Storage Tank PressControl Rev1.xls

June 14, 2018 | Author: sachinumarye | Category: Valve, Pressure, Gases, Vacuum, Liquids
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Description

Pressure Control for Liquid Storage Tanks Scheme Selection Logic Diagram (See referenced standard arrangements for piping and instrument details.)

Start

Identify Storage Tank and Contents

Is Presence of O2 in Tank Hazardous?

Yes

Is Tank Design Pressure 16 in. WC?

Is Abatement Device Required?

N2 Pad Tank; Dual N2 Supply and LP Alarm Required

Yes

Yes

No

No

Use Pressure-only Vent to Atm. (see Std Arrgt A)

No

Use Back-pressure Regulator or Control Valve (see Std Arrgt B)

Not generally acceptable without extensively engineered solution.

Does O2 or H2O Affect Product Quality? (Note 1)

Yes

Is Abatement Device Required?

N2 Pad Tank; Single N2 Supply and LP Alarm Required

No

Is Material an Alkaline-Initiator or Is It H2OReactive?

No

Use Conservation Vent (see Std Arrgt C)

Yes

Is Device Hazardous w/O2 (i.e., Flare or Incinerator)?

Yes

Is System Vented thru a Vacuum Pump?

No

Use Back-pressure Regulator or Control Valve (see Std Arrgt D)

Yes

Yes

Yes

No

No Is Pressure Sufficient to Use a Control Valve?

Install O2 Analyzer in Header to Device

Is Abatement Device Required?

No

Yes

Is Device Hazardous w/O2 (i.e., Flare or Incinerator)?

Yes

N2 Pad Tank; Single N2 Supply Required (Note 2)

No

Is System Vented thru a Vacuum Pump?

Use Gooseneck or Conservation Vent to Atm. (see Std Arrgt H)

Use Pipe-away Vent Valve (see Std Arrgt E)

No

Is System Vented thru a Vacuum Pump?

No

Use Conservation Vent and Pipe-away Vent Valve (see Std Arrgt J)

Use Back-pressure Regulator or Control Valve (see Std Arrgt F)

Yes

Yes

Yes No

Use Back-pressure Regulator or Control Valve (see Std Arrgt K)

Is Pressure Sufficient to Use a Control Valve?

No

Use Pipe-away Vent Valve (see Std Arrgt G)

Notes: 1. O2 sensitivity is indicated if shipping containers must be purged. 2. O2 analyzer must be installed in header to abatement device.

Pressure Control Schematic for Liquid Storage Tanks Standard Arrangement A (see Scheme Selection Logic Diagram)

PI

set @ "A"

PAL

Pressure Relief set @ "C"

PT Radar Level Gauge

½" 316SS tubing (typ.) from N2 Supply Header

Primary Pressure Supply set @ "B"

LO LO

PI

Pressure Control/Relief Sequence

LO

LO

LO

PI

PI

Backup Pressure Supply set @ "A"

A B C

2 in. WC 6 in. WC Dead Band Greater of 0.5 x Tank's MAWP or 8 in. WC 12 psig

Primary N2 Pressure Supply

closes opens

"B"

Backup N2 Pressure Supply

closes opens

"A"

"C"

Pressure Vacuum

Typical Values Atmospheric Tank

opens closes

LO

Bleed

Setting

Pressure Relief

Dead Band

Stepdown Regulators set at "D"

LO

PI

Pressure Vessel Case-specific* Min. = A + 4 in. WC

Max. = Vessel's MAWP

Case-specific** D * Based on vapor pressure and/or properties of stored material. ** Based on "B"; stepdown regulator may not be required.

Notes:

1. Replaced Ball Float-and-wire level indicator with Radar Level Gauge.

Pressure Control Schematic for Liquid Storage Tanks Standard Arrangement B (see Scheme Selection Logic Diagram)

PI Primary Pressure Bleed set @ "C"

set @ "A"

PT

Backup (Emergency) Pressure Relief set @ "D"

Radar Level Gauge

½" 316SS tubing (typ.)

Primary Pressure Supply set @ "B" (See Note 1)

from N2 Supply Header

PAL

to Abatement Device (with or without Vacuum System)

LO LO PI

PI

LO

LO

Primary Pressure Bleed

PI

PI

Backup Pressure Supply set @ "A" (See Note 1)

Bleed

A B C D E

opens closes

Typical Values Atmospheric Tank

2 in. WC 6 in. WC Dead Band D - 4 in. WC Greater of 0.5 x Tank's MAWP or 12 in. WC 12 psig

Pressure Vessel Case-specific* Min. = A + 4 in. WC

"D"

opens closes

LO

LO

Setting

Backup Pressure Relief

LO

"C" Dead Band

Stepdown Regulators set at "E" (See Note 1)

Pressure Control/Relief Sequence

Primary N2 Pressure Supply

closes opens

"B"

Backup N2 Pressure Supply

closes opens

"A"

Pressure Vacuum

Max. = Lesser of 0.9 x D or Vessel's MAWP - 4 in. WC Max. = Vessel's MAWP

Case-specific** * Based on vapor pressure and/or properties of stored material. ** Based on "B"; stepdown regulator may not be required.

Notes: 1. Capacities of Primary and Backup N2 Regulators must satisfy primary pressure bleed fail open case.

2. Replaced Ball Float-and-wire level indicator with Radar Level Gauge.

Pressure Control Schematic for Liquid Storage Tanks Standard Arrangement C (see Scheme Selection Logic Diagram)

PI

set @ 0 " WC

PAL

Pressure Bleed/Relief set @ "C"

Backup Vacuum Relief set @ "A"

PT Radar Level Gauge

½" 316SS tubing (typ.)

from N2 Supply Header LO

Pressure Control/Relief Sequence Pressure Supply set @ "B" LO

Stepdown Regulator set at "D"

PI

PI

LO

LO

Pressure Bleed/Relief

opens closes

N2 Pressure Supply

closes opens

"C"

Bleed

Dead Band

"B"

Pressure Vacuum

Setting A B C D

Vacuum Relief

Typical Values Atmospheric Tank

Pressure Vessel

½ oz./in.2 Vacuum 2 in. WC Dead Band Greater of 0.5 x Vessel MAWP or 4 in. WC 12 psig

N/A

closes opens

"A"

Notes:

1. Replaced Ball Float-and-wire level indicator with Radar Level Gauge.

Pressure Control Schematic for Liquid Storage Tanks Standard Arrangement D (see Scheme Selection Logic Diagram) Backup Vacuum Relief set @ "A" Primary Pressure Bleed set @ "C"

PI set @ 0 " WC

PAL

to Abatement Device (with or without Vacuum System)

Backup (Emergency) Pressure Relief set @ "D"

Radar Level Gauge

PT

½" 316SS tubing (typ.)

from N2 Supply Header LO

Pressure Control/Relief Sequence Pressure Supply set @ "B" (See Note 1) LO

Stepdown Regulator set at "E" (See Note 1)

PI

PI

Backup Pressure Relief

opens closes

"D"

Primary Pressure Bleed

opens closes

"C"

N2 Pressure Supply

closes opens

LO

LO

Bleed Dead Band

Setting A B C D E

"B"

Pressure Vacuum

Typical Values Atmospheric Tank

Pressure Vessel

½ oz./in.2 Vacuum 2 in. WC Dead Band D - 4 in. WC Greater of 0.5 x Tank's MAWP or 8 in. WC 12 psig

N/A

Backup Vacuum Relief

closes opens

Notes: 1. If abatement device is O2-sensitive, capacities of N2 Regulator and Pressure Supply Valve must satisfy Primary Pressure Bleed fail open case. 2. Replaced Ball Float-and-wire level indicator with Radar Level Gauge.

"A"

Pressure Control Schematic for Liquid Storage Tanks Standard Arrangement E (see Scheme Selection Logic Diagram) Backup Vacuum Relief set @ "A" Primary Pressure Relief set @ "C"

PI set @ 0 " WC

PAL

Backup (Emergency) Pressure Relief set @ "D"

to Abatement Device (without Vacuum System) Radar Level Gauge

PT

½" 316SS tubing (typ.) from N2 Supply Header LO

Pressure Control/Relief Sequence Pressure Supply set @ "B" (See Note 1) LO Stepdown Regulator set at "E" (See Note 1)

PI

PI

Backup Pressure Relief

opens closes

"D"

Primary Pressure Bleed

opens closes

"C"

N2 Pressure Supply

closes opens

LO

LO Bleed

Dead Band

Setting A B C* D E

Typical Values Atmospheric Tank

½ oz./in.2 Vacuum 2 in. WC Dead Band D - 4 in. WC Greater of 0.5 x Tank's MAWP or 8 in. WC 12 psig

Pressure Vacuum

Pressure Vessel

Backup Vacuum Relief

closes opens

N/A

* Setting is dependent upon pressure required to flow through abatement device.

"B"

Notes: 1. If abatement device is O2-sensitive, capacities of N2 Regulator and Pressure Supply Valve must satisfy Primary Pressure Relief fail open case. 2. Replaced Ball Float-and-wire level indicator with Radar Level Gauge.

"A"

Pressure Control Schematic for Liquid Storage Tanks Standard Arrangement F (see Scheme Selection Logic Diagram) Backup Vacuum Relief set @ "A"

Primary Pressure Bleed set @ "C"

to Abatement Device (with or without Vacuum System)

Backup (Emergency) Pressure Relief set @ "D"

Radar Level Gauge

½" 316SS tubing (typ.)

from N2 Supply Header LO

Pressure Control/Relief Sequence Pressure Supply set @ "B" (See Note 1)

LO Stepdown Regulator set at "E" (See Note 1)

PI

PI

Backup Pressure Relief

opens closes

"D"

Primary Pressure Bleed

opens closes

"C"

LO

LO Bleed

Dead Band N2 Pressure Supply

closes opens

"B"

Pressure Vacuum

Setting A B C D E

Typical Values Atmospheric Tank

Backup Vacuum Relief

Pressure Vessel

closes opens

2

½ oz./in. Vacuum 2 in. WC Dead Band D - 4 in. WC Greater of 0.5 x Tank's MAWP or 8 in. WC 12 psig

N/A Notes: 1. If abatement device is O2-sensitive, capacities of N2 Regulator and Pressure Supply Valve must satisfy Primary Pressure Bleed fail open case. 2. Replaced Ball Float-and-wire level indicator with Radar Level Gauge.

