suc de mere

Memoriu justificativ Lucrar Lucrarea ea işi propun propunee prezen prezentar tarea ea princi principal palelo elorr aspect aspectee legate legate de sucurile sucurile naturale naturale de fructe: compoziţi compoziţiaa fructelor, metode metode de preparare, ambalare ambalare,, aparatura şi liniile aferente. În ulti ultimu mull timp timp,, sucu sucuri rile le de fruc fructe te au căpă căpăta tatt o larg largăă util utiliz izar are, e,  putându-se vorbi de o terapie terapie prin scuri de fructe în cele cele mai diverse afecţiuni. Lipsa totală a unei vitamine e gravă, dar mai rar întalnită. e cele mai multe ori, apare o lipsă parţială a vitaminelor, iar tulburările metabolice în acest caz sunt mai puţin grave. !"cesul de vitamine poate duce la #ipervitaminoze, care se manifestă, de obicei prin apariţia unor dezec#ilibre în organism. Însă cei mai mulţi dintre noi se confruntă cu o lipsă, nu cu un surplus în organism. $cest lucru se rezolvă consumand o cantitate mare de legume şi fructe proaspete. %ructele mai conţin şi fibre alimentare, care nu au valoare energetică, dar care sunt deosebit de utile pentru aparatul digestiv. %ibrele solubile &conţinute în mere' frânează absorbţia za#ărului, dar pot împiedica absorbţia unei părţi a colesterolului asimilat odată cu alimentele şi a(uns în intestin împreună cu bila. )ai trebuie menţionat faptul că fructele au un conţinut ridicat de apă în ma(oritatea cazu cazuri rilo lorr ap apro ro"i "ima mati tivv *+ *+. . rot rotei eine nele le se gă găse sesc sc în co conc ncen entra traţi ţiii de sub sub , , neprezentând interes special. %ructele sunt însa o sursă foarte bună de glucide, în special solubile dintre care: glucoza, fructoza /ucurile de fructe conţin cea mai mare parte de glucide, vitamine şi săruri minerale minerale a materiilo materiilorr prime având valoare nutritivă nutritivă şi dietetică. dietetică. 0 cantitate cantitate mare de glucide din sucuri este sub formă de fructoză fiind tolerată şi de diabetici. atorită conţinutului mare de săruri de potasiu, sucurile de fructe dau bune rezultate în tratamentul şi profila"ia bolilor cardio- vasculare. /e ştie că sodiul are 

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capacitatea de a reţine apa în organism, iar potasiul favorizează eliminarea ei. În dieta cu sucuri de fructe cantitatea de potasiu este de 1 ori mai mare decât în dieta normală. $stfel sucurile acţionează favorabil asupra întregii activităţi a muşc#iului cardiac, măresc travaliul inimii având efecte benefice în bolile cardio- vasculare: #ipertensiu #ipertensiune, ne, infarct infarct miocardic, miocardic, arterosclero arteroscleroză./u ză./ubstan bstanţele ţele minerale minerale &calciul &calciul şi  potasiul' au un efect alcalinizant neutralizând acidul clor#idric din mucoasa stomacală, fiind indicate în combaterea #iperacidităţii în cazul bolilor digestive. /ucurile sunt indicate şi în bolile de ficat sau ale vezicii biliare datorită absenţei grăsimilor şi cantităţii mari de za#aruri şi vitamine. atorită conţinutului redus de substanţe azotoase şi a acţiunii de alcalinizare, sucurile de fructe sunt indicate în bolile de rinic#i acute şi cronice. $cestea previn formarea calc calcul ulil ilor or rena renali li sau sau bili biliar arii şi sunt sunt

reco recoma mand ndat atee atun atunci ci când când organ organism ismul ul

acum acumul ulea ează ză o cant cantit itat atee ma mare re de aciz acizii în diab diabet et,, subn subnut utri riţi ţiee şi îmbă îmbătr trân ânir irea ea ţesuturilor. În cazurile de obezitate, cura cu sucuri de fructe atenuează senzaţia de foame şi permite eliminarea e"cesului de apă datorită sărurilor de potasiu. /ucurile de fructe au o actiune antiinfecţioasă şi antimicrobiană fiind recomandate în diverse boli ale pielii2 au acţiune antito"ică prin protecţia asupra: ficatului, splinei, rinic#i &sucul de mere, struguri, caise, coacăze negre'. 3a urmare a acestui fapt, industria sucurilor de fructe s-a dezvoltat încercând obţinerea de produse de o calitate superioară. Lucrarea de faţă este structurată în mai multe părţi, fiecare dintre acestea având o importanţă deosebită în realizarea a ceea ce se numeşte produs finit.

