' ve66el /a3a 6aa- -e>a'a' / 6-ea,'7a ,a68 -' ,e'7e9a9>a' a6 7a' ,e'a'3' CO 3a' CO 2 96a ,a6> >e ve66el. ". o'-a,'a' Fee3 a6 /o6e6 8a6 9e68 3a 6lf 3a' /a->el&/a->el 6ol3; >ae'a ,e/a>a' a4' /e,a'e' 9a >a-al6 ,e-a'a-o; 9a8>a' efe>'7a le98 9e6a 39a'3' 3 >a-al6 efo,e. ae'a 9la -ela8 -e>e'a 6lf; ala/' a6 7a' ,a6> >e,9al 9e68; a>-v-a6 >a-al6 -3a> a>a' >e,9al 6e/e- 6e,la; 9e9e3a 3e'a' 3 efo,e. !e,/ea-e ,e-8a'a6 8'a %00 oC 6aa ,a68 9el, 4>/ '-> ,e'6 6lf. o'-a,'a' la' 6e/e- ,'7a>; 3a/a- ,e,9'>6 66 a>-f >a-al6 ,e-8a'a6. U'-> ,e'4ea8 >ea3a' '; 96a 3/a6a' O ol /o6e9el, ,e-8a'a-o '-> ,e,6a8>a' ol 3e'a' >o'-a> >a-al6. o'-a,'a' 9e/a a/ a 3ala, >o'6e'-a6 4>/ -' 3a/a,e'8a,9a- ea>6 ,e-8a'a6
PT. PUPUK SRIWIDJAJA
Hal 21 of 25
Bagian Ammonia P-II
Rev : 00
DEPARTEMEN OPERASI I
Na,a Ala!a'al o3e
#O2 REMO(AL MAIN !ENFIELD 22 A/l 200% 101&E A. Kondisi Operasi 101E dan 102E De,6-' Pa3 LJ3 D6-9-o Fle R' @1.*" ," Pall R' @1).* ,"
101 & E
102 & E CO2 '?oPe'7ea/ S.G. @
Pe66 2 2 @>?4, A !e,/ @oC 122 Pe66 0.* 2 @@>?4, A !e,/ @oC 12( 1 ? 0.1 @ ,ol Be'fel3 @2CO"; DEA; $2O5; UCON 500 HB 1.25 = 1.2* ?44
!. Rea"si
LJ3 D6-9-o Fle R' @% ," Pall R' @"2.1 ,"
Fle R' @% ," Pall R' @2(.2 ," Fle R' @).( ,"
101&E
2CO" 2CO2 H2O 2 HCO" Rea>6 >e >a'a' -ea3 3 A96o9e @101 = E 3a' 9e6fa- e>6o-8e,6 6e3a'>a' >e > -ea3 3 6-//e @102 = E. #. Des"ripsi U$%$ S6-e, CO2 e,oval #a' Be'fel3 9e-a' '-> ,e,'>a' a6 6'-e6a; 7a- ,e,6a8>a' a6 6'-e6a o-le- L!SC 3a CO 2 3e'a' /o6e6 a96o96&6-//'. Po6e6 /e,6a8a' ' ,elal a96o96 >,a ole8 la-a' 2CO" 7a' 3al>a' 9elaa'a' aa8. La-a' 48 Be'fel3 7a' -ela8 ,e'7ea/ CO 2 >ela 3a 9aa8 a96o9e ,e' >e 6-//e '-> 3ee'ea6 >e,9al ,e'a3 la-a' lea' Be'fel3 3a' 6e, lea' Be'fel3 7a' 3'a>a' la '-> ,e'7ea/ CO 2 3 a96o9e.