"A"

Pressure Control Schematic for Liquid Storage Tanks Standard Arrangement G (see Scheme Selection Logic Diagram) Backup Vacuum Relief set @ "A" Primary Pressure Relief set @ "C"

Backup (Emergency) Pressure Relief set @ "D"

to Abatement Device (without Vacuum System) Radar Level Gauge

½" 316SS tubing (typ.)

from N2 Supply Header LO

Pressure Control/Relief Sequence Pressure Supply set @ "B" (See Note 1) LO Stepdown Regulator set at "E" (See Note 1)

PI

PI

Backup Pressure Relief

opens closes

"D"

Primary Pressure Bleed

opens closes

"C"

N2 Pressure Supply

closes opens

LO

LO Bleed

Dead Band

Setting A B C* D E

Typical Values Atmospheric Tank

½ oz./in.2 Vacuum 2 in. WC Dead Band D - 4 in. WC Greater of 0.5 x Tank's MAWP or 8 in. WC 12 psig

Pressure Vacuum

Pressure Vessel

Backup Vacuum Relief

closes opens

N/A

* Setting is dependent upon pressure required to flow through abatement device.

"B"

Notes: 1. If abatement device is O2-sensitive, capacities of N2 Regulator and Pressure Supply Valve must satisfy Primary Pressure Relief fail open case. 2. Replaced Ball Float-and-wire level indicator with Radar Level Gauge.

"A"

Pressure Control Schematic for Liquid Storage Tanks Standard Arrangement H (see Scheme Selection Logic Diagram)

Gooseneck Atmospheric Vent Radar Level Gauge

Notes:

1. Replaced Ball Float-and-wire level indicator with Radar Level Gauge.

Pressure Control Schematic for Liquid Storage Tanks Standard Arrangement J (see Scheme Selection Logic Diagram) Vacuum Relief set @ "A" Primary Pressure Relief set @ "B"

to Abatement Device (without Vacuum System)

Radar Level Gauge

Backup (Emergency) Pressure Relief set @ "C"

LO LO

Pressure Control/Relief Sequence

opens closes

"C"

Primary Pressure Bleed

opens closes

"B" Dead Band

Backup Pressure Relief

Pressure Vacuum

Setting A B* C

Typical Values

Backup Vacuum Relief

Atmospheric Tank

Pressure Vessel

½ oz./in.2 Vacuum Dead Band C - 4 in. WC Greater of 0.5 x Tank's MAWP or 2 in. WC

N/A

* Setting is dependent upon pressure required to flow through abatement device.

closes opens

"A"

Notes:

1. Replaced Ball Float-and-wire level indicator with Radar Level Gauge.

Pressure Control Schematic for Liquid Storage Tanks Standard Arrangement K (see Scheme Selection Logic Diagram) Primary Pressure Bleed set @ "B"

Backup Vacuum Relief set @ "A"

to Abatement Device (with or without Vacuum System)

Radar Level Gauge

LO

Backup (Emergency) Pressure Relief set @ "C"

LO

LO

Pressure Control/Relief Sequence

opens closes

"C"

Primary Pressure Bleed

opens closes

"B" Dead Band

Backup Pressure Relief

Pressure Vacuum

Setting A B* C

Typical Values Atmospheric Tank

Pressure Vessel

½ oz./in.2 Vacuum Dead Band C - 4 in. WC Greater of 0.5 x Tank's MAWP or 8 in. WC

N/A

* Setting is dependent upon pressure required to flow through abatement device.

Backup Vacuum Relief

closes opens

"A"

Notes:

1. Replaced Ball Float-and-wire level indicator with Radar Level Gauge.

Art Montemayor

Storage Tank Venting Operations

UNDERSTANDING TANK SAFETY

March 11, 2004 Rev: 1(03-23-04)

This section is devoted to assist those who are designing tanks or tank installations for the storage of flammable or volatile liquids, and to aid in the specification and use of tank fittings and related equipment designed to provide optimum efficiency and maximum protection for the tank and its contents. The topics covered include: 1. The need for providing pressure and vacuum relief for storage tanks. 2. Methods of protecting flammable vapors in the tank, and in connecting piping, against a source of ignition. 3. The role that blanketing of the tank's vapor space with an inert gas plays in safe and efficient tank operations.

STORAGE TANK VENTING FOR CONSERVATION, SAFETY & ENVIRONMENTAL PROTECTION Tank conservation vents are intended for use on flammable liquid storage tanks that operate at pressures of 15 PSIG or less. This worksheet explains why tank venting equipment is needed and how it may be properly specified. The hazards associated with pressure and vacuum accumulation in a tank storing flammable and combustible liquids are studied. The operation of vents, their role in safe plant operations, the method of sizing and specifying vents and their importance in minimizing evaporation losses and fugitive emissions are discussed. Definitions of terms commonly encountered in the tank venting industry are provided. DEFINITIONS Atmospheric Tank Combustible Liquid Diaphragm Design Pressure Flammable Liquid Flashpoint Leak Rate Low Pressure Tank Pallet Assembly

Pressure Vessel Set Point Seat Tank Vent

Tank MAWP

Tank MAWV

A storage tank that has been designed to operate at pressures from atmospheric through 0.5 PSIG. A liquid having a flashpoint at or above 100 oF. The sealing (gasket) material that is part of the pallet assembly and which seals against the seat surface when the vent is closed. The design pressure or vacuum that a storage tank can withstand without damage to its structure. This does not apply to attached or connected equipment in the system. A liquid having a flashpoint below 100 oF. The minimum temperature at which a liquid gives off vapor in sufficient concentration to form an ignitable mixture with air near the surface of the liquid. The leakage of vapor from the vent prior to reaching the set point. A storage tank which has been designed to operate at pressures above 0.5 PSIG but not more than 15 PSIG. This usually is according to API 650 and/or API 620. The weight or spring loaded disc housed within the vent that moves in response to the tank pressure, allowing flow into or out of the tank. The pallet assembly covers the vent seat when in the closed position. A storage tank or vessel which has been designed to operate at pressures above 15 PSIG. The tank pressure and/or vacuum at which the vent begins to open. The machined orifice within the vent housing on which the pallet assemblies seat (by gravity or spring force) when the vent valve is in the closed position. A device intended to provide pressure and/or vacuum relief for atmospheric or low pressure storage tanks. The set points of the vents may be provided by weight loading, spring loading, or buckling pin. The tank's Maximum, safe, Allowable Working Pressure as determined by the existing mechanical design of its components and its configuration. This is a calculated value obtained by using the actual, empirically obtained design data. A tank cannot be allowed to exceed this value. The tank's Maximum, safe, Allowable Working Vacuum. A counterpart to its MAWP.

Page 12 of 46

FileName: 161250009.xls.ms_office WorkPage: Venting Operations

Art Montemayor

Storage Tank Venting Operations

March 11, 2004 Rev: 1(03-23-04)

PRESSURE/VACUUM ACCUMULATION The use of large capacity tanks and vessels for the temporary storage of flammable or combustible liquids is a common practice in a wide range of commercial and industrial enterprises. These tanks provide fixed volume containers to hold liquids transferred (filling and emptying) through connected piping systems. In any such fixed roof tank, the volume above the liquid level is known as the vapor space. Assume that a tank is completely vapor tight and that liquid is being pumped into and out of the tank. Filling the tank raises the liquid level and causes the vapor space to decrease (vapors are compressed), with a resulting increase in the pressure in the vapor space. Alternatively, if liquid is withdrawn from the tank, the vapor space increases (vapors are allowed to expand) and the pressure in the vapor space decreases.

Now, assume that the tank is again completely vapor tight, no liquid is being transferred (the liquid level does not change), but the liquid in the tank is being heated or cooled. The addition of heat causes the liquid's vapor pressure to increase, with a subsequent increase in vapor evolved into the closed vapor space. The result is an increase in pressure in the vapor space. Cooling of the liquid leads to a decrease in vapor pressure in the vapor space. The scenarios outlined above reflect common hazards associated with the storage of flammable liquids in fixed roof tanks. Unless the tanks are equipped with properly designed and specified venting devices, excessive pressure and/or vacuum accumulations in the vapor space can result in severe tank damage. Conservation vents for pressure and vacuum relief are specifically designed to address and eliminate this potentially hazardous situation. Normal Venting -

In day-to-day tank operations, changes in the liquid level are caused by routine filling and emptying of the tank. Changes in the temperature of the vapors and liquids in the tank are the result of variations in the ambient atmospheric temperatures (e.g. higher temperatures during the day; cooler temperatures at night). Discharging the volume of vapors generated (pressure relief), or inbreathing the volume of make-up air required (vacuum relief), during such activities is defined as normal venting (Vents That Provide Normal Pressure/Vacuum Relief).

Emergency Venting -

The temperature of the stored liquid and vapors may also increase as a result of the tank being exposed to an external fire. A significant amount of heat may be transferred through the tank shell into the stored liquid and the volume of vapors generated as a result of this heat input can be substantial. Providing a means of discharging this large volume of vapors and arresting an increase of pressure within the tank is defined as emergency venting (Vents That Provide Emergency Pressure Relief).

EVAPORATION LOSSES In addition to protecting a tank from excessive pressure and vacuum, conservation vents also play a key role in the reduction of product evaporation losses and fugitive emissions. The vents are designed to remain closed until they must open to protect the tanks. Vapors are contained within and are not released into the atmosphere. The reduction in product loss as compared to an open atmospheric vent is significant. The emission of vapors into the atmosphere is minimized. Tank vents are an important tool in any company's attempts to comply with the Clean Air Act mandates concerning air pollution. VENT OPERATION The method of operation of conservation pressure/vacuum vents is straightforward. The vents are mounted on a nozzle connection that leads to the tank's vapor space. Each vent includes a machined seat that is closed by a moveable sealing disk (pallet assembly). The pallet assembly is held in its closed position by weights, springs or buckling pin (depending on the vent style). The amount of closing force applied determines the set point of the vent. The pressure in the tank's vapor space pushes against the pallet assembly, in opposition to the closing force. When the tank pressure reaches the vent set point, the pallet assembly lifts and vapors are allowed to escape from the tank through the vent. The pressure and/or vacuum in the tank's vapor space is maintained within a safe range.

