HAZOP Centrifuge and Dryer
August 19, 2022 | Author: Anonymous | Category: N/A
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HAZOP ANALYSIS To manufacture of Ambroxol hcl
Sta"e
Proce
Hazop Study - Proce ! for Ambroxol Stage-1 Po$ble Hazard % Opera#on &emed$al Ac#on fa$lure Ope perraona onal contr ontrol ol - cch hec eckp kpoi oin nt shal hall be Boom valve in incl clud uded ed in the the ba batch shee heet to to ind ndiicat cate opened, or eakage !hether the boom valve has been closed of Boom "alve prior to charging methanol # is not eaking$ %harging of ðanol, ðanol addion pipe is kept to the Boom 'ire ire ha ha((ard d due ue stac electricit)
Stag St agee-1 1
eacon of -Amino-.,/ibromo Ben(aldeh)de !i !ith th 3ransans-4 4-a -am minoino%)clohexanol,in m me ethanol !ith Sodium boroh)dride
%harging of -amino .,/ ibr ibromob omoben en((aldeh ldeh) )de# de# 3rans-4-amino c)clo6exanol
to of th the e rea eact ctor or *ipe lines are all S S and e+uipment motors are 0ame proof$ 2nstrucon is aid in the SO* , 3o Avoid Spil pillag lage ou outt sid side e tthe he spi pill llag age e outs outsid ide e tthe he 5 5+ +ui uipm pmen ent, t,a a) ) do do!n !n th the reactor, *ol) Bags to %ollect the spilled &aterial,# 3ransfer to the reactor 'ir 'ire eh ha( a(ar ard d due due to SS scoops scoops to avoid avoid sta stacc e elec lectri tricit cit) )$ 3he 3he sta tac c el elec ectr tric icit it) ) re reac acto torr iiss ear earth thed ed b) cond conduc ucn ng g! !ir ires es 2r 2rri rita tao on n to to ski skin n e)es
e0uxing the reacon os osss o off ð ðano anoll mass
# 7sin 7sing g hand hand gl glov oves es # g gog oggl gles es$$ 3he temperature is raised b) slo! heang ll re0ux8 the methanol "apour oss is due to 5xces 5xcessiv sive eh hea eat, t, 2ns 2nstru truco con n iiss 9iv 9iven en iin nS SO* O*,, 3o 3o Open the steam valve to Opmum so as to maintain the re0ux
3he centrifuge is earthed b) conducng !ires$ 3he :ltraon is carried out through a centrifuge$ %entrifuges are high speed machines and sources of ha(ard in a chemical plant$ Ample precauons are taken to carr) out the centrifuging as ha(ard free as possible$ ;e are using a 4< inch dia SS.1= centrifuge, boom driven and top discharge$ this is a four point 'ire ha(ard ha(ard due to sta stac c suspe suspension nsion mac machines hines !hi !hich ch are put on special special vibra 3o sepa separrat ate e the the elec electr tric icit it) ), oper operat ator or mo moun untt for for smoo smooth th vi vibr bra aon on ffre ree en noi oise sele less ss oper opera aon$ on$ ha(ard ha(a rd if an) loadi loading ng > 3he sp speed eed is cont controlle rolled d b) a vari variable able fre+ue fre+uenc) nc) drive drive 2st Stage 'rom the unlo unload adin ing g acv acvit it) ) and and the the fee eedi ding ng of th the e cent centri rifu fug ge is done done b)
%entrifuging
li+uid
%harging *uri:caon of
carri carried ed out in a runnin running g pneum pneumac acall) all) con control trolled led valv valves es at lo!e lo!err *& under centrifuge nitrogen purging$ 5ven the bearing housing of the centrifuge is provided !ith a nitrogen purging facilit)$ An interlocking s)stem is provided for ensuring that the lids cannot be opened !hile the centrifuge is running and thereb) prevenng an) operaonal ha(ard b) human error $ All the limits s!itches and the safet) interlocking s!itches are 0ame proof including the "' controls$ of