CO2 8a6 3/6a8>a' >ae'a : CO2 ,e/a>a' 9a8a' 9a> Uea CO2 ,e/a>a' a4' 9a >a-al6 A,,o'a Co've-e 6e8'a 3a/a- ,e,9e'-> a,,o', 4a9a,a-e 3 3aea8 loo/ 7a' ,e'7e9a9>a' >oo6f 3a' ,e,9a8a7a>a' 4o,/e66o 10"&
PT. PUPUK SRIWIDJAJA
Hal 22 of 25
Bagian Ammonia P-II
Rev : 00
DEPARTEMEN OPERASI I
De,6-' Pa3 T1
De,6-' Pa3 T2
LJ3 D6-9-o T1
Hol3 Do' Ga-' Pa4>' S//o-
G3 S//o-
Daoff Pa' LJ3 D6-9-o T2
Daoff Pa'
201&E
o'6e'-a6 CO2 7a' 9e6a 3a o-leL!SC 3a/a,e,9a8a7a>a' >a-al6 ,e-8a'a-o Se/e- 7a' 63a8 3ela6>a' 3 CO 2 e,oval fee3 -ea-'; ,a>a 9e9ea/a 8al 7a' /el 3/e8a->a' 3ala, o/ea6o'al CO 2 e,oval : 1. Ra-e S>la6 8a6 4>/ 2. o'36 !e>a'a' 3a' !e,/ea- 4>/ 9a> ". o,/o66 La-a' Be'fel3 4>/ 9a> %. o'36 U,/a' 4>/ 9a> Dala, 8al /e'4ea8a' >oo6; 3'a>a' va'a3, 6e9aa a'- >oo6. U,,'7a 3 la-a' 9e'fel3 -e3a/a- 10 = 100 //, 9e6. Hal ' ,e'a3 a4a' -'>a- >e9e68a' /a3a /e'44a' aal; 6e/e- a3a'7a /a->el 9e6 ,a6> >e 676-e, ,elal a ,a>e /; 9a8a' >,a -3a> ,' 3a' >o'-a,'a' a6 /o6e6. >a >e4e/a-a' ala' la-a' Be'fel3 ,ele98 'o,al 3a' la-a' 9e9e'-a' la'6' 3e'a' 3'3' 9aa; >oo6 lo4al 3a/a- -ea3 3a' ,e'a,9a8 ,la8 9e6 -ela-. U,,'7a >a3a 9e6 8'a 200&"00 //, 63a8 3a'a/ -'. U'-> ,e'a-a6 8al -e6e9- /el 3'a>>a' >o'6e'-a6 $ 2O5 8'a 0.)&0.-. Pa3a a>- AOP; 676-e, /e'7ea/a' CO 2 -ela8 39a8 ,e'a3 !en*ie+d Lo, ea Pro:ess . S6-e, ' ,e'ea/>a' 6e,&lea' 6ol-o' fla68 7a' 9eo/ea6 6e9aa 9e>-: Se9aa' 6e,&lea' 4a9o'a-e 6ol-o' 3>ela>a' 3a -a/ o- /a' 7a' -ele-a> 3 9aa8 9e3 >e-a 3a' 3al>a' >e 6e, lea' 6ol-o' fla68 -a'> @11*&F. D 3ala, fla68 -a'>; -e>a'a' la-a' 3-'>a' 6e4aa 9e-a8a/ 3ala, % -'>a-. Fla68 6-ea, 3a ,a6' ,a6' -'>a3>e,9al>a' >e 6-//e 3 a-a6 9e3 >e&% 3e'a' ,e''a>a' 6-ea, ee4-o; ,o-ve 6-ea, 3a H! 4o'3e'6a-e e9ole @15"&C 3a' LS 8ea3e. Se, lea' 6ol-o' ,e'al >e /o,/a 6>la6 10)&
PT. PUPUK SRIWIDJAJA
Hal 2" of 25
Bagian Ammonia P-II
Rev : 00
DEPARTEMEN OPERASI I
Na,a Ala!a'al o3e
AMMONIA #ON(ERTER 22 A/l 200% 105&D A. Kondisi Operasi 10; D
!e,/ O/6 '?o!e,/ ,'?,a !e>a'a' Ra6o H2?N2 a-al6 o'6e'-a6 NH "
2%0 ? %20 oC 2(0 ? 520 oC 1"0 & 1(0 >?4, 2 2. = ".0 ,ol Fe @o3e *0 2.1 ? 15&1( ,ol
'?o-
∆P
U, -e>'6
2." = 2. >?4, 2 Q 10 & 12 -a8'
!. Rea"si
Rea>6 3 A,,o'a Co've-e : N2 "H2 2NH" @52.5 ?,ol E>6o-8e,6
#. Des"ripsi U$%$
Rea>-o -7/e /a4>e3 9e3 ,la8 9e3 : " !o-al e'48 : " $ol Be3 -o-al: 50 = 51 , " Be3 Ca-al76>o've-e: !'> a1 2 " !o-al
$ol,e @," %.% *.( 1%.) 2.)