Page 13 of 46

FileName: 161250009.xls.ms_office WorkPage: Venting Operations

Art Montemayor

Storage Tank Venting Operations

March 11, 2004 Rev: 1(03-23-04)

SIZING AND SPECIFICATION Pressure/Vacuum relief vents are available in a range of sizes. Larger size vents provide greater flow capability than smaller size vents. When choosing a proper size venting device the following information is significant: 1. THE AMOUNT OF VAPOR/AIR THAT MUST PASS THROUGH THE VENT. The amount of vapors that must be relieved is usually stated in Standard Cubic Feet of Air per hour (SCFH). Methods of calculating these volumes for specific normal venting and emergency venting situations can be found in 29CFR - OSHA 1910.106. 2. THE DESIGN PRESSURE/VACUUM OF THE STORAGE TANK. Storage tanks are mechanical structures. There are limits as to how much pressure and vacuum they can withstand before they are damaged. These limits are known as the tank's MAWP and MAWV. 3. ANY OPERATING CHARACTERISTICS OF THE TANK SYSTEM THAT REQUIRE A SPECIFIED PRESSURE OR VACUUM TO BE MAINTAINED IN THE TANK (MINIMUM VENT SET POINT). The relief vent will remain closed until its set pressure is reached. If there is a need to maintain some pressure in the tank during normal operations, the vent should be set so that it will not open and begin relieving below that pressure. 4. THE FLOW CAPABILITY OF THE VENT BEING CONSIDERED FOR USE. Each size and style of vent will flow specific volumes of vapors at a given tank pressure. These vent flow capabilities are available from the manufacturer.

Page 14 of 46

FileName: 161250009.xls.ms_office WorkPage: Venting Operations

March 11, 2004 Art Montemayor Storage Tank Venting Operations The key to sizing a vent for pressure or vacuum relief is to make sure that the vent (with set point) chosen will Rev: 1(03-23-04) flow the required amount of vapors at a tank pressure less than the MAWP of the tank. This insures that the tank's MAWP or MAWV are never exceeded. The tank's design pressure is inherently equal to or less than the MAWP. In the same logical sense, the tank's design vacuum rating is equal to or greater than the MAWV. The process or project engineer should pay heed to the difference between the Design Pressure/Vacuum and the MAWP/MAWV ratings. The differences can sometimes be sufficient to cause a mis-application and lead a severe storage tank failure. It is always conservative and, far more, safety-wise to employ the MAWP/MAWV values as the maximum criteria for setting the limits on storage tank operations. By doing so, the owner is forced to monitor the actual, physical conditions of his storage tanks and take all wear, changes and modifications into consideration when attaching a maximum pressure and vacuum to a storage tank. This is in keeping with the spirit and intent of OSHA 1910 and all other safety regulations or guidelines. A storage tank's Design Pressure is simply the quasi-theoretical value calculated by the owner's process engineer or the fabricator's design engineer. This value serves as the target, or benchmark, by which the fabricator will proceed to actually fabricate the ultimate, final tank. Note that the Design Pressure is the target that the fabricator uses to ensure that his product will meet (& probably exceed) the specified pressure and vacuum conditions set forth by the purchaser/owner. In the real, practical fabrication of the storage tank the fabricator will employ those materials and components that - more often than not - exceed the specifications because certain components (such as the steel plates) are only available in standard thicknesses and grades. Another variable is the fabricator's incentive to employ his stored inventory of components and steel plate. In doing so, the fabricator again is often guided by his desire to employ his inventory rather than purchase additional materials. His incentive to rotate his inventory forces him to select applicable steel plate material that often surpasses the specifications - because of its existence and also because of standard sizing. As a net result, the newly-built storage tank's MAWP and MAWV are often in excess of the values specified for fabrication. These values may or may not be revealed to the Owner, depending on whether their calculations are specified as part of the agreed fabrication contract. The Design Pressure is usually the value stamped on the Tank's fabrication name plate - unless otherwise dictated by the Owner, since the MAWP/MAWV calculations may not be included in the fabrication price. Once the new tank is installed and operating, it is the Owner's responsibility to make sure that the tank is properly and safely protected from pressure or vacuum hazards. Initially, at the onset, the use of the Design Pressure as the guideline in setting instrument setpoint is a conservative one since the MAWP and MAWV exceed their Design counterparts. However, as the tank normally undergoes wear, corrosion, changes, modifications, and repairs during its normal operating life the safety values undergo a reversal of conservative design. Corrosion and wear alone will lower the value of the MAWP and increase the value of the MAWV - and if allowed to continue, the Design Pressure and Design Vacuum values will be exceeded and a radically different safety situation will exist. That is why OSHA strongly advises all storage tank owners to implement on-going mechanical inspection programs on all storage tanks. And these inspection programs should dove-tail with up-dated MAWP and MAWV calculations for the subject tank that reflect the actual, real condition of the tank. Therefore, it can be seen that the Design Pressure and Design Vacuum values are of importance to any tank only at the initial use of these vessels. Afterwards, it is the MAWP and MAWV values that should be identified and allowed to control a tank safety situation. For the above practical reasons, then, it is recommended that an Owner employ only the MAWP and MAWV actual values in applying safety pressure and vacuum relief devices to his/her storage tanks. MATERIALS OF CONSTRUCTION Conservation vent devices are available in a wide range of materials (aluminum, stainless steel, ductile iron, Hastelloy, PVC, FRP, etc.). The material must be compatible with the service conditions. Improper material choice can lead to contamination of the product being stored or reduction in the vent's ability to operate safely. Information on the corrosion resistance of materials under various service conditions is available in corrosion handbooks and chemical dictionaries.

Page 15 of 46

FileName: 161250009.xls.ms_office WorkPage: Venting Operations

Art Montemayor

Storage Tank Blanketing

TANK BLANKETING - A Versatile Tool against Fire & Explosions

March 12, 2004 Rev: 0

Tank blanketing valves are commonly used in tank storage systems where it is desirable to reduce the hazards associated with flammable liquids or to minimize contamination or product degradation that may result from drawing air into the tank's vapor space. In this WorkSheet, some basic information on blanketing valves will be provided. It is suggested that you contact a recognized supplier (such as ProtectoSeal Co.) when reviewing a specific tank blanketing application. This WorkSheet also explains the function of blanketing valves, describes their method of operation and provides guidelines for sizing and specification of the valves. Definitions of terms commonly associated with tank blanketing valves are listed below. DEFINITIONS A device that senses the pressure in the vapor space of a storage tank and controls the flow of an inert gas (usually Nitrogen) into the vapor space so that the tank pressure can be maintained within an acceptable range. The total pressure difference between the blanketing valve opening pressure Deadband (or set point) and resealing pressure. This applies to the main valve. Some minor leakage through the pilot will occur above the main valve resealing pressure. In a pilot operated blanketing valve, the pressure in the dome volume. Dome Pressure In a pilot operated blanketing valve, the chamber between the poppet in the Dome Volume pilot valve and the piston in the main valve. A small cylinder which may installed in the valve to partially block the flow of Flow Plug inert gas through the valve. The portion of the valve through which supply gas flows into the storage tank. Main Valve In a pilot operated valve, the portion of the valve that senses tank pressure Pilot Valve and controls the opening and closing of the main valve. The component in the valve which moves in response to changes in pressure Poppet in the sensing diaphragm chamber and which, when unseated, allows flow through the device. Pressure Balanced Poppet - A poppet designed so that the supply pressure will not have an effect on its opening or closing characteristics. Most blanketing valves have pressure balanced poppets. The space below the diaphragm chamber to which the sense line pressure, Sense Chamber from the tank, is directed. The pressure in the sense chamber controls the opening and closing of the poppet. A thin, non-metallic disc in the diaphragm chamber which flexes in response Sense Diaphragm to changes in the sense line pressure. A tube running from the tank's vapor space to the sense port of the blanketing Sense Line valve. This tube transmits tank pressure to the sense chamber. The pressure at which the main valve opens and flows. Set Point MAWP The tank's Maximum Allowable Working Pressure. Blanketing Valve -

HARDWARE EXAMPLES Products of the ProtectoSeal Company are used in this Workbook as examples of the applied hardware. Other manufacturers also produce similar or competitive devices. ProtectoSeal in one of the original and recognized world-wide suppliers of storage tank relief and blanketing equipment.

Page 16 of 46

FileName: 161250009.xls.ms_office WorkSheet: Blanketing Concept

March 12, 2004 Art Montemayor Storage Tank Blanketing FUNCTION OF A BLANKETING VALVE Rev: 0 A blanketing valve uses a supply of high pressure gas to maintain a blanket of low pressure gas above the stored material in a storage tank. The gas is usually non-flammable and chemically non-reactive when mixed with the vapors of the stored product. The gas, usually inert Nitrogen, is injected as necessary in order to maintain a non-flammable atmosphere in the vapor space. The blanketing pressure is usually very low, less than 1 pound per square inch gage (psig). It is set at a value that ensures that any leakage will be outward. Blanketing valves serve several purposes: 1. Maintain the vapor space of the storage tank within an acceptable, safe pressure range; 2. Keep the vapors non-flammable by eliminating oxygen-rich air; 3. Minimize or eliminate evaporation losses (and product losses); and, 4. Reduce product degradation and tank corrosion by keeping contaminants, air, and moisture from entering the tank vapor space. BLANKETING VALVE OPERATION A blanketing valve is typically mounted on top of a storage tank along with a pressure/vacuum conservation vent and an emergency pressure relief vent. The blanketing gas supply pipe is connected to the valve inlet, and the valve outlet is piped to the tank roof. A "sense" line from a high point on the tank roof is connected to the valve's sense port, thus supplying the control pressure for the valve.

The blanketing valve provides primary vacuum relief for the tank. It opens and supplies gas to the vapor space when tank vapor space pressure decreases to the valve's set point. When vapor space pressure increases, the valve reseals. A conservation vent (for example, Series No. 8540H) is installed on the tank roof to take care of overpressure and vacuum conditions brought about by unforeseen conditions or equipment failures. The pressure setting of the conservation vent is set at a slightly higher setting than the blanketing set pressure in the tank - but below the tank's MAWP. Similarly, the vacuum pallet is set at a higher vacuum setting than normal operating conditions bring about and below the maximum vacuum pressure the tank can withstand. A flame arrester (Series No. 4950) is placed below the conservation vent to provide additional protection in the event of inert gas failure. An emergency relief vent (Series No. 7800) is also placed on the tank to account for an emergency - such as the Fire Case. The set pressure of the emergency vent is slightly above the conservation vent pressure setting.

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FileName: 161250009.xls.ms_office WorkSheet: Blanketing Concept

March 12, 2004 Art Montemayor Storage Tank Blanketing Pilot Operated Blanketing Valve Rev: 0 A pilot operated blanketing valve (Series No. 20 - Pilot Operated Blanketing Valve) consists of two separate valves, working in tandem (the main valve and the pilot valve). The main valve inlet connects to the high pressure gas supply source. The valve outlet is piped to the tank vapor space. The piston in the main valve is held in its closed position by supply line pressure accumulated in the dome volume (the space between the poppet in the pilot valve and the piston in the main valve). This accumulated pressure is called the dome pressure.