Ambroxol
Boom valve opened, or eakage of Boom
Operao Operaonal nal control - checkpoint shall be included in the batch sheet to indicate !hether the boom valve
"alve
eaking$
acetone,
Stage-
%rude B) %arbon 3reatment # %r) %r)sstalli(aon b) 6c 6cl, centrifuging %harging of Amb mbrroxol %r %ru ude
has been closed prior to charging methanol # is not
Spillage out side the react eactor or,,
2nstrucon is aid in the SO* , 3o Avoid spillage outside
the 5+uipment,a) do!n the *ol) Bags to %ollect the spilled &aterial,# 3ransfer to the reactor
'iltraon
6cl Ad Addion
3he 'iltraon Operaon Operaon is %arried out in %losed SS %loth ine, 'ilter cloth cleaned for 5ver) Batch # this Block %leaning of the 'ilter along !ith %loth is 2ncorporated 2n the B* Acetone %harging SS pipe is 'ixed to the Boom of 'ire ha(ard due to the rre eactor stac ele elect ctri rici cit) t) *ip ipe e llin ines es are are a all ll SS and and e e+ +ui uipm pmen entt mot motor orss ar are 0am 0ame e proof$ 3he Addion of 6)drochloric acid is charged through acid the %lose 6)drochoric losed d li lin nes es,, !i !ith thou outt an) Spi pillla lag ge, e,pe perrsonn sonnel el Spillage # 2rritaon *rotecve *rotecv e 5+uipments are 7sed to avoid the 5xposure # tackle the irritaon 3he centrifuge is earthed b) conducng !ires$ 3he :ltraon is carried out through a centrifuge$ %entrifuges are high speed machines and sources of ha(ard in a chemical plant$ Ample precauons are taken to carr) out the centrifuging as ha(ard free as possible$ ;e are using a 4< inch dia SS.1= centrifuge, 'ire ha(ard due to bo boom om d driv riven en a and nd top top dis discha charg rge$ e$ this this is a ffour our point point stac electricit), suspension machines !hich are put on special vibra operator oper ator ha(ard ha(ard if an) mount mount fo forr smo smooth oth v vibra ibraon on free noiseless noiseless oper operaon aon$$ Spillage,'ilter
unloading 3he speed is controlled b) a variable fre+uenc) drive loading > acvit) acv it) carri carried ed out in a and the feedin feeding g of the centri centrifuge fuge is done b) runn runnin ing g ccen entr trif ifug uge e pneu pneuma mac cal all) l) cont contro roll lled ed valv valves es at lo!e lo!err *& *& unde underr nitrogen purging$ 5ven 5ven the bearing housing of the centrifuge is provided !ith a nitrogen purging facilit)$ An interlocking s)stem is provided for ensuring that the lids cannot be opened !hile the centrifuge is running and thereb) prevenng an) operaonal ha(ard b) human error$ error$ All the limits s!itches and the
safet) interlocking s!itches are 0ame proof including the "' controls Solvent recover)
r)ing Separaon of solvents from operaon the product
?o spec speci: i:cc ha( ha(ar ard d %harging of & 6a(ardous !aste a@er disllaon
Al Alll cha charg rgin ing g iiss don done eb b) )v vac acuu uum m ssuc ucki king ng to avoid void spillages and through the closed SS pipe lines$
r)ing of the product in ?o speci:c ha(ard otocone vacuum r)er
%" is :ed !ith 0ame proof motors$ 7nloading into the bins b) actuated valve, 6ence ?o- ess 5xposure 6and gloves # goggles should be used$
To manufacture of Anatrozole Hazop Study - Proce ! for Anastro(ole Sta"e
Proce
Opera#on
Po$ble Hazard % fa$lure
%har %hargi ging ng of , , , ,,-