1 F155 ""* 51* 101"
Ga6 7a' 3,'>a' 3-e>a' 8'a (( >?4,2 3 4o,/e66o -'>a- /e-a,a 3a 4o,/e66o 10"& 3a' 33''>a' ,elal " -'>a-a' : 1. #e''a>a' HE '-> ,e,a'a6 a6 7a' a>a' ,a6> ,e-8a'a-o 2. Ga6 33''>a' 3e'a' a /e'3'' 3 '-e6-ae 4oole. ". De'a' a,,o'a> efea'-o' 3 '-e 6-ae 48lle. C8lle a>a' ,e'3''>a' a6 6a,/a oC; 6e8'a a a>a' ,e'e,9' 3a' 3>ela>a' ,elal 6e/aa-o /e-a,a Ga6 67'-8e6a 7a' ,e'a'3' 6e3>- a lal ,e' 4o,/e66o -'>a- II 3a 0"& 3a' 3-e>a' 6a,/a 1"% >?4, 2; 6ela'-'7a a6 ' ,a6> >e 67'-8e6a loo/. Pa3a AOP; 4a-3e6 3 4o've-e 39a " 9e3 >a-al6 3e'a' ,e''a>a' ala' aal a3al. Be3 7a' /al' a-a6
DEPARTEMEN OPERASI I
PT. PUPUK SRIWIDJAJA
Hal 2% of 25
Bagian Ammonia P-II
Rev : 00
,e,/'7a 9e3
Ya' /al' >e4l 39a'3' 9e3 la''7a. e4e'3e'a' /a'a6 ea>6 7a' -,9l 3 9e3 T1 le98 9e6a >ae'a ea>6 7a' /al' 4e/a- -ea3 36'. Pe''aa' '-e4oole 97 /a66 3a' Je'48 a6 flo 3 'le- 9e3 T2 '-> ,e'a- 68 7a' 3l8a->a' ole8 /a'a6 ea>6 aa -e4a/a -e,/ea-e 7a' 3>e8e'3a>. D6-96 >a-al6 3 " 9e3 ,a6' ,a6' 4o've-e 3a/a- 3l8a/a3a >e-ea'a' 3 9aa8 a,9a 4o've-e. Pengaruh Variabel Operasi !e,/ea- 1. Pe'a8 /e9a8a' -e,/ea-e /a3a a,,o'a 4o've-e a3a 2 ,a4a,; 7a- 9e/e'a8 -e8a3a/ persenase "esei$a' >ae'a ea>6 /e,9e'->a' NH " 9e6fa- eo-8e,4; 6e8'a /a3a >e'a>a' 68; ,a>a >e4e/a-a' ea>6 a>a' 'a> -a/ ,e''>a' /e6e'-a6e >e6e,9a'a'. I' ,e''3>a6>a' 9a8a /a3a >o'36 a8 3a >e6e-,9a'a'; >e'a>a' -e,/ea-e a>a' ,e'a>>a' >o've6; -e-a/ 6e9al>'7a /a3a >o'36 ,e'3e>a- 6e-,9a'; >e'a>a' 68 a>a' ,e''>a' >o've6. Hal&8al 7a' ,e'7e9a9>a' >e'a>a' -e,/ea-e a3ala8 : e'a>a' ,la8 a6 7a' ,a6> >e 67'-8e66 Pe'a'a' 3a a6 7a' 36>la6>a' Pe'3e>a-a' -e8a3a/ /e9a'3'a' H 2 : N2 7a' o/-,, e'a>a' -e>a'a' 4o've-e Pe'a'a' ,la8 a6 3'' @Je'48 >e 4o've-e Pe''a' >o'6e'-a6 'e- 3ala, a6 7a' 36>la6>a' e'a>a' a>-v-a6 >a-al6 6e63a8 -ea3 >ea4'a' 6e,e'-aa !e,/ea- 7a' 9a> '-> o/ea6 a3ala8 -e,/ea-e -ee'3a8 7a' ,e'8a6l>a' /o3>6 NH " 6e,a>6,al ,'>' 3e'a' >e6-a9la' 7a' -' -e8a3a/ /e9a8a' -e>a'a'. !e,/ea-e 7a' 9ele98a' a>a' ,e'a' a>-v-a6 >a-al6 3a' ,e,/e/e'3e> lfe -,e >a-al6. 2.