Opening and closing of the main valve is controlled by the pilot valve. The tank's vapor space pressure is transmitted, via the sense line, to the diaphragm sense chamber. Decreases in the sensed pressure result in movement of the pressure balanced poppet in the pilot valve. The poppet unseats and allows gas to flow out of the dome volume. This results in a reduced pressure in the dome volume and opening of the main valve piston to allow gas to flow into the tank. Increases in tank pressure cause the poppet to reseal, the dome pressure to increase and the main valve piston to reseal. Pilot operated blanketing valves provide very accurate sensing of the tank pressure and also provide full open flow through the main valve at a pressure very near to the blanketing valve set point. Spring-Operated Blanketing Valve A spring-operated blanketing valve (Series No. 30, Spring-Operated Blanketing Valve) functions in a manner similar to a spring loaded valve. The valve's inlet is connected to the supply gas and the outlet is connected to the tank. The pressure balanced poppet provides the primary seal. The tank's vapor space pressure is transmitted, via the sense line, to the diaphragm sense chamber. Decreases in the sensed pressure result in movement of the sealing, pressure balanced poppet. This results in flow through the valve, into the tank. Increases in tank pressure cause the poppet to reseal, stopping flow into the tank.

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FileName: 161250009.xls.ms_office WorkSheet: Blanketing Concept

March 12, 2004 Rev: 0 Spring operated blanketing valves are often used on smaller tanks and vessels and in situations where the very small dead band provided by a pilot operated device is not considered necessary.

Art Montemayor

Storage Tank Blanketing

SIZING AND SPECIFICATION OF BLANKETING VALVES Data concerning the flow characteristics of blanketing valves is available from Protectoseal. This information defines the maximum flow of gas through the device for a specific supply gas pressure and a specific set point. This full flow rating through the valve can be reduced by the use of specially designed flow plugs. The proper blanketing valve to meet the flow requirements of the tank system can be determined.

Once the basic valve has been chosen, options that may enhance or simplify system operations should be reviewed. Among the most common options are: 1. Optional connections for piping to supply and tank. 2. Material choice for soft goods (gaskets, o-rings, etc.). 3. Pressure gauges to accurately record supply and/or sense line pressures 4. Integral purge system to constantly direct a small volume of supply gas through the outlet and sense line. This prevents tank vapors from entering the valve's pressure sensing chamber. 5. Field test option to allow for checking and changing of set point in the field. It is recommended that you contact a supplier (such as ProtectoSeal) for full information on the sizing, specification and use of tank blanketing valves. For example, fully documented User's Guides and Installation & Maintenance Instructions are available, upon request, for the Series No. 20, Pilot-Operated Blanketing Valve and the Series No. 30, Spring-Operated Blanketing Valve.

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March 12, 2004 Art Montemayor Typical Blanketing Valves Tank Blanketing Valves provide an effective means of preventing and controlling fires in storage tanks containing Rev: 1(02/10/07 flammable liquids. Vapors cannot be ignited in the absence of an adequate supply of oxygen and in most instances, this oxygen is provided by air drawn into the tank from the atmosphere during tank emptying or fluid transfer operations. Tank Blanketing Valves are installed with their inlet connected to a supply of pressurized inert gas (usually Nitrogen), and their outlet piped into the tank's vapor space. When the tank pressure drops below a predetermined level, the blanketing valve opens and allows a flow of inert gas into the vapor space. The blanketing valve reseats when pressure in the tank has returned to an acceptable level. Since the blanketing gas is an inert, no atmospheric air (Oxygen) is allowed to enter the tank. The vapors, therefore, are never allowed to form a flammable mixture which could ignite due to static electricity or other sparking sources. Tank Blanketing Valves help maintain the vapor space in a non-flammable condition, and also provide make-up gas during liquid out-flow to insure that the tank's vapor space is not subjected to a vacuum A direct-operating, simple, and reliable state-of-the-art blanketing valve is produced by the ProtectoSeal company and has given consistent performance. A typical installation looks as follows:

Note that the valve is mounted directly on the tank's roof, within access from a tank platform. This type of installation allows for protection from ground traffic and freedom from unauthorized tampering. More importantly, it greatly reduces the signal errors and timing from the tank's vapor space and eliminates a lot of pressure drop from the valves outlet and into the tank vapor space. The tank vapor space pressure sensing line should always be kept 100% filled with true vapor space pressure. That is why it (and the outlet pipe to the vapor space) are installed on top of the vapor space and always free-draining. Vapor can condense inside these lines as the outside ambient temperature changes during day-to-night time intervals. If these lines are installed below the tank vapor space, condensed liquid can accumulate there and cause a serious, flawed pressure signal to the Tank Blanketing Valve. The valve is 100% Stainless Steel construction, so atmospheric and chemical exposure presents no corrosion hazard. The tank blanketing valve is available in two basic designs: 1. Spring operated, Series No. 30 This design and model is the original concept which was introduced into the industry around 1985, approximately. 2. Pilot operated, Series No. 20 This model is an improvement on the Series 30, direct-acting model. It is quicker and more accurate in response to the measured pressure signal calling for make-up inert gas. This model allows for effective operation within an inherent, narrow dead band.

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FileName: 161250009.xls.ms_office WorkSheet: Blanketing Valves

March 12, 2004 Rev: 1(02/10/07 Protectoseal Series No. 30, Spring Operated Tank Blanketing Valve, is designed to regulate the flow of a blanketing gas (usually Nitrogen) into the vapor space of a flammable liquid storage tank or vessel. The Series No. 30 valve is spring operated. The pressure balanced poppet is held in its closed position by direct spring force. The tank's vapor space pressure is sensed in the diaphragm case and the valve opens to allow a flow of gas into the tank when the pressure drops below its set point. When tank pressure returns to an acceptable level, the flow of gas is stopped.

Art Montemayor

Typical Blanketing Valves

The pressure-balanced valve poppet ensures that a consistent opening set pressure is realized over the range of existing inert gas supply pressures. The Series No. 30 valve is suitable for use on smaller tanks and vessels. Standard 2" NPT inlet and outlet connections are provided. The valve has the following characteristics: 1. Designed specifically for tank blanketing 2. Compact, light weight design 3. 2" NPT inlet and outlet standard 4. Optional flanged or threaded inlet and outlet connections available 5. Accommodates inlet gas pressures from 10 PSIG to 200 PSIG 6. Set points from -0.1 inches water column to 69.2 inches water column 7. Optional flow plugs to meet specific flow requirements 8. Fully field serviceable 9. Pressure balanced poppet provides consistent opening over a full range of inlet gas pressures 10. Optional sense line gauges 11. System purge and field test capability available 12. Factory tested and certified The valve's available Materials of Construction are: VALVE BODY & COMPONENTS FITTINGS & HARDWARE SPRINGS SOFT GOODS

STANDARD: CUSTOM: STANDARD: CUSTOM:

316 Stainless Steel Others 316 Stainless Steel Others 302 Stainless Steel STANDARD: Buna-N CUSTOM: Neoprene, Viton®, EPDM, Chemraz®, Kalrez® & others

DIAPHRAGM FILTER

STANDARD: Aluminum/Zinc/Polypropylene/Buna-N/Acetal CUSTOM: Stainless Steel/Polypropylene/Viton®/Acetal

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FileName: 161250009.xls.ms_office WorkSheet: Blanketing Valves

March 12, 2004 Art Montemayor Typical Blanketing Valves Protectoseal Series No. 20, Pilot Operated Tank Blanketing Valve, is designed to regulate the flow of a Rev: 1(02/10/07 blanketing gas (usually Nitrogen) into the vapor space of a flammable liquids storage tank. The valve senses the pressure in the vapor space and opens to allow a flow of gas into the tank when the pressure drops below its set point. When tank pressure returns to the valve's set point, the flow of gas is stopped. The Series No. 20 valve consists of a main valve (which controls the flow of inert gas into the tank), and the pilot valve (which accurately senses the tank's pressure and controls the opening and closing of the main valve). This tandem valve arrangement provides extremely accurate control of the flow of gas into the tank. The pressure balanced poppet in the pilot ensures that a consistent opening set pressure is realized over the range of available inert gas supply pressures. The Series No. 20, Pilot Operated Tank Blanketing Valve, requires a very narrow band of pressure to effectively cycle from closed, to open and fully flowing, and to resealed. The valve has the following characteristics: 1. Designed specifically for tank blanketing 2. Pilot operated design provides very tight operating band 3. Compact, light weight design 4. 1" NPT inlet and outlet standard 5. Optional inlet and outlet connections available 6. Accommodates inlet gas pressures from 20 PSIG to 200 PSIG 7. Set points from -0.5 inches water column to 69.2 inches water column 8. Optional flow plugs to meet specific flow requirements 9. Fully field serviceable 10. Pressure balanced poppet provides consistent opening over a full range of inlet gas pressures 11. Optional pilot and sense line gauges 12. System purge and field test capability available 13. Factory tested and certified The valve's available Materials of Construction are: STANDARD: 316 Stainless Steel VALVE BODY & COMPONENTS CUSTOM: Others STANDARD: 316 Stainless Steel FITTINGS & HARDWARE CUSTOM: Others SPRINGS 302 Stainless Steel STANDARD: Buna-N SOFT GOODS CUSTOM: Neoprene, Viton®, EPDM, Chemraz®, Kalrez® & others DIAPHRAGM STANDARD: Aluminum/Zinc/Polypropylene/Buna-N/Acetal FILTER CUSTOM: Stainless Steel/Polypropylene/Viton®/Acetal

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September 30, 2005 Rev: 0

Art Montemayor

Storage Tank maximum liquid inventory =

75,000 gallons =

Storage Tank straight height =

10,026 ft3

25.0 feet

Storage tank internal diameter =

2.5 ft

22.60 feet

Assume a fixed, cone-roof storage tank as shown: 2 Volume of Cone roof = (3.1416 r ) (h) / 3 3 = 334.2 ft 3 Vol. of cylindrical vapor space = 401.0 ft 3 Total vapor space Volume = 735.2 ft

Total tank volume = % tank vapor space volume =

22.6 ft 23.6 ft

3 10,761.3 ft

6.83%

If an API fixed, cone-roof tank is equipped with an inflatable rubber "balloon" or "lung" as a gasholder, and the tank is designed for 24" MAWV and 5 psig MAWP, the additional gasholder volume required would be: P1 V1 = n R T = P2 V2

where,

V2/V1 = P1/P2 V2/V1 = V2 =

P1 =

15 psia

P2 =

20 psia

V1 = Total empty tank volume, ft3 V2 = Total tank + gasholder, ft3

0.75 0.75 V1

V2 = Gasholder volume + 0.0683 (total empty tank volume, V1) Gasholder volume = (0.75 V1 - 0.0683 V1) = 0.6817 V1 So, the gasholder would have to have a full volume capacity of approximately 70% of the total empty tank volume. This estimate assumes that the volume occuppied by the interconnecting piping between the tank and the gasholder is negligible. This is quite a large volume and occupies a very large space besides, or on top of, the tank.

