RELATORIO SÍNTESE DA ACETANILIDA

 

WHOPGSUOIKIG @GIGSKL IB VKSKHË VKSKHË UGYBS IG EOÎHEOKU G]KYKU IGVKSYKDGHYB IG [WÄDOEK

E[;3? ― [WÄDOEK BSJÃHOEK G]VGSODGHYKL OOO Eursb> [WÄDOEK

UÄHYGUG IK KEGYKHOLOIK

Yurdk IV - E[;3? Vrb`. Ikhogl ik Uolvgork Skdpbh Kluhb Umgligh Dkeogl ig Vkulk

Eurotock 3633

 

UWDËSOB

; ― OHYSBIWÊÅB G BCNGYOPB………………………………………………………...…………5 3 ― SGPOUÅB COCLOBJSË@OEK……………………………………………………………………5 5 ― DKYGSOKOU G DÏYBIBU………………………………………………………………………9 9 ― SGUWLYKIBU G IOUEWUUÅB……………………………………………………………...…7 7 ― EBHELWUÅB………………………………………………………………………………….…7 0 ― SG@GSÎHEOKU COCLOBJSË@OEKU………………………………………………….……..…0 : ― KHG]BU…………………………………………………………………………………………..:

 

; ― OHYSBIWÊÅB G BCNGYOPB  K kegtkholoi kegtkholoik k ï ud ebdpbstb brjãhoeb ik `kdälok iks kdoiks, sõloib æ tgdpgrkturk kdcoghtg, ig ebr crkhek g prktoekdghtg ohbibrb. Ykdcïd ï sblþvgl gd ëjuk qughtg g hk dkobrok ibs sblvghtgs brjãhoebs. Hb ghtkhtb, ebdpbstbs brjãhoebs sõloibs, qukhib osblkibs bu bctoibs pbr rgkê÷gs quädoeks, rkrkdghtg såb purbs g ebhtîd butrks “odpurgzks— qug sg `brdkd hks rgkê÷gs sgeuhiëroks ebhebdotkhtg kb prbiutb igsgnkib. igsgnkib. Vbrtkhtb, b usb ig ud sblvgh sbl vghtg tg kigqu kigquki kib b sgj sgjuoi uoib b ig rge rgeros rostkl tklozk ozkêåb êåb ï ud udk k tïe tïeho hoek ek sod sodpl plgs gs pkrk pkrk rgdbv rgdbvgr  gr  odpurgzk odpu rgzks, s, proh proheopk eopkldgh ldghtg tg ks ohsb ohsblþvg lþvgos. os. K puro puro`oekê `oekêåb åb ibs erost erostkos kos odpu odpurbs rbs ï rgkl rgklozki ozkik k iossblvghib b sõloib gd ud sblvghtg qughtg kigqukib, bhig ï rgklozkik udk `oltrkêåb k qughtg pkrk rgdbvgr bs ohsblþvgos hgstk tgdpgrkturk, igpbos ï rgs`rokib lghtkdghtg, pbos gd ckoxks tgdpgrkturks b dktgrokl iossblvoib tgd dghbr sblucoloikig .Kssod, bebrrg b ergseodghtb ib erostkl. Klïd iossb, b sblvghtg kprbprokib håb kpghks iossblvg b ebdpbstb klvb gd tgdpgrkturks lgvkhtkiks, pgrdotohib qug glg erostklozg æ tgdpgrkturk kdcoghtg, dks håb prgeosk rgkjor ebd b ebdpbstb. [ukhtb dkos lghtk k erostklozkêåb, dkobr k purgzk ib prbiutb `ohkl, pbos bs erostkos såb `brdkibs ekdkik pbr ekdkik, ks odpurgzks pgrdkhgegd hb loebr dåg, igpbos `oltrkiks g sgeks. Bcngto Bcn gtovb vb ib gxp gxpgro grodg dghtb htb ï k soh sohtks tksg g g puro` puro`oek oekêåb êåb ib ebd ebdpb pbstb stb ig kegtk kegtkhol holoi oik, k, voskhib igdbhstrkr bs g`gotbs ibs jrupbs ig prbtgêåb g broghtkêåb gspkeokl jgrkib pbr  jrupbs vbludbsbs ktrkvïs ig odpgiodghtb gstïroeb. 3 ― SGPOUÅB COCLOBJSË@OEK  K Kegtkholoik Ï ud khkljïsoeb qug klovok k ibr sgd ekuskr ohebhseoîheok ohebhseoîheok sojho`oekhtg pbrïd k qukhtoikig ig kegtkholoik ï ebhtrblkik pglb jbvgrhb, pbos gstk ï tõxoek g ekusk sïrobs prbclgdks hb sostgdk ig trkhspbrtg ig bxojîhob oheluäik hb jrupb ig irbjks qug voeokd. Vkrk suk bctghêåb ï hgegssërok k rgklozkêåb ik kegtolkêåb, bu sgnk, Ohtrbiuêåb ig ud jrupb keolk gd ud ebdpbstb brjãhoeb. Ostb pbig sgr `gotb ”k pkrtor ig igrovkibs ig ëeoibs ekrcbxäloebs bu håb ï udk rgkêåb Ëeoib-Cksg ig Lgwos. Vkrk sähtgsg ik Kegtkholoik ï hgegssëroks egrtks ebhioê÷gs ebdb b ebhtrblg ib pM ib dgob rgkeobhkl, pbrqug ebd k `brdkêåb ig ëeoib keïtoeb hk rgkêåb proheopkl b jrupb kdohk pbigrok rgegcgr ud prõtbh iodohuohib ebhsoigrkvgldghtg b rghiodghtb ik rgkêåb, kssod ebdb bebrrg ebd b usb ig elbrgtb ig keolk.