".
!e>a'a' Rea>6 /e,9e'->a' a,,o'a ,e'7e9a9>a' vol,e a>a' 9e>a' >ae'a /e'a'a' ,la8 ,ole>l; ,a>a /e6e'-a6e >e6e,9a'a' /e,9e'->a' NH " a>a' 'a> >ala -e>a'a' 3'a>>a'. e4e/a-a' ea>6 ,e''>a- ole8 >e'a>a' -e>a'a'; ,a>a >o've6 a>a' 'a> /a3a -e>a'a' -' S/a4e $elo4-7 >a ,la8 a6 /o6e6 ,a>' 9e-a,9a8 @6/a4e velo4-7 3ala, 4o've-e le98 -' ,a>a a>- ea>6 67'-8e66 a>a' le98 6e3>- 6e8'a a6
DEPARTEMEN OPERASI I
PT. PUPUK SRIWIDJAJA
Hal 25 of 25
Bagian Ammonia P-II
Rev : 00
>ela a,,o'a 4o've-e ,e'a'3' 6e3>- NH " 39a'3' >ala >e4e/a-a' a6 7a' ,e'al >e 4o've-e le98 la,9a-. Na,' 8a6l'7a -3a> /o/o6o'al 39a'3'>a' 3e'a' >e'a>a' 6/a4e velo4-7. e'a>a' /o3>6 NH " >ae'a ,la8 a6 7a' ,e'al >a-al6 +ea&>a ":1. Se4aa -eo-6 3a/a- 3ela6>a' 9a8a 39-8>a' 1 ,ol N 2 3a' " ,ol H 2 '-> ,e,9a- 2 ,ol NH ". Na,' /a3a 4o've-e; /e9a'3'a' H 2 3a' N2 7a' o/-,, 9ea3a /a3a 2.5 : 1 6a,/a ".0 : 1. Ra6o 3ala, fee3 a6 9ole8 9e9a8 3a " : 1 '-> ,e'3a/a->a' a-o o/-,, 3ala, a6 4a,/a' 3e'a' a6 'e- 7a' >e ea4-o. Hal 7a' 3a/a- ,e9a8 /e9a'3'a' H 2 3a' N 2 a3ala8 : Pe9a8a' >o,/o66 a6 3a 3aea8 efo,' 3a' /f4a-o'. Pe9a8a' >e4e/a-a' a6 6'-8e6a Pe9a8a' ,la8?>o'6e'-a6 NH " 3ala, a6 7a' 36>la6>a' Pe9a8a' a6 'e- 3a a6 7a' 36>la6>a'. Ga6 I'eSe,la8 a6 7a' 3>ela>a' 6e4a >o'-'7 ,elal 64-o' 4o,/e66o 10"& >e 676-e, /e a6. Ala' /e ' a>a' ,e'a- >o'6e'-a6 CH% 3a' Ao' 7a' -ea>,la6 3 aea 67'-8e6a loo/. I' a>a' ,e'7e9a9>a' >e'a>a' -e>a'a' 3 3ala, 676-e, 6e8'a -e>a'a' /a6al 3a a6 6'-8e6a a>a' -' 6e8'a 3a/a- ,e''>a' >o've6 3a' >a/a6-a6 /o3>6 e4e/a-a' a6 6'-8e6a e'a>a' >e4e/a-a' a6 6'-8e6a a>a' ,e'a,9a8 /o3>6 NH " -e-a/ a>a' 9ea>9a- /a3a : !e>a'a' 676-e, a>a' 'a> !e,/ea- 9e3 >a-al6 'a> a'3'a' a6 'e- 'a> Ra6o H2 = N2 a>a' 9e9a8 Hal ' 9ela> 6e9al>'7a. Pa3a >o'36 o/ea6 'o,al; >e4e/a-a' a6 3-e'->a' ole8 >e9-8a' /o3>6. e'a>a' a-e a6 >e 4o've-e 3a/a34a/a 3e'a' ,e'a>>a' a-e /o3>6 3 3aea8 3e/a''7a.
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