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Art Montemayor

Tank Blanketing: A Complete Guide for Designers, Installers and Users Part I of IV

Nov 01, 2005 Rev: 0

by Paul R. Ostand, PE Knowledge is key to protecting a tank's stored product, protecting the tank itself, the atmosphere that workers breathe, and -- last but not least -- life and property from accidental fires.

The Nature of the Process and Definitions Tank blanketing is a term commonly used in industry to refer to the procedure in which a stored liquid is protected by a gas space (blanket or pad) above the liquid. Nitrogen is commonly used, although other gases may be employed. This process also is referred to as tank blanketing, inert gas blanketing, inerting, nitrogen blanketing, padding, or any combination of these terms. These terms will be used interchangeably in these articles. The process consists of providing a gas delivery system to maintain the pressure of the gas blanket as the temperature and liquid level in the tank varies. These will vary due to liquid transfer, leakage, or thermal effects. Tank blanketing has been in use for several decades. The process can be divided into two components: pad (make-up) and de-pad (vent). Pad is the portion of the process that provides blanket gas into the tank’s vapor space, maintaining its pressure and thereby its gas blanket. This involves admitting an inert gas into the tank when the liquid level or the pressure in the gas space drops. The liquid level will drop when pumping off, resulting in a decrease of the gas space pressure (due to its increased volume) and requiring additional inert gas to maintain the vapor space pressure. Additionally, the gas space pressure will decrease due to diurnal effects, weather changes, or temperature drops in the process. In any case, this will necessitate adding inert gas to maintain the blanket pressure in the gas space. The de-pad process functions to remove gas from the tank’s vapor space in cases where the pressure in the gas space increases. This is a venting function. The de-pad valve is also referred to as a tank vent. The liquid level will rise when pumping liquid into the tank, resulting in a decrease in the volume of the gas space, requiring removing gas to maintain the pressure. In addition, the pressure of the gas space will rise due to diurnal effects, weather changes or temperature increases in the process. In any case, this will necessitate removing or venting gas to maintain the blanket pressure. The combination of these two operations may also be called make-up and vent. Valving is used to perform the operations. It may involve two independent valves or a combination unit. In addition to the pad and de-pad equipment, a tank will usually have an additional vacuum and pressure vent. These have set-points outside of the nitrogen blanket system's operating pressure range. They function to protect the tank, personnel and property in case of failures. The vacuum vent’s purpose is to prevent tank collapse from vacuum. The pressure vent protects against damage from over-pressurization of the tank. This vent is also called the normal vent, or simply tank vent. You might use or have heard the term “ullage” or “ullage space” . This is the same as the vapor space mentioned above.

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Purpose

Of course, there are sound reasons why a tank blanketing system is used. There are several reasons and their use depends mostly on the nature of the liquid in storage. This will also influence the nature of the gas used. From the beginning of this article, it is apparent that the gas pressure in the vapor space is being controlled. This pressure control also, indirectly controls the concentration of blanket gas within that space. (More about this in Part IV, in the September Flow Control, under Initial Purge.) Possibly the most common reason for using gas blanketing is to prevent, or reduce, damage by oxidation to the stored product or the tank’s internal wall material. In such cases, a gas such as nitrogen is used - hence, the term nitrogen blanketing. This replaces atmospheric air contact with the stored product or the tank material. The product and the material are both protected to resist degradation by contact with the oxygen and moisture content in atmospheric air. In some cases, the goal might be to protect the stored product from contamination by atmospheric air. Atmospheric air contains moisture as well as particulate contaminants. If these can spoil or degrade the stored product, air contact must be avoided. Commonly used for this are also nitrogen and carbon dioxide. In other cases, we are not trying to protect the stored product but are trying to protect the atmosphere that we breathe from product vapor emissions. In this case, the blanketing system maintains and contains a gas atmosphere inside the tank. This gas does not vent to the atmosphere. A pipe-away vent is used to direct vapors to a processor. The processor will remove or dispose of objectionable vapors. Last, but certainly not least, is to reduce the possibility of combustion. In the case of combustible or flammable liquids, replacement of atmospheric air with an inert gas blanket enhances safety. Again, nitrogen blanketing seems to be the gas of choice for the industry. These cases may be justified on economic grounds or as just inherently necessary to the process.

Economic Justification To justify the equipment economically one might consider the savings from the following: 1) 2) 3) 4)

Protecting the stored product from damage or degradation. Protecting the tank material from corrosion. Protecting the atmospheric air we breathe from contamination. Protecting life and property from damage by fire.

What Industries Are Known to Use Gas Blanketing? I hesitate to indicate which industry might be the largest user. However, it is true that the chemical industry is a large user of gas blanketing. There are so many chemicals protected by gas blanketing that I will not attempt to list them. Suffice it to say that any chemical that needs to be protected for any of the purposes in the previous section is certainly a candidate for gas blanketing protection.

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The food processing industry is a user of nitrogen blanketing. Protection of the product from the atmospheric Rev: 0 air is the reason. Air can spoil the food product by oxidizing, which leads to spoilage. Air also can contaminate the food by water and particle contamination. Protecting stored vegetable oils is a major application here. The manufacture of electronic semi-conductors requires cleanliness far in excess of that required by common chemicals and food products. In addition, this industry uses some chemicals, which if left uncontrolled would be an air pollutant. In this category are volatile organic chemicals (VOCs), which must be kept from evaporating into the air. Gas blanketing will control this type of fugitive emission. Hydrocarbon fuel storage is another controlled product. As above, using gas blanketing could control the fugitive emissions of vapors from these products. High temperature oil is used as a heat transfer medium. This oil is heated to very high temperatures and is affected by contamination with atmospheric air or moisture. Some of these hot oil systems protect their oil with dry, inert gas blankets.

Methods and Requirements The central piece of equipment in tank blanketing is the tank. The tank size is determined by the needs of the process. In sizing, ullage space is provided for expansion as well as to prevent overflow of stored product. These tanks are usually low-pressure tanks. One definition of low pressure is less than 15 psig. However, as we shall see, gas blanket pressures are usually less than one psig. Tanks need be pressure tight to satisfy the needs of tank blanketing. In fact, when older, existing tanks are put into tank blanketing service, pressure tightness can be a problem. Several organizations provide guidance and recommended practices for the tank construction and operation. These include API1, FM2, NFPA3 and UL4. ASME5 pressure vessel codes refer to tanks at or above 15 psig. While there are codes that apply to tank construction and operation, there are not any codes that directly cover the blanketing process. The API Standard 20006 does offer some information that is helpful in determining how to size the pad and de-pad systems. I shall deal with this in some detail in the section on sizing next month. API offers several publications regarding storage tanks. NFPA has information on handling and storing flammable liquids7. Contact the organizations referenced at the end of this paper for a list of their publications. The valves, fittings, and connections used in tank blanketing are only special in that the controlled pressure is very low, necessitating valves that can reliably maintain the pressure. They must be able to react quickly to changes in the controlled variable. The engineer will take into consideration pressures, temperatures, and acceptable materials of construction in selecting valves and fittings. As in all installations, safety must be taken into consideration. Don’t be fooled by the low-pressure operating conditions. There is always the possibility of an accident due to incorrect design, even with low pressures. In fact, a low-pressure system can be more prone to failure due to its low-pressure capability. When put into low-pressure service, an atmospheric type of tank may have a factor of safety. However, the maximum pressure rating is still very low. So be careful; don’t be fooled by very low working pressures.

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Art Montemayor

When considering safety in relation to the gas blanketing system, bear in mind the following. The tank must Rev: 0be capable of operating at the desired pressure, with an appropriate factor of safety. The tank must be protected from vacuum and pressure that might occur outside of the operating pressure range and within safe limits of tank operation. Take into account industry or government regulations that apply. The tank must have appropriate safety railings and platforms to protect personnel installing or maintaining the equipment. The equipment must to be installed in a manner that enables these safety requirements. The pad valve must have the capacity to respond and deliver enough gas to keep the tank pressure above the minimum limits set. The tank vacuum protection valve must have adequate capacity to protect against vacuum collapse should the normal operating equipment fail to maintain the tank pressure above the minimum. In a like manner, the de-pad tank blanketing vent valve must be able to respond and maintain the tank upper operating pressure below the maximum limit set. The tank pressure protection valve must have adequate capacity to protect the tank against failure due to over-pressurization. Finally, there may be an emergency fire exposure vent. While outside of the operating range of the equipment previously described, it must be properly sized for this important function. Consider one more safety point: Do not be fooled into thinking nitrogen is safe. It is in the context we have been discussing, but it will not support life. We need oxygen as well as nitrogen to breathe. Personnel need to be trained that they must not enter a tank containing nitrogen, without wearing supplemental breathing apparatus. Carbon dioxide and other gases also present hazards to recognize.

Selection of an Appropriate Blanketing Gas Selecting a blanketing gas requires you to answer some questions. Which gases are compatible with your product? What are the costs of these gases? How available are they to your site in the quantities you will need? As I mentioned earlier, nitrogen is a commonly used blanketing gas. It is easy to handle and available almost anywhere. It can be either be produced on-site or purchased for bulk delivery to your site. However, some operations have other gases available on-site that are a by-product of their processes. If these gases meet the specifications of a blanketing gas, then these may be the best choice instead of nitrogen blanketing. Some of the most commonly used gases are nitrogen, carbon dioxide, and natural gas. Please keep in mind that these all have very different specific gravities. When sizing, they will require different sized valves and piping. More will be said about this in Part II. References: 1 American Petroleum Institute (API), 1220 L St., Washington, D.C. 20005-4070, 202 682-8000 2 Factory Mutual, 1301 Atwood Ave., P.O. Box 7500, Johnston, R.I. 02919, 401 275-3000 3 National Fire Protection Association (NFPA), 1 Batterymarch Park, P.O. Box 9101, Quincy, MA 02269-9101, 617 770-3000 4 Underwriters Laboratory, 333 Pfingsten Rd. Northbrook, IL 60062-2096 Page 27 of 46

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5 ASME International, Three Park Ave., New York, NY 10016-5990, 800 843-2763 Rev: 0 6 API Standard 2000, Venting Atmospheric and Low Pressure Storage Tanks, Non-refrigerated and Refrigerated. 7 Flammable and Combustible Liquids Code Handbook, Robert P. Benedetti, C.S.P., Ed., NFPA

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Art Montemayor

Tank Blanketing: A Complete Guide for Designers, Installers and Users Part II of IV by Paul R. Ostand, PE

This second of four articles looks at several styles of valves suitable for tank blanketing and focus on how to select the atmospheric discharge vent and the pipe away vent valves. There are several styles of valves suitable for nitrogen blanketing. However, some are more suitable. Further, we need to look at the application, both pad (make-up) or de-pad (vent). Venting can further be divided into the tank pressure-temperature (PV) vent, the emergency fire exposure vent, the atmospheric discharge vent, and the pipe away vent. The last two are usually part of the tank blanketing system. I shall briefly treat each device, but the purpose of this paper is to discuss tank blanketing, so my emphasis shall be on those two valves and their function. Before discussing hardware, we need to look at how all of these devices’ settings are related to each other. This will also make their purpose clearer. In each case the term “set-point” refers to the pressure at which the device is set to open. In fact, manufacturers' precise definition of this pressure may be somewhat different. What is important is that you know how they define it. Starting at the lowest value on the chart, I will explain each.