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1. TEMA PROIECTULUI ime imens nsio iona nare reaa un unei ei secţ secţii ii de ob obţi ţine nere re a sucu suculu luii de me mere re cu o capacitate de 5 tone pe zi produs finit.

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2. TEHNOLOGIA TEHNOLOGIA FABRICĂRII FABRICĂRII SUCULUI DE MERE 2.1. PROPRIETĂŢILE PRODUSULUI FINIT 2.1.1. CULOAREA, GUSTUL ŞI AROMA SUCULUI DE MERE /ucurile de fructe sunt produse destinate consumului direct şi sunt obţinute prin e"tragerea sucului celular din fructe prin presare. in punct de vedere te#nologic sucurile de fructe pot fi clasificate în sucuri fără pulpă &limpezite' şi sucuri cu pulpă &nectare'. /ucurile naturale sunt cele obţinute dintr-un singur fruct, iar cele cupa(ate sunt obţinute prin amestecarea a două, trei sucuri de specii de fructe diferite. La prelucrarea merelor în vederea obţinerii sucului s-a stabilit că 4 parametrii esenţiali ai sucurilor sucurilor culoarea şi aroma, sunt foarte foarte sensibili, în sensul că suferă suferă degradări atunci când a(ung în contact cu diferiţi factori inevitabili în timpul prelucrării. intre factorii care influenţează negativ calitatea aromelor şi coloranţilor din sucuri cei mai importanţi sunt fenomenele de o"idare, căldura şi manipulările. manipulările. Culoarea

limpede trebuie să fie alb 7 gălbuie până la slabe nuanţe de verde, în

funcţie de soiul supus prelucrării.  Aroma  este

plăcută specifică merelor utilizate ca materie primă, fără mirosuri

străine de mucegai sau oţet. $romele sunt componente volatile şi se găsesc în cantităţi foarte mici, cel mai adesea sub  p.p.m. $romele fructelor rezultă prin combinarea unui nr. mare de substanţe. În cazul aromei de mere, nr. de substanţe aromate depăşeşte cifra de 8+. rincipalele substanţe aromatizante identificate la mere sunt: alcooli cca *4 , alde#ide 1  şi eteri 4 . eoarece aromele sunt volatile se poate împiedica pierderea lor din sucuri, prin evitar evitar

încălz încălziri iriii tim îndel îndel gat la tem

aturi aturi mai

i decât decât cel indic indicate ate şi evitar evitar

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În cazul în care sucurile se brunifică prin reacţii de o"idare enzimatice sau neenzimatice are loc şi o alterare a aromelor. $stfel sucul devine înc#is la culoare fără gust şi aromă specifică.

2.1.2. DEFECTE ŞI REMEDII ÎN OBŢINEREA SUCULUI DE MERE $ccidentel $ccidentelee si defectele defectele de fabricaţie fabricaţie ale sucurilor sucurilor sunt, sunt, de cele mai multe ori, datorate microorganismelor care pot afecta parţial sau total calitatea acestora. /c#imbări mai  profunde se datorează mucegaiurilor, mucegaiurilor, care elaborează enzime pectolitice

ce pot produce

clarificar clarificarea ea sucurilo sucurilor. r.  Phyalophora mustea  poate produce o îmbrunare a sucurilor după cum aspectul aspectul micilagin micilaginos os poate fi produs datorită datorită prezenţei prezenţei speciilor speciilor  Leuconostoc. În sucuri pot apărea anumite cantităţi de alcool, uneori din folosirea unei materii prime ce a suferit un proces lung de depozitare datorate propriilor enzime din ţesutul vegetal. rocesul de apariţie a alcoolului se datorează în principal dro(diilor dro(diilor şi mai rar a mucegaiurilor şi bacteriilor. /e ştie că o dată cu zdrobirea unui măr imediat încep modificări ale culorii &se  brunifică' ca urmare a e"punerii pulpei şi sucului la un contact direct cu 0 4 din aer. $ceastă modificare a culorii este rezultatul activităţii enzimelor o"idante care se pot dezvolta în mediu  prielnic. /e mai constată că în acest caz au loc distrugeri ale aromei şi ale substanţelor substanţelor colorante specifice. 0dată cu pierderea integrităţii fructelor, la zdrobire sau când sunt lovite,în locurile unde coa(a, pieliţa sunt distruse în contact cu aerul atmosferic, apar imediat fenomene de fermentare sau mucegăire şi oţetire. %enomenul de o"idare enzimatică poate fi prevenit prin prezenţa vitaminei 3, care împiedică transformarea polifenolidelor polifenolidelor în substanţe de culoare brună. 0"idă 0" idăril rilee neenzi neenzimat matice ice se dator datoreaz eazăă unor unor reacţi reacţiii de o"idar o"idaree accele accelerat ratee de  prezenţa sărurilor de fier şi cupru. $ceste săruri pot a(unge în sucuri în urma contactului cu utila(e confecţionate din %e şi 3u pe care acizii din suc le atacă uşor. $stfel se recomandă construirea utila(elor din materiale rezistente la acţiunea