Spil Spilla lag ge o out ut side side the the reactor,
tetrameth)l-/- meth)l-1,.- ben(ene diacetonitrile eacon of of , , , ,-
Stage-1
tetrameth)l-/- tetrameth )l-/- meth)l1,.ben(ene diacetonitrile !ith Acetonitrile, n-bromo succinamide, 5th)l acetate and ;ater then separate the organic la)er and disllaon organic la)er and added c)clohexa c)clohexane ne
&emed$al Ac#on
2nstrucon is aid in the SO* , 3o Avoid spil spilla lag ge o out utsi side de th the e5 5+u +uip ipme men nt,a t,a) )d do! o!n n tthe he *ol) Bags to %ollect the spilled &aterial,# 3ransfer to the reactor 'i 'ire re h ha( a(ar ard d due due to SS ssco coop opss to a avo void id ssta tac c e ele lect ctri rici cit) t)$$ 3he 3he st sta acc elec electr tric icit it) ) re reac acto torr iiss ear earth thed ed b b) ) con condu duc cng ng !i !irres 2r 2rri rita tao on n to skin skin # 7sin 7sing g ha hand nd glo glove vess # go gogg ggle les$ s$ e)es Operaonall control - checkpoint shall be Operaona included in in tth he b ba atch ssh heet to to in indicate !hether !hether tthe he b boom oom valv valve e ha hass been been cclosed losed prior to charging Acetonitrile # is not eaking$ Acetonitrile addion pipe is kept to the to Boom oom of the the rea react ctor or *ipe *ipe li line ness are are al alll SS and and e e+u +uip ipme ment nt moto motors rs
Boom v va alve opened,, or eak opened eakage age of Boom "alve Acetonitrile 'i 'irre ha ha(ard du due e st sta acc e ele lect ctri rici cit) t)
n-bromo succinamide
are 0ame proof$ 2nstrucon is aid in the SO* , 3o Avoid Spillage Spill age o out ut side the spill spillage age o outsid utside e the 5 5+uipm +uipment, ent,a) a) do do!n !n the reactor, *ol) Bags to %ollect the spilled &aterial,# 3ransfer to the reactor 'i 'ire re h ha( a(ar ard d due due to SS ssco coop opss to a avo void id ssta tac c e ele lect ctri rici cit) t)$$ 3he 3he st sta acc elec electr tric icit it) ) re reac acto torr iiss ear earth thed ed b b) ) con condu duc cng ng !i !irres 2r 2rri rita tao on n to skin skin # 7sin 7sing g ha hand nd glo glove vess # go gogg ggle les$ s$ e)es
Boom v va alve opened, opened , or"eak eakage of Bo Boom al alv ve age 5th)l acetate
isllaon of the organic la)er
%)clohexane
%entrifuging
3o separate the li+uid
Operaonal control - checkpoint shall be Operaonal included in in tth he b ba atch ssh heet to to in indicate
!hether !heth ercha tthe hergin b boom oom valv valve e tat ha has be cclosed losed prio pr iorr to to charg ing g 5t 5th) h)l l ace aceta tse been # en is not no t eaking$ 5th)l acetate addion pipe is kept to the 'i 'irre h ha( a(ar ard dd due ue to Bo Bo om of the the rrea eact ctor or st sta acc e ele lect ctri rici cit) t) *ipe *ipe li line ness are are al alll SS and and e e+u +uip ipme ment nt moto motors rs are 0ame proof$ 3he temperature is raised b) slo! heang ll isllaon8 the Acetonitrile os osss of Acet Acetoni onitri trile le "apo apour ur o oss ss is d due ue to 5 5xc xcess essive ive h hea eat, t, 2nstrucon is 9iven in SO*, 3o Open the steam valve to Opmum so as to maintain the isllaon$ Operaonall control - checkpoint shall be Operaona Boom v va alve included in in tth he b ba atch ssh heet to to in indicate opened, or eak opened, eakage age !hether !hether tthe he b boom oom valv valve e ha hass been been cclosed losed of Bo