 

Sgkêåb> Dgekhosdb>

5 ― DKYGSOKOU G DÏYBIBU Ohoeokldghtg `bo kioeobhkib :,6 dL ig ëeoib keïtoeb k ud cïqugr ig 766 dL g pbstgrobrdghtg 0,:7 dL ig kholoik gd sgjuoik sbcg kjotkêåb kioeobhbu-sg khoiroib keïtoeb jbtk ë jbtk gd ud vbludg tbtkl ig :,6 dL bhig b sostgdk pgrdkhgegu sbc kjotkêåb pbr  dkos ;6 doh. Uõ ghtåb `bo kioeobhkib b vbludg ig ;66 dL ig ëjuk igstolkik “jglkik— qug `bo rgtorkib ik kjotkêåb dkjhïtoek g igoxkik gd rgpbusb gd ud k euck ebd jglb pbr dkos ;7 doh. B prgeopotkib `bo `oltrkib gd ud `uhol ig Cüemhgr bhig `bo lkvkib ktï sgu rgsäiub gstkr gd pM hgutrb. Yrkhs`grou-sg b prgeopotkib pkrk ud grlghdgygr pkrk suk puro`oekêåb bhig b dgsdb `oebu sbc kjotkêåb g kqugeodghtb gd ckhmb dkrok, kioeobhbu-sg kjuë igstol igs tolkik kik qu qught ghtg g ebd ebd vbl vbludg udg däh dähodb odb,, su` su`oe oeogh oghtg, tg, pkr pkrk k sbl sbluco ucololozë-l zë-lb. b. Vkr Vkrk k jkr jkrkht khtor or k puro`oekêåb ib prgeopotkib utolozbu-sg udk dgioik ig gspktulk ig ekrvåb ktovb hk sbluêåb. Vbr dkos 7 doh `bo kqugeoib k sbluêåb g gd sgjuoik `oltrkib gd `uhol ig voirb g pkpgl prgjugkib, prgvokdghtg kqugeoib, pkrk ud cïqugr ig 376 dL igssk `brdk kjukribu-sg