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vedere respectarea parametrilor unei pasteurizări eficiente şi o îmbuteliere corespunzătore care să asigure condiţiile de calitate necesare păstrării pe timp îndelungat. )ăsurile de prevenire a accidentelor datorate microorganismelor, se realizează  prin respectarea duratelor de sterilizare şi fără derogări de la igienă din cadrul flu"ului te#nologic. urate prelungite ale tratamentelor termice pot conduce la sc#imbarea culorii şi gustului gustului,, prin formarea formarea #idro"i#idro"i-meti metil-fur l-furfuro furolulu lului.i. rezenţa rezenţa acestuia acestuia s-a constatat constatat în cazul depozitării la temperaturi de peste 6+  >

5+5,*1 +,**

> %1198 A#:h

%. 7ilanţul de materiale pentru operaţia limpezire.

unde ;  ) enzime cantitatea de enzime adăugată pentru limpezire2 - ) suc limpede cantitatea de suc limpede rezultată în urma limpezirii2 - ) reziduu cantitatea de reziduu obţinută in urma decantării impurităţilor din suc. !cuaţia de bilanţ este: ) suc brut M ) enzime > ) suc limpede M ) reziduu ) reziduu > +,4 · ) suc brut > +,4· 68*,81 > 39- A#:h ) enzime > +,+6·D*,D > +,85 g ) suc brut M +,+6· ) suc brut > ) suc limpede M +,4· ) suc brut ) suc brut &,+6 -+,4' > )  suc limpede ) suc brut >

6+5,8*1 +,D6

 > 3594- A#:h

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-. 7ilanţul de materiale pentru operaţia de filtrare.

unde: - ) suc filtrat cantitatea de de suc filtrat. !cuaţia de bilanţ este: ) suc limpede > ) suc filtrat M  ) suc limpede &-+,' > )  suc filtrat ) suc limpede >

484,.5* +,D*

 > 38%95- A#:h

 > +,· ) suc limpede >+, ·6+5,8*1 > 339-3 A#:h

. 7ilanţul de materiale pentru operaţia de adaosuri.

unde: - ) e"tract cantitatea de e"tract adăugată în suc2 - ) vit 3 cantitatea de vitamina 3 adăugată - ) suc cantitatea de suc rezultată. !cuaţia de bilanţ este: ) suc filtrat M ) e"tract M ) vit 3> ) suc )

 >+,+++5 · )

 > 8913- A#:h

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) e"tract  > +,5 · ) suc filtrat > 4892 A#:h ) suc filtrat & M+,5+5' > ) suc ) suc filtrat >

6.6,.4 .,.5+5

 > 2291%5 A#:h

. 7ilanţul 7ilanţul de de material materialee pentru pentru operaţia operaţia de $mbutel $mbuteliere. iere.

unde: - ) suc final cantitatea de suc ce rezultă în urma urma procesului te#nologic. te#nologic. !cuaţia de bilanţ: ) suc > ) suc final M   > +,++4 · ) suc > +,++4 ·66,4 > 89-2 A#:h ) suc & -+,++4' > )  suc final ) suc >

6.4,5 +,**D

 > 313912 A#:h  25952 l:h /

Consumul specific Cs este calculat cu relaţia: 3 s >

 . mere  .  suc

  final 

 >

54D,65 6.4,5

 > ,1*

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acă bilanţul de materiale serveşte la urmărirea circulaţiei materialelor printr-o instalaţie şi face posibilă determinarea randamentului de fabricaţie şi a dimensiunilor instalaţiei respec respectiv tive, e, întocm întocmire ireaa bilanţ bilanţulu uluii termi termicc permit permitee stabil stabilire ireaa necesa necesarul rului ui de căldu căldură ră pentr pentruu desfăşurarea în bune condiţii a procesului te#nologic. @ilanţ @ilanţul ul termic termic se întoc întocmeş meşte te după după ce se cunoaş cunoaşte te bilan bilanţul ţul de materi materiale ale şi  proprietăţile  proprietăţile termodinamice ale materialelor ce intră şi ies din proces. În general bilanţul termic  poate fi e"primat cu relaţia: relaţia:

∑/ = ∑/ + ∑/ i

e

pi

în care: ^i , ^ e, ^ pi 7 reprezintă: căldurile căldurile intrate, ieşite şi respectiv respectiv pierderile de căldură. căldură. @ilanţul termic se va realiza pe baza unei sc#eme realizate, considerată fiind mai eficientă datorită recirculării sucului pasteurizat in vederea unui consum scăzut de abur ca agent termic. $stfel sucul nu este trecut din zona de menţinere direct în zona de răcire, ci este folosit ca agent termic la operaţia de preîncălzire $ceasta este sc#ema de funcţionare a sc#imbătorului de căldură care are patru zone de lucru. lucru.