Boom "al alv ve prio priorr to to cha charg rgin ing g% %)c )clo lohe hexxane ane # is is not not eaking$ %)clohexane %)clohex ane addion pipe is kept to the 'i 'irre h ha( a(ar ard dd due ue to Bo Bo om of the the rrea eact ctor or st sta acc e ele lect ctri rici cit) t) *ipe *ipe li line ness are are al alll SS and and e e+u +uip ipme ment nt moto motors rs are 0ame proof$ 3he centrifuge is earthed b) conducng 'ire ha(ard due to !ires$ stac electricit), 3he :ltraon is carried out through a operator ha(ard if centrifuge$ % %e entrifuges ar are high sp speed an) loading > machines and sources of ha(ard in a chemical unloading acvit) plant$ Ample precauons are taken to carr)
Solvent re recover)
%harging of & 6a(ardous !aste a a@ @er
carr carrie ied d out out in a running runnin g cent centrif rifug uge e
out out th the e ce cent ntri rifu fugi ging ng as as ha ha((ar ard d free free a ass pos possib sible$ le$ ; ;e e are are using using a 4< 4< inc inch h di dia a SS SS.1= .1=
?o ssp peci:c h ha a(ard
centrifuge, driven and machines top discharge$ this is a fourboom point suspension !hich are put on special vibra mount for smooth vibraon free noiseless operaon$ 3he speed is controlled b) a variable fre+uenc) drive and and the feeding of the centrifuge is done b) pneumacall) controlled valves at lo!er *& under nitrogen purging$ 5ven the bearing housing of the centrifuge is provided !ith a nitrogen purging facilit)$ An interlocking s)stem is provided for ensuring that the lids cannot be opened !hile the centrifuge is running and thereb) prevenng an) operaonal ha(ard b) human error $ All the limits s!itches and the safet) interlocking s!itches are 0ame proof including the "' controls$ All charging is done b) vacuum sucking to avoid ssp pillages and through the closed S SS S
?o spec speci: i:cc ha ha(a (ard rd
pipe lines$ "3 is :ed !ith 0ame proof motors$ 7nlo 7nload adin ing g iint nto o the the b bin inss b) b) act actua uatted v val alv ve,
disllaon r)i r)ing ng
Sepa Separraon aon o off sol solve vent ntss fro from m
r r)i )ing ng of th the ep pro rodu duct ct in in
operaon
the product
"3
Stage-
eacon of Stage C 2 material, !ith Acetone, *otassium carbonate and %harging Acetone 1,,4-3ria(ole then :ltrated
Boom valve opened, or eakage of Boom "alve
6ence ?o- ess 5xposure 6and gloves # goggles should be used$ Operaonall control - checkpoint shall be Operaona included in the batch sheet to indicate !hether the boom valve has been closed prior to charging charging Acetone # is not eaking$
and added 5th)l acetate and 6)drochloric acid
'ire ha(ard due st sta acc e ele lect ctri rici cit) t)
*otassium carbonate
1,,4-3ria(ole
'iltraon
Acetone addion pipe is kept to the Boom to of o f the reactor
*ipe *i pe0ame li line ness proof$ are are al alll SS and and e e+u +uip ipme ment nt moto motors rs are 2nstrucon is aid in the SO* , 3o Avoid Spillage Spill age o out ut side the spill spillage age o outsid utside e the 5 5+uipm +uipment, ent,a) a) do do!n !n the reactor, *ol) Bags to %ollect the spilled &aterial,# 3ransfer to the reactor 'i 'ire re h ha( a(ar ard d due due to SS ssco coop opss to a avo void id ssta tac c e ele lect ctri rici cit) t)$$ 3he 3he st sta acc elec electr tric icit it) ) re reac acto torr iiss ear earth thed ed b b) ) con condu duc cng ng !i !irres 2r 