Vacuum Vent Set-Point The tank low pressure protective device is the vacuum vent. It is usually a component of the tank vent. It is considered part of the normal venting function. Most tanks can tolerate very little (or no) vacuum, so its setting will be very close to atmospheric pressure. Besides protecting the tank, it is the lowest system operating pressure. Should this vent operate, it will admit atmospheric air to the tank. Careful consideration of the conditions must be taken into account when selecting and sizing. It should not open under normal operating conditions.

Tank Blanketing (Pad) Set-Point This is the operating pressure for the pad valve. It must be far enough above the vacuum vent setting so that there is no overlap that would cause the vacuum vent to open. This requires additional explanation. Most blanketing valves have an operating curve, referred to as a droop curve. "Droop" is a drop-off in controlled pressure as the valve opens further and further. Should the controlled pressure drop into the operating range of the vacuum vent, this vent will open to protect the tank. The specifying engineer needs to determine for the blanketing valve specified that there is enough “space” so that the controlled pressure does not drop into the vacuum vent operating range. This will necessitate consulting the manufacturer’s specifications. Be also aware that the blanketing valve may require additional pressure build up to fully shut off. This pressure rise above set is called “lock-up”. Lock-up occurs as the valve mechanism applies further force on the valve trim to seat it and fully shut off. This is actually a very small leakage flow. It should not be ignored, but in the big scheme of things, its effect is small. Again, the amount of lock-up pressure needs to be found from the manufacturers specifications. There will be more about this in the section to follow on PRVs.

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Art Montemayor

Tank Blanketing (De-pad) Set-Point

This is the operating pressure for the de-pad valve. The de-pad valve might simply be the tank’s normal vent doing double duty and venting to atmosphere, or "piped away" to a remote vapor collection or disposal device. In either case, it needs to be high enough above the blanketing valve’s operating range so that they do not interact. Here again, consult the manufacturer’s specifications. Should there be interaction, both the blanketing and vent valves would be open together and blanketing gas would be wasted through the vent. I shall call the separation of operating points “deadband”. That is a pressure range, or band, in which we do not want both valves to operate. The most common operating problem is when these two valves are set too close together. When the vent valve opens, the tank pressure may drop. This is especially so if the vent demand is low. Low demand could occur if the tank pressure rises slowly due to atmospheric heating. The valve, being sized for maximum conditions, would briefly open and shut. This could cause the tank pressure to drop and the blanketing pad valve to open.

Pressure Vent Set-Point This set point is the next higher on our scale. The pressure vent is necessary to protect the tank. It is the maximum working pressure that the tank might see in normal operation. This vent is usually a “tank vent” with both pressure and vacuum valves. Again, as in the previous example, we need a deadband to separate the valves.

Emergency Pressure Vent Set-Point This vent is the last-ditch pressure protection. It is a large vent valve designed to pass enough fluid to protect the tank when exposed to a fire. Knowledge of the tank's pressure capabilities is essential. Consult the manufacturer’s specifications as well as applicable codes and practices.2

The Hardware Pad Valve The types of valves available for use as a pad valve are: 1) Direct operated pressure regulating valves (PRV) 2) Pilot operated pressure regulating valves (PPRV) 3) Control valve and control loop In practice, only the first two are used. The control valve is usually inappropriate. Blanketing is not a continuous type of process. Typically, the valve is not flowing for long periods. Pump-out operations are usually of short duration. Control valves require some time to cycle in to their set-points. Usually, there is not enough time available before the demand ceases. In addition, the control valve and loop components are the most expensive option.

PRV This is the basic valve for control of pressure. It has the fastest response. Control pressure is applied to a spring-loaded diaphragm, which operates the valve plug to open or close the valve. The design of the PRV is such that droop is a characteristic of these valves. It occurs when flow is increased. The spring is extended to move the plug and its force diminishes. This is the force applied to the diaphragm. The magnitude of this force, over the area of the diaphragm, defines the controlled pressure (force ÷ unit area). As the valve opens, the force is reduced and the controlled pressure “droops” off. Rising tank pressure closes the valve. Falling tank pressure Page 30 of 46

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opens the valve. Droop should not be a reason to reject using a PRV valve. Knowing droop, one can Rev: 0 accommodate it into the design. The droop will merely extend the operating range of the valve. This, then, will help in establishing the blanketing valve set-point above the vacuum vent to avoid pressures lower than those desired. Lock-up is another characteristic of the PRV. In operation, when the internal valve plug contacts the valve seat, full shut off is not obtained. This is because the seat will leak until an additional force is applied to the plug to stop leakage flow. The additional force is obtained from the controlled pressure acting on the diaphragm. In other words, the tank pressure continues to rise (due to the leakage flow) and applies added force to the valve plug by means of the diaphragm. The controlled pressure will continue to increase until the valve is shut terminating leakage flow. The additional tank pressure increase is called “lock-up” pressure. This shut-off is bubble tight and can only be achieved with a soft seated valve. Be advised that there are different styles of valve construction, which lock up differently. Only soft seat valves are appropriate for tank blanketing. A properly selected and sized PRV is an excellent choice for tank blanketing.

PPRV The PPRV can be considered a combination of two valves. These are usually in one “package”. One is a small PRV that operates as the PRV previously described. The second valve is operated by the first. While the internal construction of various manufacturers’ valves might differ, the purpose is the same. A diaphragm and spring operate the pilot valve. The pilot valve is very small and only has to supply a controlled flow to operate the main valve. Being small, it also has a short stroke to open and close the pilot. The short stroke means that the spring travel is small and will result in less droop. The PPRV does have less droop and can control closer to set-point. The PPRV is also more appropriate for larger flow requirements because the diaphragm does not have to provide the higher seating force that a larger plug requires. The pilot valve also extends rangeability, as its two-valve construction makes it capable of controlling very small flow rates. The PPRV does still have droop and lock-up as mentioned previously. The droop should be less than a PRV of the same capacity. Lock-up may or may not be less. Again, check specifications with the manufacturer.

Sensing Line The location of the sensing line is an important consideration regardless of the style of blanket valve. In all cases, the sensing connection must be at the tank. It must sense the vapor space pressure in order to provide accurate control. In operation, the backpressure (piping friction loss) created by flowing gas from the valve to the tank can be as much or more than the controlled pressure. This backpressure is not constant but varies exponentially with the flow rate. If sensing is attempted in or near to the valve, such as in the valve body or the delivery piping, it will sense the sum of the tank pressure and the backpressure, resulting in premature shut off. Upon shut off, flow terminates, and the backpressure component disappears. The valve now senses the tank pressure only, which is below set and the valve opens, repeating the cycle. This is a constant cycling of the valve without the tank reaching set-point. The blanketing valve must not be configured for internal pressure registration. It must have a connection for field installation of a remote sensing line direct to the tank vapor (ullage) space.

Valve Materials of Construction Proper selection of the materials of construction is essential for a reliable system. Improperly applied materials can lead to poor performance or even the failure of the hardware to perform its function. The points to consider are: a) Compatibility of the materials with their environment; and, b) Compatibility of the materials within the expected range of temperatures.

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Manufacturers may only offer certain materials in their product. It is still prudent for the user to confirmRev: that 0all materials are appropriate for their expected usage. In most cases, the materials expert is the user. The user most likely has other hardware in similar service. Under normal conditions, pad valves are exposed to the blanketing gas, and the vent valve is exposed to the tank vapors. When considering this, be aware that although the blanketing valve may normally handle nitrogen, it is possible to overfill the tank and expose the valve to tank contents. Purges and check valves may be employed to limit exposure. Don’t ignore the importance of selecting the proper elastomers and plastics. These materials are more sensitive to temperature and chemical contact than the metals. Material hardening, softening or even dissolving can cause serious problems and system failure. Further, contact a supplier’s technical department for assistance in selecting materials.

Venting Venting refers to several different functions. It is performed by several different pieces of hardware. The tank pressure and vacuum ratings must be known in advance in order to select the vents and the operating pressures. Used tanks, without PV ratings, must be cautiously and carefully evaluated to see if they are safe to use. The pressure-vacuum vent (PV) is a protective device. It is also called the normal vent or tank vent. It often contains both functions in a single unit. It would have separate vacuum and pressure sections. Usually, it is has a weighed pallet construction. The weights determine the operating vacuum or pressure. The pallet functions as the valve. They are very simple in construction. The vacuum vent provides essential protection against vacuum collapse. Most tanks have little capability to resist internal vacuum. A collapsed tank will result in a spill, a non-repairable tank, and possible damage to associated equipment. It would be a hazard to life and property – both on-site and off-site. Select this vent carefully, working with the tank and vent manufacturers. API publications offer help in this area. The pressure portion of the PV tank vent protects against tank overpressure. It is set above the blanketing system operating range. Depending on the system, it may also function as the blanketing vent. Systems allowed to vent to atmosphere combine the blanketing upper limit and pressure vent setting into a single vent. This simplifies the installed system. This vent can be direct to the atmosphere or pipe away to a remote location. In a pipe-away vent, any backpressure in the discharge will change the vent set-point. This pressure directly adds to the pallet loading pressure.system operating range. Depending on the system, it may also function as the blanketing vent. Systems allowed to vent to atmosphere combine the blanketing upper limit and pressure vent setting into a single vent. This simplifies the installed system. This vent can be direct to the atmosphere or pipe-away to a remote location. In a pipe away vent, any backpressure in the discharge will change the vent set-point. This pressure directly adds to the pallet loading pressure. Characteristics of these vents include small seat leakage, additional pressure buildup and reseat pressure. Because of their construction, these products are not capable over time of remaining bubble tight. There is an additional pressure buildup in the tank to fully open the valve. During full flow, the tank pressure will have to rise to some percentage above the set pressure. Additionally, when tank pressure reduces, the vent will not reseat until the tank pressure drops somewhat below the opening set pressure. If these characteristics are not acceptable, then consider using pilot operated vents and de-pad valves. If pipe-away venting is required, it often is for environmental reasons. The tank vapors are directed to a device to process the vapors. Several methods are in use including refrigeration and thermal oxidizers. Pipe-away venting involves backpressure buildup. The tank vent must be able to operate at its set-point, regardless of the backpressure. In this case, some manufacturers offer de-pad venting valves that meet this requirement. Some combine the pad and de-pad valves Page 32 of 46

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into a single packaged unit.