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unde: -

^  > m · 3 p · t 1

&ZGs'

căldura sucului supus preîncălzirii

-

^ 4 > m 4· 3 p4 · t 2

&ZGs'

căldura agentului termic &în cazul nostru suc'

-

^ 6 > m · 3 p6 · t 3

&ZGs'

căldura sucului preîncălzit

-

^  > m 4· 3 p · t 4

&ZGs'

căldura agentului termic uzat

!cuaţia de bilanţ este: ^  M ^ 4 > ^ 6 M ^  M ^  &considerate > + ' ^  - ^ 6 > ^  - ^ 4 m · 3 p · t 1 - m · 3 p6 · t 3 > m 4· 3 p · t 4 - m 4· 3 p4 · t 2 m  &3 p · t 1 - 3 p6 · t 3 ) = m 4 &3 p · t 4 - 3 p4 · t 2 ' m  · 3 p mediu · & t 7 t6 ' > m 4 · 3 p mediu · & t 7 t4 ' m  · 3 p 64,5 · & t 7 t6 ' > m 4 · 3 p 18,5 · 45

& t 7 t6 ' >

m

4

⋅ C  P  C  P 

18 , 5

⋅ 45

64, 5

t  > t  M 45,5 > 4%9% º C

 > 45,5

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unde: - ^  4 > m $b· 3 p4 · t 2 - ^  > m $b uzat · 3 p · t 4

&ZGs'

căldura agentului de pasteurizare

&ZGs'

căldura agentului de pasteurizare uzat

 ^  > m · 3 p · t 1

&ZGs'

căldura sucului supus pasteurizării

 ^ 6 > m · 3 p6 · t 3

&ZGs'

căldura sucului pasteurizat

!cuaţia de bilanţ este: ^  M ^ 4 > ^ 6 M ^  M ^  &considerate > + ' ^  - ^ 6 > ^  - ^ 4 m · 3 p · t 1 - m · 3 p6 · t 3 = m $b uzat · 3 p · t 4 - m $b· 3 p4 · t 2 m $b uzat = m $b m ( 3 p · t 1 - 3 p6 · t 3) = m $b ( 3 p · t 4 - 3 p4 · t 2 ) C P 62,75 = 3627,77 ZG&Jg X'

3 4+ > 44 ZG&Jg X' +,51 · 6148,88 · 6,5 > m $b · 44 · 6+

m 0b B 8922 A#:s  1 A#:h/

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unde: -

^  > m · 3 p · t 1

&ZGs'

căldura sucului supus răcirii

-

^ 4 > m $r · 3 $r  · t 2

&ZGs'

căldura agentului de răcire

-

^ 6 > m · 3 p6 · t 3

&ZGs'

căldura sucului răcit

-

^  > m $r uzată· 3 $r uzată · t 4

&ZGs'

căldura agentului de răcire uzat

!cuaţia de bilanţ este: ^  M ^ 4 > ^ 6 M ^  M ^  &considerate > + ' ^  - ^ 6 > ^  - ^ 4 m · 3 p · t 1 - m · 3 p6 · t 3 = m $r uzată · 3 $r uzată · t 4 - m $r · 3 $r  · t 2 m $r uzată = m $r   ( 3  $r uzată · t 4 - 3 $r  · t 2 ) m ( 3 p · t 1 - 3 p6 · t 3) = m $r  (

3  + > 65D+ ZG&Jg X' 3  8,5 > 4+ ZG&Jg X' +,51 · 65D+ · 6+ > m $r · 4+ · 5

m 0r B 89%518 A#:s  2129% A#:h/

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3.1.UTILA#UL PRINCIPAL.

0le#erea utilajului asteurizarea rapidă se utilizează în special la conservarea produselor lic#ide înainte de îmbuteliere. În acest scop se va folosi o instalatie de pasteurizare ce realizează  pasteurizarea sucului la temperatura de 8+- D+ X · $· ΔFm  - X coeficient global de transfer termic, [G &m 4 X'2 -  ΔFm diferenţa medie de temperatură temperatură intre agentul agentul de încălzire şi suc, X2 - $ aria suprafeţei de transfer termic, m 4. 3ăldura cedată s-a calculat în bilanţul termic: ^ > 4+51,8 ZGs iferenţa medie de temperatură se calculează astfel:

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Bnde: - α coeficient parţial de transfer de căldură al sucului, [G&m 4 X'2 - α4 coeficient parţial de transfer de căldură al agentului de încălzire, [G&m 4 X'2 - δ grosimea plăcii, m2 - λ conductivitatea plăcii, [G&m X'2 3aracteristicile termofizice ale sucului la F med >64,4 şi F med > 18,5 sunt prezentate sub formă de tabel: Femperatura º 3

ensitatea ρ

3apacitatea termică masică 3, ZG&Jg X' 651,4 6168,85

XgG m6 64,5 18,5

+D+ ++

Ompunem o viteză de curgere v  > +,5D mGs n>

 . m

 ρ  ⋅ v. ⋅ S +

+,..51

=

.+D+ ⋅ +,5D ⋅ 161 ⋅ .+

n- numărul de canale, v- viteza de curgere, mGs /+- aria secţiunii de curgere, m 4

−1

 > +,4* canale

Eâscozitate dinamică , η ma ·s ,448 +,116

3onductivitate termică λ, [G&m X' +,5+ +,55

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$vem regim de curgere intermediar şi pentru acest regim calculez Husselt:  Hu > c· Ie+,8D·r +,1·ε > +,+15·(6+16,+D' +,8D·D,8+,1· ,1*  Hu > 5,8 3alculul valorii randtl: C  p ⋅η  651:, 4 ⋅,448 ⋅+ −6 = r > > D,8 λ 

+,5+

+., 45

  -r      ε  =   -r  p      

 Hu >

α . ⋅  ech λ 

+ , 45

 D,8:   =    ,+5   ⇒

α .

=

= ,1*

.5:,8: ⋅ +,5+ 1 ⋅ .+

−6

  >4D*5 [G&m4 X'

entru agentul termic: Ie >

⋅ ⋅

 ρ  v  ech η 

=

+,5D ⋅ +,++1 ⋅ ..++ +,116 ⋅ .+−6

 > 5886,85

3alculul valorii Husselt:  Hu > c· Ie+,8D·r +,1·ε = 5,*1 3alculul valorii randtl: C  p ⋅η  6168,85 ⋅ +,116 ⋅+ − = r > > ,6D 6

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3alculul numărului de canale: m> n - >  Lungimea zonei de preîncălzire este: L > 4 δ pc M δ pi M n δ p M m δc - δ pc grosimea plăcii de capăt, - δ pi grosimea plăcii intermediare, - δ p grosimea , - δc distanţa dintre plăci. L > 44+ M 84 M 5 M4 > 385 mm

89385 m/

Calculul dimensiunilor tehnolo#ice  zona de $ncălzire.

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.

X>

. α .

δ  +

λ 

+

.

` [G & m4 X' 

α 4

Bnde: - α coeficient parţial de transfer de căldură al sucului, [G&m 4 X'2 - α4 coeficient parţial de transfer de căldură al agentului de încălzire, [G&m 4 X'2 - δ grosimea plăcii, m2 - λ conductivitatea plăcii, [G&m X'2 3aracteristicile termofizice ale sucului la F med >14,85 şi ale aburului laF  med > 4+ sunt prezentate sub formă de tabel: Femperatura º 3

ensitatea ρ XgG m6

3apacitatea termică masică 3 ZG&Jg X'

Eâscozitate dinamică , η ma

3onductivitate termică λ, [G&m X'

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 Hu >

α . ⋅  ech λ 

⇒

α .

=

.*D,81 ⋅ +,5: 1 ⋅ .+

−6

  >8DDD,*4 [G&m 4 X'

entru agentul termic: Ie >

⋅ ⋅

 ρ  v  ech η 

=

+,6D ⋅ +,++1 ⋅ ..4. .4,D+ ⋅ .+ −6

 > 4+,+6

3alculul valorii Husselt:  Hu > c· Ie +,8D·r +,1· ε = **D,+5 3alculul valorii randtl: r >

C  p ⋅η 

λ 

=

+., 45

  -r      

4.4: ⋅.4,D+ ⋅.+ −6 +,+41 + , 45

 +:5 11  

> +5,11

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- δc distanţa dintre plăci. L > 44+ M 84 M 5 M4 > 385 mm

89385 m/

Calculul dimensiunilor tehnolo#ice  zona de răcire. 3alculul suprafeţei de transfer termic: ^ > X · $· ΔFm  - X coeficient global de transfer termic, [G &m 4 X'2 -  ΔFm diferenţa medie de temperatură temperatură intre agentul agentul de încălzire şi suc, X2 - $ aria suprafeţei de transfer termic, m 4. 3ăldura cedată s-a calculat în bilanţul termic: ^ > 61*61,54 ZGs iferenţa medie de temperatură se calculează astfel:

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- λ conductivitatea plăcii, [G&m X'2 3aracteristicile termofizice ale sucului la F med >+ şi ale apei la F med > 8,5 sunt prezentate sub formă de tabel: Femperatura º 3

ensitatea ρ XgG m6

+ 8,5

+D5 ***,

3apacitatea termică masică 3, ZG&Jg X' 65D+ 4+

Ompunem o viteză de curgere v  > +, mGs n>

 . m

 ρ  ⋅ v. ⋅ S +

=

+,..51 .+D5 ⋅ +,: ⋅ 161 ⋅ .+

−1

 > +, canale

Eâscozitate dinamică , η ma ·s ,+D6 ,+85

3onductivitate termică λ, [G&m X' +,5+5 +,5*+

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 Hu > c· Ie +,8D·r +,1· ε = 4,1+ 3alculul valorii randtl: r >

C  p ⋅η 

λ 

=

+ 45

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3onsiderăm diametrul secţiunii secţiunii de curgere în zona de menţinere d > 6++mm. /> v>

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Onstalaţiile moderne de sortare au banda construită din role de oţel ino"idabil ce se rotesc în (urul a"ului, permiţând e"punerea întregii suprafeţe a fructului şi o mai bună sortare. entru unele operaţii de sortare calitativă, în special sortarea după culoare, s-a înlocuit sortarea manuală cu sortarea pe bază de celule fotoelectrice.

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Tabelul 1. Caracteristicile tehnice sunt următoarele: 3apacitatea de prelucrare 3apacitatea cuvei 3onsumul de apă Lăţimea benzii

6 +++ 75 +++ JgG#  m6 4,5 m6G# 1*+ mm

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PRESA HIDRAULICĂ. În industria sucurilor se folosesc prese discontinue cu şurub #idraulice şi prese continue cu şurub. 3aracteristice pentru industria sucurilor de fructe sunt presale #idraulice cu  pac#ete sau eta(e, care permit obţinerea obţinerea unui randament randament mai ridicat, datorită datorită faptului că stratul stratul de

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entru o lună: 3 $L >

C  A%  4

 > 38%9%88- 61 m

l > 4 m

= > ,5 m.

/ > & 61 " ,5 " 4 ' M &4 " ,5 " 4 ' M & 4 " 61 ' > 12-5 m2 Suprafa Suprafaţa ţa

pereţi pereţilor lor interi interiori ori

se compun compunee din (umăta (umătatea tea difer diferenţ enţei ei dintre dintre

suprafaţa totală şi suprafaţa pereţilor e"teriori: / i >

S t  − S e7t 

4

 >

68+*, −41* 4

> 44+,+5 m 4

eci suprafaţa construită a clădirii este:  44+,+5 M 41* > 24598% m2

6aloarea suprafeţei construite &i a terenului. ?r )estinaţia spaţiului Crt. 1 !ecţia de fabricare suc L> 41m l> D m => ,5 m - pere pereţi ţi lung lungi: i: 41 " ,5 ,5 " 4 > 46 46 - pere pereţi ţi scur scurţi ţi:: D " ,5 ,5 " 4 > 84 84 palfon M pardosea: 41 " D " 4 > 1 2 )epozit produs finit L> Dm l> 6 m => ,5 m - pere pereţi ţi lung lungi: i: D " ,5 ,5 " 4 > 84 - pere pereţi ţi scur scurţi ţi:6 :6 " ,5 ,5 " 4 >48 >48 palfon M pardosea: D " 6 " 4 > D 3 )epozit materie primă L> *m l> 1 m => ,5 m - pere pereţi ţi lung lungi: i: * " ,5 ,5 " 4 >D >D - pere pereţi ţi scur scurţi ţi:1 :1 " ,5 ,5 " 4 > 5 5 palfon M pardosea:1 * 4 +D