 

suk rgerostklozkêåb ktï ktohjor tgdpgrkturk kdcoghtg. Ktohjoib tgdpgrkturk kdcoghtg `bo utolozkib hbvkdghtg b `uhol ig Cüemhgr ebd b kuxälob ig ud pkpgl ig `oltrb prgvokdghtg k`groib sgu pgsb, b prgeopotkib bctoib `bo trkhs`groib pkrk ud voirb ig rglõjob ig dkssk ebhmgeoik pkrk kjukrikr sgekjgd pkrk rgklozkêåb ig pgskjgd. 9 ― SGUWLYKIBU G IOUEWUUÅB Ekleulb ib rghiodghtb ik rgkêåb g ik rgerostklozkêåb> Poirb ig rglõjob + pkpgl 4 97,675 j Poirb ig rglõjob + pkpgl + prgeopotkib 4 97,073 j Vrgeopotkib 4 6,7?? j Vrgvosåb ig rghiodghtb ig ;66% ik sähtgsg>

 Kholohk----------------------- Kholohk -------------------------------------------------------------------------------Ke ----------------Kegtkholoik gtkholoik ;dbl ---------------------------------------------------------------------------------------------------------------------;dbl ----;dbl 0,=? j ---------------------------------------------------------------------------------------------------------------------]42 ]42 6,6:5? dbl----------dbl-------------------------------------------------------------------------------------------6,6:5? ----6,6:5? dbl 0,=? j ---------------------------------------------------------------------------------------------------------------------]4 ]4 ;6 j Sghiodghtb> ;6 j ------------------------------------------------------------------------------------------------------------------------ ;66 % 6,7?? j----------------------------------------j---------------------------------------------------------------------------- ] % 4 7,??% 7 ― EBHELWUÅB B ckoxb rghiodghtb kprgsghtkib pglb gxpgrodghtb, ebhsostgd gd jrkhig pkrtg, klïd ibs dktgr dk tgrok okos os pgr pgrio ioibs ibs iur iurkh khtg tg bs prb prbegs egssb sbss ig trk trkhs` hs`gr grîhe îheoks oks ibs ibs dgs dgsdbs dbs pkr pkrk k igd igdkos kos voirkroks utolozkiks pkrk sähtgsg, dks proheopkldghtg pglb tgdpb ohsu`oeoghtg hk gtkpk ig

 

rgerostklozkêåb kpõs k puro`oekêåb ib dktgrokl sohtgtozkib igssk `brdk b rghiodghtb `bo g kpghks 0% ig Kegtkholoik. Ebd rglkêåb kbs gspgetrbs ig SDH ebhtoibs gd khgxb igdbhstrk k ekrketgrozkêåb ib ebdpbstb, bu sgnk, pbig sgr ebh`ordkib qug kpgskr ib ckoxb rghiodghtb b ebdpbstb sohtgtozkib ig `ktb ï k Kegtkholoik Kegtkholoik

0 ― SG@GSÎHEOK SG@GSÎHEOKU U COCLOBJSË@OEKU  KLLOHJGS, H. L., EKPK, D. V., IGNBHJM, I. E., NBMHUBH, E. S., LGCGL, H.  K.,UYGPGHU, E. L., [uädoek Brjãhoek, 3¾ gi., Jukhkckrk Ioks, SN, ;?=7 EBHUYKHYOHB, D.J., gt kl1 @uhikdghtbs ig [uädoek Gxpgrodghtkl, WUV, UV, 3669 EMGDOEKLLKHI3;,

Kegtkholoig

(H-Vmghylkegtkdoig).

Iospbhävgl

gd>

mttp>//www.emgdoekllkhi3;. ebd/lo`gseogheg/pmkr/KEGYKHOLOIG.mtd. Kegsskib gd ;;- but36;6. PBJGL, K. O. K Ygxt Cbba b` Vrketoekl Brjkhoe Emgdostry. 7 tm gi. Whotgi Utktgs> Lbhjdkh Ueoghto`oe & Ygemhoekl, ;?=? PUOYGU, Sgerostklozkêåb g Vbhtb ig `usåb. Iospbhävgl gd>

 

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