2rri rita tao on n to skin skin # 7sin 7sing g ha hand nd glo glove vess # go gogg ggle les$ s$ e)es 2nstrucon is aid in the SO* , 3o Avoid Spillage Spill age o out ut side the spill spillage age o outsid utside e the 5 5+uipm +uipment, ent,a) a) do do!n !n the reactor, *ol) Bags to %ollect the spilled &aterial,# 3ransfer to the reactor 'i 'ire re h ha( a(ar ard d due due to SS ssco coop opss to a avo void id ssta tac c e ele lect ctri rici cit) t)$$ 3he 3he st sta acc elec electr tric icit it) ) re reac acto torr iiss ear earth thed ed b b) ) con condu duc cng ng !i !irres 2r 2rri rita tao on n to skin skin # 7sin 7sing g ha hand nd glo glove vess # go gogg ggle les$ s$ e)es 3he 'iltraon Operaon Operaon is %arried out in Spillage, Spill age,'ilt 'ilter er %l %loth oth %lose %losed d SS ine, 'ilter 'ilter cl cloth oth cleane cleaned d fo forr 5ver) 5ver) Block Batch # this %leaning of the 'ilter along !ith %loth is 2ncorporated 2n the B* Acetone %harging %harging S SS S pipe is 'ixed to the 'i 'irre ha ha(ard du due e to Boom oom of the the rea react ctor or st sta acc e ele lect ctri rici cit) t) *ipe *ipe li line ness are are al alll SS and and e e+u +uip ipme ment nt moto motors rs are 0ame proof$
Boom v va alve opened, opened , or"eak eakage of Bo Boom al alv ve age 5th)l acetate
6)drochloric acid
isllaon of the organic la)er
%entrifuging
3o separate the li+uid
Operaonall control - checkpoint shall be Operaona included in in tth he b ba atch ssh heet to to in indicate
!hether !heth ercha tthe hergin b boom oom valv valve e tat ha has be cclosed losed prio pr iorr to to charg ing g 5t 5th) h)l l ace aceta tse been # en is not no t eaking$ 5th)l acetate addion pipe is kept to the 'i 'irre h ha( a(ar ard dd due ue to Bo Bo om of the the rrea eact ctor or st sta acc e ele lect ctri rici cit) t) *ipe *ipe li line ness are are al alll SS and and e e+u +uip ipme ment nt moto motors rs are 0ame proof$ Operaonall control - checkpoint shall be Operaona Boom v va alve included in in tth he b ba atch ssh heet to to in indicate opened,, or eak opened eakage age !hether !hether tthe he b boom oom valv valve e ha hass been been cclosed losed of B Bo oom " "a alve prior to to ch charging 6)drochloric acid # is not eaking$ 6)drochloric acid addion pipe is kept to the 'i 'irre h ha( a(ar ard dd due ue to Bo Bo om of the the rrea eact ctor or st sta acc e ele lect ctri rici cit) t) *ipe *ipe li line ness are are al alll SS and and e e+u +uip ipme ment nt moto motors rs are 0ame proof$ 3he temperature is raised b) slo! heang ll isllaon8 the Acetone and eth)l oss oss of Acet Aceton one e acet aceta ate "apou apourr os osss is is due due to 5xce 5xcess ssiv ive e and eth eth)l )l a acet cetat ate e hea heat, t, 2nst 2nstruc rucon on is 9iv 9iven en in S SO* O*,, 3o 3o O Open pen the steam valve to Opmum so as to maintain the isllaon$ 3he centrifuge is earthed b) conducng 'ire ha(ard due to !ires$ stac electricit), 3he :ltraon is carried out through a operator ha(ard if centrifuge$ % %e entrifuges ar are high sp speed an) loading > machines and sources of ha(ard in a chemical unloading acvit) plant$ Ample precauons are taken to carr)
r)i r)ing ng
Sepa Separraon aon o off sol solve vent ntss fro from m
r r)i )ing ng of th the ep pro rodu duct ct in in
operaon
the product
"3
Stage-.