References 1 American Petroleum Institute (API), 1220 L St., Washington, D.C. 20005-4070, 202 682-8000 2 API Standard 2000, Venting Atmospheric and Low Pressure Storage Tanks, Nonrefrigerated and Refrigerated.

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Tank Blanketing: A Complete Guide for Designers, Installers and Users Part III of IV by Paul R. Ostand, PE

Failure to size valves correctly can result in operational problems, damage to the stored product or even damage to life and property. It is important to determine the correct size and capacity required, for the valves and tank vents used in tank blanketing. The hardware’s purpose, in combination, is provided to protect from under or overpressure conditions during operation. Failure to do so can result in operational problems, damage to the stored product or even damage to life and property. Sizing is not difficult if one knows under what parameters the system will operate. Proper sizing results in a proper operating system. In Part I the relationship of the various pressure/vacuum set points were discussed and how they might interact if not properly set in relation to each other. All of this hardware, combined, is a system and must be evaluated as such. I have often been asked about reducing gas usage by means of lower set-points for the pad valve. In fact, the lower the set-point, the less gas will be used. However, this saving is very small. The volume of gas saved is in ratio to the absolute pressures, not the gage pressures. While it is worthwhile to reduce gas usage, it should not be a primary objective. It is more important and worthwhile to raise the pad set-point to prevent interaction with the vacuum vent. Following this train of thought, accuracy of regulation is important only when related to the deadband between valves and vents. The actual accuracy is not important unless compared to the available deadband. The more deadband available, the less accuracy required. In your design, emphasize selecting set-points in relation to the deadband between devices.

API 2000 - Recommended Practices API 2000 is recognized as the authority for sizing. Most, if not all, hardware manufacturers reference it. In addition, it offers insights into the proper design of venting for tanks. To its credit, there is an Appendix which provides background as to how the sizing method has been derived. I strongly recommend reading this publication. In order to use API 2000 for sizing you will need to know the flash or boiling point for the stored liquid. Table 1, contained in API 2000, provides normal venting requirements due to liquid flow. Table 2 will give thermal venting capacity requirements for inbreathing (vacuum vents) as well as outbreathing (pressure vents). The sum of the flows from Table 1 and 2 determine the vent requirement. An additional amount need be considered for the pressure vent. One need determine the maximum flow that could pass through the tank-blanketing valve, should it fail open. This value is available from the manufacturer. The outbreathing venting requirement previously determined from tables 1 and 2 needs to be at least this large. Further, an engineering analysis need consider whether the combination of maximum pump-in, maximum thermal outbreathing and blanketing failure could simultaneously occur. In such a case, the pressure vent requires the capacity to handle the sum of all three.

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Tables 3 and 5 included in the API standard are used for emergency vent requirements. Knowing these Rev: 0 requirements allows you to go to the vent manufacturers catalog and find the appropriate size vent. When sizing pad and de-pad valves, the engineer should carefully review the basis for the sizing to determine whether the basis used in API 2000 is appropriate for the specific application. Tables 1 and 2 again can be used to determine the normal liquid transfer and thermal portion of pad (inbreathing) and de-pad (outbreathing) flows. However, they may well oversize the pad and de-pad valves, which can cause some operational problems. The possible problem is best understood by reading Appendix A of API 2000. It was developed, in part by assuming the tank to be in the southwestern USA, and cooled by a sudden rainstorm on an otherwise hot day. This would rapidly cool the tank and require rapid inbreathing to protect the tank. Outbreathing was assumed to require 60 percent of inbreathing flows. These assumptions may well oversize the PV vents. On a simple, non-blanketed, storage tank that is not a problem. The tank vents are relatively inexpensive, especially as compared to the cost of a tank. In addition, oversized vents in that application are not likely to cause an operational problem. When determining the requirements for the pad and de-pad valve, I recommend that careful consideration be given to the selected flow requirement. Look at it this way, if our problem were to be blanketing water contained in an indoor tank, there is no need to compensate for liquid volatility or thermal changes for pad and outbreathing sizing. Simple direct displacement, gallon for gallon would suffice. Some users recognize the issues with API 2000 to their specific operation and apply their in-house correction factors to those tabulated values in API 2000.

Tank Integrity Possibly the most prevalent operational problem encountered with tank blanketing can be related to storage tank leakage. This is usually due to leaking gaskets in the vapor space. A leaking tank will result in a constant inflow of blanketing gas through the pad valve. This is a continual waste of gas. This outflow will be a mixture of tank vapors and blanket gas. The only way to avoid this problem is to seal all leaks.

Location of Valves or Tank Vents Install all of the hardware discussed in this paper on top of the tank. Tank vents need be in communication with the vapor space so that there is no liquid transfer through them. This means vents need be directly fastened to the top of the shell of a horizontal tank, or the roof of vertical tanks. Piping between the vent and the tank is not recommended. Vents capacities are based on direct connection; additional piping or fittings will reduce the valve's installed relief capacity. There is an additional reason for locating the pad blanketing valve on the top of the tank. This relates to the sensing line. It may be easier to discuss this by considering a pad valve located at ground level and having its outlet and sensing lines running vertically to the top of the tank. Further, assume a blanketing set-point of two inches water column (in. WC). Condensation, or collection of liquid, in the sensing line will apply a head pressure to the valve diaphragm. A collection of two inches of liquid would equal the set-point and the valve would never open, because it would consider the tank pressure to be at set. This condition can result in ingress of atmospheric air through the vacuum vent. In a worst-case scenario a vacuum collapse of the tank. For this reason, all pad valves need be located above the liquid level in the tank and have piping self-draining to the tank.

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The delivery line from the pad blanketing valve should extend a short distance in to the tank, above the maximum Rev: 0 liquid level. The sensing line should be located away from this discharge line to avoid interaction. Some manufacturers offer special fittings to connect both connections to a single tank nozzle. These devices are designed to avoid interaction and are well-worth their cost. All of the following devices are optional. I will describe their advantages and merits for consideration.

Isolation Valves Isolation valves are very useful should a pad valve need be replaced. They allow the blanket gas source and the tank vapor space to be isolated, preventing leakage from either. These valves should be full flow valves, such as ball valves, and be rated for the service pressure, temperature, and product contact. It is very important that they be operated in the correct sequence to prevent damage. Incorrect sequencing can cause over pressurization and failure. For this reason, it is advisable to place the appropriate warning tags on the equipment and remove the valve handles. The sequence for opening the valves is as follows: 1. Open the discharge isolation valve (located between the pad valve and tank). 2. Open the sensing line isolation valve 3. Slowly open the pad valve inlet isolation valve. When the valves need be closed, and removing the pad valve would cause system problems, first shut the process down. The sequence for closing the valves is: 1. Close the pad valve inlet isolation valve. 2. Close the discharge isolation valve. 3. Close the sensing line isolation valve. Do not remove the hardware unless you are sure that no pressure or hazardous gas or liquid product is trapped in the valve or piping.

Check Valve Check valves can be provided to prevent liquid from backing up into the pad blanketing valve. They can only be installed on the pad blanketing valve tank (gas delivery) line. Never use a check valve on a sensing line. Sensing lines require bi-directional flow. A check valve would cause system failure. Never use check valves on vents or de-pad valve. They would reduce the installed flow capacity and could be a safety hazard.

Purges Purges are commonly used to prevent or reduce the amount of tank vapors migrating into the pad valve. They would be connected to the pad blanketing valve discharge and sensing lines, close to the pad valve. These are useful devices but bear in mind that to function, they must continually deliver gas. The gas is metered through a Page 36 of 46

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rotameter and adjusted for a flow of about 0.5 scfh of gas. The purge flow will be continuously vented by the0 Rev: normal pressure vent or de-pad valve. The tank pressure will stabilize at the vent set-point pressure. Manufacturers can provide these on their equipment. It is not necessary to purge vents or de-pad valves as they must be able to handle contact with the tank vapors.

Blanket Gas Supply Line Sizing The sizing of the blanket gas lines must be considered. This is the line providing blanket gas to the pad blanketing valve. Merely using piping the same size as the valve may not be adequate. The piping, and gas supply, must be of adequate size, to provide the full gas flow to the blanketing valve at the necessary pressure as measured at the valve inlet. For this reason it is good engineering practice to provide an inlet pressure gage at this valve. Undersized piping may provide adequate pressure at low flow rate demands. Yet, at higher flow rates, the pipe size may be inadequate. Piping restricts flow by causing pressure drop. This is caused by the pipe fittings, diameter of the pipe and the roughness. It is not difficult for a piping engineer to properly size piping at the design stage. It is very difficult and expensive to correct for improperly sized piping after it is installed.

Pipe Away Vent or De-pad Line Sizing First, pipe away with a standard, pallet weight loaded, vent is not good. These vents are directly affected by the backpressure in the pipe away. That pressure is the sum of the piping friction losses and the backpressure created by any associated downstream device. The backpressure is not constant; it is dependent upon velocity (flow rate). The actual, in service, set point of weight-loaded vents is the sum of the backpressure plus the weight setting. Therefore, the tank pressure also rises above what it would be without pipe away. If this variable pressure can be tolerated by the system, there is no problem. Otherwise in order to have a constant set-point you will need to use piloted venting or de-pad valves that are not affected by backpressure.

Safety In all cases, always consider the safety of all plant personnel and equipment in that order. o Install the necessary guards, railings, and stairways for both installation and operational work. o Be sure that pipe, valves, and fittings have the appropriate safe working pressures and corrosion resistance for the application. Apply the appropriate engineering or legal codes into design considerations.

o Consider the effect of a reduction of wall thickness, over time, due to corrosion. o Consider the effect of corrosion over time on the pipe internal roughness. Use a higher roughness factor to compensate.

o Provide the proper pipe and valve supports to reduce structural piping stresses, tank loads and bending loads on valves. Valves are not pipe supports.