!uprafaţa construită9m2

22

14

243

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%

-





5

18

11

12

13

palfon M pardosea: D " 6 " 4 > D 7irou &ef secţie L> 6m l> 6 m => ,5 m - pere pereţi ţi lung lungi: i: 6 " ,5 ,5 " 4 > 48 - pere pereţi ţi scur scurţi ţi:: 6 " ,5 ,5 " 4 > 48 48 palfon M pardosea: 6 " 6 " 4 > D 0telier mecanic L> 8 m l> 6 m => ,5 m - pere pereţi ţi lung lungi: i: 8 " ,5 ,5 " 4 > 16 - pere pereţi ţi scur scurţi ţi:6 :6 " ,5 ,5 " 4 > 48 48 palfon M pardosea: 8 " 6 " 4 > 4 0telier electric L> 1 m l> 6 m => ,5 m - pereţi lungi: 1 " ,5 " 4 > 5 - pere pereţi ţi scur scurţi ţi:6 :6 " ,5 ,5 " 4 >48 >48 palfon M pardosea: 1 " 6 " 4 > 61 !ecretariat L> 6 m l> 6 m => ,5 m - pere pereţi ţi lung lungi: i: 6 " ,5 ,5 " 4 > 48 - pere pereţi ţi scur scurţi ţi:: 6 " ,5 ,5 " 4 > 48 48 palfon M pardosea: 6 " 6 " 4 > D 7irou director L> 5 m l> 6 m => ,5 m - pere pereţi ţi lung lungi: i: 5 " ,5 ,5 " 4 > 5 - pere pereţi ţi scur scurţi ţi:: 6 " ,5 ,5 " 4 > 48 48 palfon M pardosea: 5 " 6 " 4 > 6+ !ală de protocol L> 1,6 m l> 6 m => ,5 m - pere pereţi ţi lung lungi: i: 1,6 1,6 " ,5 ,5 " 4 > 51,8 51,8 - pere pereţi ţi scur scurţi ţi:6 :6 " ,5 ,5 " 4 > 48 48 palfon M pardosea:1,6 " 6 " 4 > 68,D 7iro 7irouu admi admini nist stra raţi ţiee &i cont contab abil ilit itat atee L> 5,* m l>  m => ,5 m - pere pereţi ţi lung lungi: i: 5,* 5,* " ,5 ,5 " 4 > 56, 56, - pere pereţi ţi scur scurţi ţi:: 6 " ,5 ,5 " 4 > 48 48 palfon M pardosea:5,* " 6 " 4 > 65, 6estiar femei L> 1,5 m l> 1 m => ,5 m - pere pereţi ţi lung lungi: i: 1,5 1,5 " ,5 ,5 " 4 > 5D,5 5D,5 - pere pereţi ţi scur scurţi ţi:1 :1 " ,5 ,5 " 4 > 5 5 palfon M pardosea: 1,5 " 1 " 4 > 8D GC  du& fe femei L> , m l> 6 m => ,5 m

2

132

11

2

182

  1219%

11%9%

  1589%

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L> 1 m

1%

11 1 15

l> 6 m => ,5 m - pere pereţi ţi lung lungi: i: 5,5 5,5 " ,5 ,5 " 4 > *,5 *,5 - pere pereţi ţi scur scurţi ţi:6 :6 " ,5 ,5 " 4 > 48 48 palfon M pardosea: 5,5 " 6 " 4 > 66 GC  du& bărbaţi L> 5 m l> 6 m => ,5 m - pere pereţi ţi lung lungi: i: 5 " ,5 ,5 " 4 > 5 - pere pereţi ţi scur scurţi ţi:6 :6 " ,5 ,5 " 4 > 48 48 palfon M pardosea: 5 " 6 " 4 > 6+ Culoar 1. L> 61 m l> 4 m =>,5 m Culoar 2. L> 41 m l> 4 m => ,5 m Culoar 3. L> 1 m l> 4 m => ,5 m Culoar 4. L> D,5 m l> , m => ,5 m

  1859%

182

--3%518%91

!uprafaţa totală

38591

'aloarea cl#irii(

entru construirea unui m 4 de clădire clădire sunt sunt necesa necesari ri -8 %888 ,* & 6: 4 vol'.

•

6. )od de lucru. Într-o eprubetă cu dop rodat se introduc: 5 ml e"trac diluat de 5+ de ori, 5 ml amestec n butanol-=3l şi se omogenizează bine. /e citeşte e"tincţia la 55+ nm, în cuvă de + mm, faţă de soluţia de n butanol-=3l &e + '. /e fierbe pe baia de apă timp de 4+ de minute & dopul se va imobiliza în prealabil ', după care se răceşte cu apă. /e citeşte din nou e"tincţia ca mai sus &e '. . 3alcul. F p >

4+D ⋅ ( e.

−

.+++

e+ )

⋅   =

+,·& e 7e+  ' gGl

Bnde: 4+D coeficient stabilit din dreapta de etalonare cu proantocianidină.

)eterminarea alcaloizilor. Ieactivi •

=4/0 diluat

•

3loroform

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)od de lucru /e iau 5 ml de e"tract &suc', se adaugă 5 ml acid sulfuric diluat şi se titrează cu iod, +, n până la o coloraţie albastră persistentă & indicator: amidon'. /e ştie că  ml iod +, n corespunde la +,++DD+1 g vitamina 3. entru evidenţierea rezultatelor e"perimentale e"perimentale , acestea vor fi prezentate sub formă tabelară.

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Fabelul . rezentarea rezultatelor e"perimentale. e"perimentale.