eacon of stage C22 material, Sodium carbonate and 5th)l acetate ! !iith ! !a ater tth hen separated the la)er and added 5th)l acetate and c)clohexane c)clohexa ne tnen
carr carrie ied d out out in a runnin run ning g cent centrif rifug uge e
out out th the e ce cent ntri rifu fugi ging ng as as ha ha((ar ard d free free a ass pos possib sible$ le$ ; ;e e are are using using a 4< 4< inc inch h di dia a SS SS.1= .1=
?o spec speci: i:cc ha ha(a (ard rd
centrifuge, driven and machines top discharge$ this is a fourboom point suspension !hich are put on special vibra mount for smooth vibraon free noiseless operaon$ 3he speed is controlled b) a variable fre+uenc) drive and and the feeding of the centrifuge is done b) pneumacall) controlled valves at lo!er *& under nitrogen purging$ 5ven the bearing housing of the centrifuge is provided !ith a nitrogen purging facilit)$ An interlocking s)stem is provided for ensuring that the lids cannot be opened !hile the centrifuge is running and thereb) prevenng an) operaonal ha(ard b) human error $ All the limits s!itches and the safet) interlocking s!itches are 0ame proof including the "' controls$ "3 is :ed !ith 0ame proof motors$ 7nlo 7nload adin ing g iint nto o the the b bin inss b) b) act actua uatted v val alv ve,
Spillage o Spillage out ut side the reactor, Sodium cca arbonate 'ire ha(ard due to stac electricit)
6ence ?o- ess 5xposure 6and gloves # goggles should be used$ 2nstrucon is aid in the SO* , 3o Avoid spill spillage age o outsid utside e the 5 5+uipm +uipment, ent,a) a) do do!n !n the *ol) Bags to %ollect the spilled &aterial,# 3ransfer to the reactor SS scoops to avoid stac electricit)$ 3he reactor is earthed b) conducng !ires 7sing hand gloves # goggles$
centrifuge the reacon mass
2rritaon to skin e)es
#
Boom v va alve opened,, or eak opened eakage age of Boo Boom m "al alve ve 5th)l acetate 'ire ha(ard due st sta acc e ele lect ctri rici cit) t)
isllaon of the organic la)er
to
oss of 5th)l acetate
Boom v va alve opened, or eak opened, eakage age of Bo Boom "al alv ve %)clohexane 'ire ha(ard due st sta acc e ele lect ctri rici cit) t)
%entrifuging
3o separate the li+uid
'ire ha(ard due to stac electricit), opera ope rator tor ha( ha(ard ard if an) loading >
to
Operaonall control - checkpoint shall be Operaona included in in tth he b ba atch ssh heet to to in indicate !hether !hether tthe he b boom oom valv valve e ha hass been been cclosed losed prio priorr to char chargi ging ng 6)dro 6)droch chlo lori ricc acid acid # is not not eaking$ 6)drochloric acid addion pipe is kept to the Boom of the reactor *ipe *ipe li line ness are are al alll SS and and e e+u +uip ipme ment nt moto motors rs are 0ame proof$ 3he temperature is raised b) slo! heang ll isllaon8 th the 5th)l acetate " "a apour oss is due to 5xcessive heat, 2nstrucon is 9iven in SO*, 3o Open the steam valve to Opmum so as to maintain the islla isllaon$ on$ Operaonall control - checkpoint shall be Operaona included in in tth he b ba atch ssh heet to to in indicate !hether !hether tthe he b boom oom valv valve e ha hass been been cclosed losed prio priorr to to cha charg rgin ing g% %)c )clo lohe hexxane ane # is is not not eaking$ %)clohexane %)clohex ane addion pipe is kept to the Boom of the reactor *ipe *ipe li line ness are are al alll SS and and e e+u +uip ipme ment nt moto motors rs are 0ame proof$ 3he centrifuge is earthed b) conducng !ires$ 3he : :ltr ltra aon on is ccarr arried ied o out ut th throu rough gh a centrifuge$ %en %entrifuges ar are e hi hig gh spe speed
unloading acvit) carr carrie ied do out ut in a runnin run ning g cen centri trifug fuge e
Solvent re recover)
%harging of & 6a(ardous !aste a a@ @er disllaon
?o ssp peci:c h ha a(ard
r)i r)ing ng
Sepa Separraon aon o off sol solve vent ntss fro from m