Multiple Tank Installations Conditions arise where several tanks need to be gas blanketed. These tanks are usually in close proximity and require the same blanketing gas and pressure. When this occurs plant operators may desire to use one tank-blanketing valve for the entire group of tanks. This would involve installing a manifold to interconnect all of the tank vapor spaces to a single pad-blanketing valve. This may be possible. Before proceeding with Page 37 of 46

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an analysis, the engineer must be able to answer yes to the following questions regarding the pad valve. Rev: 0 o Is it acceptable if liquid or vapors from the various tanks intermingle? o Are all of the connected tanks rated to operate at the same design pressures? o Can the blanketing valve control gas flows and tank pressures from the smallest anticipated flow rate requirement from any single tank up to the maximum flow rate required for all tanks simultaneously? o Is it acceptable, if in case of valve failure, that all tanks go out of service at that time? If the answer to all of the above is YES, then the engineer can proceed to estimate the installed cost of the manifold piping and a single valve as compared to multiple valves, without the manifolding. Should this show an economic advantage, then a single valve serving multiple tanks may be the best for this job. Otherwise stay with one valve per tank, or in the case of a large number of tanks, look at serving a smaller group of tanks with a single pad-blanketing valve. It is never recommended that the tanks share normal PV, de-pad, or emergency vents. Common piping could cause large backpressures, venting problems, and possibly an accident.

Other Installation Issues It is good practice to provide pressure gages. Gages provide a great way to observe operation and analyze any problems that may arise. In the overall scheme of things, they are inexpensive. It is valuable to know the inlet blanket gas pressure and tank vapor space pressure to evaluate system performance. The location of the gages depends on the installation. Whether they should be at the point of measurement, or remote with transducers, is entirely the decision of the plant operator or engineer. Two gages are required. Install an inlet pressure gage at the inlet of the pad blanketing valves gas supply line. Second, a pressure gage measuring the tank vapor space pressure. Use gage isolation valves between the gage and system. This allows for removal and replacement. Some operations also install flowmeters in the blanket gas supply. These can be anything from a simple vane instrument to indicate a relative flow rate or even a totalizing meter indicating usage volumes. (Bear in mind that these flow measuring devices will only show flow for those short – and hopefully few – periods when the tank requires makeup blanket gas. Also keep in mind that some flowmeters do cause friction loss. Assure that this loss will not impede providing the necessary gas flow rate under maximum conditions. An instantaneous flow measurement only serves the practical purpose of indicating the existence of a flow at a specific moment. However a totalizing flowmeter serves to measure the consumption of inert gas by the tank serviced and is a measure of the efficiency of the operation.

Initial Tank Purge The last item in this section is initial tank purging. When a new tank is put into service or an existing one back into service, it is likely that the vapor space will contain a very high percentage of air. It is desirable to reduce this to a very low proportion of air by diluting the tank vapors with blanketing gas. This can be done by introducing a volume of blanket gas into the tank. The question is: what amount of gas is adequate to achieve the desired concentration?

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Suppliers of Nitrogen gas have looked at this question and can provide answers to their customers. I encourage Rev: 0 the engineer to contact such a source. One supplier (Air Liquide) has posted a paper dealing with this subject on their Internet site (2). This paper is worthwhile to download. It contains information of methods and shows how to achieve results. This initial purge can be done by a bypass valve and flowmeter. In applications where life, safety, or equipment is at risk an O2 sensor should be employed to confirm the adequacy of the purge.

Summary Providing a tank blanketing system is not a difficult task. However, it does require advance planning and attention to engineering practices and procedures. It should be given the same priority that would be given to any process system design and installation. First and last, consider safety of personnel, the environment, and equipment. In planning be able to identify your needs. Work with operations, engineering, and supply people. Know what size the tank is or will be. Know the pressure capabilities of the tank. Know the product to be stored. Know the liquid flow rates. Know the environmental concerns. Understand the strengths and limits of available equipment. Complete a detailed plan to identify possible problems ahead of time. Determine the amount of gas needed to properly blanket under liquid movement out and thermal contraction. Determine the pressure venting requirements to compensate for liquid movement in, thermal expansion, and possible pad valve failure in the open position. Determine the vacuum vent capacity required to compensate for pad valve failure under the combined conditions of liquid movement out and thermal contraction. Consider the set-points of all the hardware as a system, taking into considering each device’s expected operating pressure range above and below set-point pressure. Consider the effects of the piping size, length, and fittings on supplying adequate blanketing gas. Consider all aspects of safety. By following a solid plan from beginning to end, success is almost assured. But then I think that you know that. I hope that this paper will enable you to reach that goal.

References 1) API Standard 2000, Venting Atmospheric and Low Pressure Storage Tanks, Non-refrigerated and Refrigerated. 2) How to Purge With Nitrogen. Air Liquide web posting at: http://www4.us.airliquide.com/cgi-bin/USBVP10/ReferenceLibrary.jsp?0&OID=-14860

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Tank Blanketing: A Complete Guide for Designers, Installers, and Users Part IV of IV by Paul R. Ostand, PE

Sometimes it seems inevitable that operational problems will occur in your tank blanketing system. When these do, it is often easy to analyze the problem by observing the operating conditions -- especially the gas and tank pressures. When the system has been thoughtfully designed and installed, few problems are likely. Should you have problems, the following charts may help you identify and correct them. 1. The tank pressure is low and out of range. Cause or Symptom

Action or Explanation

The tank is leaking gas beyond the ability of the pad valve to supply gas.

Seal the tank leaks.

Undersized blanket gas supply piping.

Increase supply pressure to increase capacity or replace piping.

Inadequate gas supply pressure or volume.

Increase to necessary amounts.

The pad valve is undersized and unable to deliver adequate blanketing gas.

Increase trim size if possible, or install a properly sized valve.

2. Tank Pressure remains above blanketing set-point when there is no pump out. Cause or Symptom Very oversized pad blanketing valve causes overshooting of pressure. Valve lock-up pressure.

Action or Explanation Install reduced trim in valve. Reduce inlet pressure to reduce capacity.

Lock-up is a normal condition. Consult manufacturer for information on your valve. If the lock-up is not causing the normal pressure vent (or de-pad valve) to release or other operational problems, then consider it as a normal system characteristic.

Purges in use (and the pressure is up to the pressure Purges supply a continual flow of blanketing gas to the tank. vent set-point). This is normal for the pressure to rise to the normal pressure vent (or de-pad valve) set-point.

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Pad blanketing valve seat leakage.

Repair seat or seals.

Thermal heating of the tank contents.

Normal if the pressure is vented properly by the normal pressure vent or de-pad valve.

If the tank pressure is above, and remains above, the normal vent or de-pad valve setting and the system is experiencing either pump in or a large thermal heat accumulation. The vent or de-pad valve is venting some gas.

This might be due to the vent or de-pad valve either not fully open or being undersized. Also, contact the manufacturer to confirm or deny that the amount of overpressure is above the normal pressure buildup that is normal for this device. These normally require a certain pressure buildup, above set, to fully open.

The tank pressure is above, and remains above; the This represents a serious situation wherein the normal normal vent or de-pad valve range and the system is pressure vent or de-pad valve may not be functioning. experiencing either pump-in, or a large thermal heat Examine the hardware to determine the cause. Consider accumulation. shutting the system down until the problem is identified and resolved.

'3. Excessive blanketing gas usage. Cause or Symptom

Action or Explanation

System consumption of gas seems to be higher than Calculate what amount of gas the system should use and what was design or is expected. compare this to the actual usage. If it is high, proceed to the next item. System consumption of gas is high and pad valve is Inspect tank for leakage and repair. continuously supplying gas. Tank pressure are at or below set-point. System consumption of gas is high and pad valve is Inspect normal vent, de-pad valve, or pad valve seat continuously supplying gas. for leakage and repair.

4. Failure of the Pad Valve to Shutoff. Cause or Symptom Blanket gas continually flows.

Action or Explanation Inspect tank for leakage and repair. Inspect normal vent, de-pad valve, or pad valve seat for leakage and repair. Pad valve failure (to shut off). Repair or replace. Inspect vent or de-pad valve for failure to shutoff.

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5. Pad Valve Cycles On and Off Cause or Symptom

Action or Explanation

During pump-off, or a cooling cycle, the pad valve This is typical of attempting to sense control pressure is cycling on and off. internally in the pad valve, or in the blanketing gas delivery piping to the tank. Relocate the sensing connection to directly sense tank vapor space pressure.

This concludes the four part article on tank blanketing. We hope that it has been helpful. Should your organization require assistance on a tank blanketing issue, we are available to provide engineering services to that end as well as general mechanical engineering design.

About the Author Paul R. Ostand, PE, principal of Ostand Design, is a mechanical engineering consultant in Charleston, WV with extensive experience in valve design and applications. He has 10 patents, including three for tank blanketing valves. He is a member of ASME and a life member of ISA. Ostand has been associated with Dover Corp., OPW Division, Richards Industries (Jordan Valve), Appalachian Controls Environmental (ACE), and Fisher Controls. He can be reached by e-mail at [email protected] or by phone at 304 984-2889. His Web site is http://www.ostand.com

This article was originally published in Flow Control , 2003 This document may be copied and freely distributed under the condition that it done so in it's entirety without additions or deletions. Rev: October 23, 2005

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The following illustrated products were developed by Paul R. Ostand for Appalachian Controls Environmental (ACE) of Charleston, WV. They are both direct and pilot operated pad valves as well as a unique (pad-de-pad) valve. These products are used for nitrogen gas blanketing and venting systems in industries such as chemical, pharmaceutical, food processing and computer chip manufacturing. Pad valves are gas make-up valves that supply gas to the vapor space of a tank to maintain a predetermined pressure. De-pad valves, or vent valves, remove gas from the vapor space of a tank in order to prevent the pressure from going below a predetermined maximum. They were designed as part of a project to produce an entirely new line of gas blanketing and venting products. This successful effort resulted in three US and one UK patents. They are now manufactured by Fisher Controls. While they were marketed as tank (nitrogen blanketing) valves, they are basically pressure regulators for very low gas pressure control.

ACE95SR Tank Blanketing Valve 2” body size For regulating gas pressures to 0.5 inch w.c.

ACE97 Tank Blanketing & Venting Valve, ½” thru 4” body sizes. For regulating gas pressures to 0.5 inch w.c. and venting to 4 psi

ACE 95jr tank blanketing valve for regulating gas pressures down to 0.5 in.wc

ACE95 Tank Blanketing Valve '1” body size. For regulating gas pressures to 0.5 inch w.c.

ls Environmental ique (pad-de-pad)

-up valves that or vent valves, a predetermined

venting products.

blanketing) valves,

Ambient temperature = 40 oC

Initial System conditions

Ambient temperature = 15 oC

Subsequent System conditions

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