Tipul eIperimentului

  >Itract Conc alcoolică %8(

)eterminarea indicelui de perman#anat depotasiu

E 8, 8,

E4 ,8 ,5

8,

,1

>Itract Conc alcoolică -8(

>Itract >Itract Conc alcoolică Conc alcoolică 8( 8( Eolumul de permanganat de potasiu folosit la titrare &ml' E E4 E E4 E E4 8,4 ,1 8, ,1 D, ,8 8,6 ,8 8,4 ,1 D, ,8 8,4

,1

8,4

,1

D,

  !uc

,D

E 1,4 1,6

E4 6,5 6,5

1,4

6,5

3antitatea de tanin corespunzătoare volumuli de X)n0  folosit la titrare & g ' +,54 +,5 +,18 +,5

+,5

)eterminarea taninurilor

e+

e

e+

condensate

+,+4*

 +,+D4

+,+*

Ealoarea e"tincţiei e"tincţiei citite la 55+ nm e e+ e e+ +,+6*

+,55

+,4+D

alcaloizilor )eterminarea

+,

+,

acidităţii totale

+,*

)eterminarea

,4

e

+,+4 +,4+4 +,+D +,6* Ealoarea indicelui F  & gGl gGl ' ,DD+ ,45D 3antittea de alcaloizi alcaloizi &g ' +, +,

Eolumul de Ha0= folosiţi la titrare &ml ' , ,D

e+

e

+,+45

+,+5 +,D64 +,6 5

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%8( )eterminarea acidităţii totale )eterminarea vitaminei C

+,+48 +,6 +,++41

-8( 8( 8( $ciditate totală & e"primată în grame acid malic ' &g Gml ' +,+4D* +,+668 +,+6 Eolumul de O în XO folosiţi la titrare titrare &ml ' +,6 +,6 +,6 3onţinutul 3onţinutul în vitamina vitamina 3 &g ' +,++41

+,++41

+,++41

+,+14 +,4 +,++81

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Concluzii

•

3reşterea concentraţiei alcoolice a e"tractului influenţează în mod favorabil

e"tracţia substanţelor polifenolice polifenolice & taninuri şi taninuri condensate '. •

3oncentraţia alcoolică nu are influenţă asupra cantităţii de alcaloizi e"trase,

deoarece aceştia sunt insolubili în alcool & solubili în cloroform, =H0 6 '. •

0 dată cu creşterea concentraţiei alcoolice a e"tractului creşte şi aciditatea

acestuia & concentraţia concentraţia alcoolică creşte în mod direct proporţio proporţional nal cu aciditatea '.

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Knfluenţa concentraţiei eItractului9 a concentraţiei alcoolice a acestuia &i a cantităţii de vitamina C adău#ată asupra acidităţii sucului de mere. /copul acestui studiu este de a observa influenţa concentraţiei e"tractului de  păducel, a concentraţiei alcoolice a acestuia precum şi a cantităţii de vitamina 3 adăugată asupra acidităţii sucului de mere. entru atingerea acestui scop, s-a folosit un program factorial 6 6, care constă în elaborarea modelelor matematice şi în calculul de optimizare. entru acest studiu de design, s-a recurs la mai multe e"perimente în care s-au e"aminat efectele a trei variabile: "  7 concentraţia e"tractului, " 4  7 concentraţia alcoolică a e"tractului

 7 cantitate de vitamina 3 adăugată în suc.

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Tabelul 1. "arametrii studiaţi &i valorile funcţiei de răspuns. 3on 3oncent centrraţia aţia e"t e"tract ractul uluui "

3on 3oncen centraţi raţiaa alco alcooolică ică "4 - & 1+ '

- &5'

+ & 8+ ' M

3an 3antitat itatea ea de vitam tamina ina 3 "6 - & +,+++5 ' + & +,+++ ' M & +,++5 ' - & +,+++5 ' + & +,+++ ' M & +,++5 ' - & +,+++5 '

$ci $cidit ditatea atea _ +,+665 +,+6D +,+61 +,+655 +,+685 +,+6DD +,+1*

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

/e calculează coeficienţii pentru efecte simple: 48

∑ 7 ⋅  y a  > ∑ 7 

9 =. 48

.9 

9 =.

9 

 > - +,+++51

4 .9 

48

∑ 7 ⋅  y a  > ∑ 7 4 9 

4

9 =. 48

4 4 9 

9 =.

9 

 > +,++68

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

/e calculează coeficieţii pentru termeni cvadratici: 48

∑

4

4

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

este 6, cu relaţia:

3alculăm pătratul erorii medii, ştiind că numărul de măsurători, n,

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3oeficienţii a 4 şi a6 sunt pozitivi, rezultă că ambele variabile " 4 şi "6 au o acţiune individuală individuală favorabilă, efectul favorabil al lui " 4 fiind mai puternic decât efectul favorabil a lui a6.

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+,+151 "4 M +,++4 "  > +,++68 +,+++4 "6 M +,++468 > +

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$stfel vom avea trei suprafeţe de răspuns caracterizate de următoarele modele matematice:

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