r r)i )ing ng of th the ep pro rodu duct ct in in
?o spec speci: i:cc ha ha(a (ard rd
operaon
the product
"3
machines and sources of ha(ard in a chemical
pl plan ant$ t$ Am Ampl ple ep pre reca cau uon onss are are tak taken to carr carr) ) out tthe he ce centr ntrifu ifugin ging g as h ha( a(ard ard dia ffree ree as possible$ ;e are using a 4< inch SS.1= centrifuge, boom driven and top discharge$ this is a four point suspension machines !hich are put on special vibra mount for smooth vibraon free noiseless operaon$ 3he speed is controlled b) a variable fre+uenc) drive and and the feeding of the centrifuge is done b) pneumacall) controlled valves at lo!er *& under nitrogen purging$ 5ven the bearing housing of the centrifuge is provided !ith a nitrogen purging facilit)$ An interlocking s)stem is provided for ensuring that the lids cannot be opened !hile the centrifuge is running and thereb) prevenng an) operaonal ha(ard b) human error $ All the limits s!itches and the safet) interlocking s!itches are 0ame proof including the "' controls$ All charging is done b) vacuum sucking to avoid ssp pillages and through the closed S SS S pipe lines$ "3 is :ed !ith 0ame proof motors$ 7nlo 7nload adin ing g iint nto o the the b bin inss b) b) act actua uatted v val alv ve, 6ence ?o- ess 5xposure 6and gloves # goggles should be used$
To manufacture of 'endamu#n Hazop Study - Proce ! for Bendamusn Sta"e
Proce
Opera#on
Po$ble Hazard % fa$lure
Stage 2
eacon of 5th)l-4-/bi bis s-h h)dro drox) eth th)l )l amino-1-meth)l-16ben(oid imida(ol-)l )lb but utan anoa oate te in pres presen ence ce of thion)l chloride$
Addion of 5th)l-4-/bis bis-h h)dr dro ox) eth eth)l amino-1-meth)l-16ben(oid imida(ol-)lb )lbut utan anoa oate te
2nstrucon is aid in the SO* , 3o Avoid spil spilla lag ge outs outsiide the the 5+u +uip ipme men nt,a ,a) do do! !n the *ol) Bags to %ollect the spilled &aterial,# 3ransfer to the reactor 'ire ha(ard due due to SS ssco coop opss to a avo void id ssta tac c e ele lect ctri rici cit) t)$$ 3he 3he stac e ellectricit) reactor is is ea earthed b) cco onducng ! !iires 2rritaon 2rrit aon to sk skin in # e e)es )es 7sing hand g glove lovess # goggles goggles$$
ineg of 3hion)l c%hhlaorrgid
Boom valve opened, or eak eakag age e of Bo Boom om "alve
Spil pillag lage out out si sid de the the reactor,
'ire ha(ard du due e stac e ele lect ctri rici citt)
%entrifuging
3o separate the 2st St Stag age e' 'ro rom m th the e li+u li+uid id
&emed$al Ac#on
to
'ire ha(ard due due to electricit), stac operator ha(ard if an) load loadin ing g > unlo unload adin ing g acvit) acv it) carried carried out in a runn runnin ing g ccen entr trif ifug uge e
O d oninalth coenbta rotcl h- csh atllebe inpcleurdae heecektpto oin intdsih ca !he !hethe therr th the e bo boo om m va valve lve has bee been n close closed d prior to charging thion)l chloride # is not eaking$ 3hion)l chloride addion pipe is kept to th the eB Bo oom om of the the rrea eact ctor or *ip ipe e li lin nes are al alll SS and e+ e+u uip ipm ment ent mo motors ors are 0ame proof$ 3he centrifuge is earthed b) conducng !ires$ 3he 3he : :lt ltra rao on n iiss car carri ried ed out out thr throu ough gh a centrifuge$ %entrifuges are high speed machines and sources of ha(ard in a chem chemic ical al pl plan ant$ t$ Am Ampl ple ep prrec ecau auo ons ns ar are e tak taken en to carr) out th the e cen centrifu trifuging ging as ha(a ha(ard rd fr free ee a ass pos possi sibl ble$ e$ ; ;e ea arre usin using ga4 4< < inch dia SS.1= centrifuge, boom driven and top discharge$ this is a four point
suspension machines !hich are put on special vibra mount for smooth vibraon free noiseless 3he speeddrive is controlled b) aoperaon$ variable fre+uenc) and the feeding of the centrifuge is done b) pneumacall) controlled valves at lo!er *& under nitrogen purging$ 5ven the bearing housing of the centrifuge is provided !ith a nitrogen purging facilit)$ An interlocking s)stem is provided for ensuring that the lids cannot be opened !hile the centrifuge is running and thereb) prevenng an) operaonal ha(ard b) human error error$$ All the limits s!itches and the safet) interlocking s!itches are 0ame proof including the "' controls$ Solvent re recover) isllaon
%harging of & 6a(ardous !a !aste a a@ @er disllaon
?o ssp peci:c ha(ard
All charging is done b b) ) va vacuum ssu ucking to avoid spillages and through the closed SS pipe lines$
To manufacture b$calutam$de
Hazop Study - Proce ! for Proce
Opera#on
eac eacon on of 1D 1D ? ?-E -E44c)an c)anoo-..-ttri0 ri0uor uorome ometh)l th)l phen)lF-.-E4-0uorophen)l thi thioFoF--h -h)d )dro rox) x)--m --meth eth)l )l propanamide and *otas otassi sium um per perma mang ngan anat ate e in A Accetonitrile$
%har %harg ging of 1 1D D ?-E4-E4-c) c)an ano o-. -.-tri0uorometh)l phe phen) n)lFlF-.-E .-E440uorophen)l th thio ioFF-h)drox)-meth)l propanamide %har %harg ging of *otassium perman per manga ganat nate e
%har %harg ging of Acetonitrile
Po$ble Hazard % fa$lure Spil Spilllag age eo out ut side ide the the react eactor or,, 'ire ha(a ha(ard rd due to stac elect lectrricit icit) ) 2rr 2rrita itaon on to skin skin # e)es
Bo oom om valve lve opened, or ea eakag kage e of Bo Boom om "alve 'ire ha(a ha(ard rd du due e to st sta acc electr electrici icit) t) Bo oom om valve lve opened, or eakage eak age of Boom Boom "alve 'ire ha(ar ha(ard d due to st sta acc elect electric ricit) it)
B2%A73A&25
&emed$al Ac#on 2n 2nsstru ruc con on is ai aid d iin n tthe he SO* , 3o Av Avoid oid ssp pil illa lag ge o out utsi side de the the 5+uipm uipmen ent, t, a) a) do do!n !n the the *ol) ol) Bags to %oll ollec ectt the spi pill lled ed &aterial,# 3ransfer to the reactor SS scoops scoops tto o av avoid oid ssta tacc elec electrici tricit) t)$$ 3he reactor reactor is ea earthed rthed b) cond conduc uc ng !ir ires es 7sing 7sing h hand and gl glov oves es # gogg goggles les$$
Oper peraona onal con control trol - ch che eckp ckpoin oint sha halll be inclu nclud ded in the the bat batch sheet to indicate !hether the boom valve has been closed prior to cchar hargi ging ng *ota *otassi ssium um p perm ermang angana anate te # is n not ot eak eaking ing$$ *otassiu *otassium m per permang manganat anate e addi addion on pi pipe pe is kep keptt to the B Boom oom of the rea react ctor or$$ *i *ipe pe lline iness are are al alll SS and e+u e+uipm ipment ent mot motor orss ar are e 0a 0ame me proof$ Oper peraona onal con control trol - ch che eckp ckpoin oint sha halll be inclu nclud ded in the the bat batch sheet to indicate !hether the boom valve has been closed prior to char charging ging Acet Acetonitri onitrile le # iiss not not eaking eaking$$ Acet Acetonitr onitrile ile ad addion dion pipe pipe is k kept ept tto o the Bo Boom om of tthe he rea reactor ctor$$ *ip *ipe e lines lines ar are e al alll SS SS and and e e+ui +uipme pment nt mot motors ors ar are e 0a 0ame me pro proof of$$
'iltraon
Spillage, %lot %loth hB Blo lock ck
'ilter 3he 'iltraon Operaon is %arried out in %losed SS ine, 'ilter cloth clea cleane ned d ffor or 5ver) ver) Ba Batc tch h # this this %lea %leani ning ng of th the e' 'il ilte terr alo along ng !i !ith th %loth is 2ncorporated 2n the B*
Sta"e
Proce
%entrifuging
Sol olv vent ent reco ecover) er)
Hazop Study - Proce ! for 'I(AL)TA*I+, Opera#on Po$ble Hazard % &emed$al Ac#on fa$lure 'ire ha(a ha(ard rd due tto o Acetone Acetone %ha %hargin rging g SS pipe pipe is ' 'ixe ixed d to the Boo Boom m of the rreact eactor or st sta acc electr electrici icit) t) *ip *ipe e li lines nes are all SS a and nd e+ e+uip uipmen mentt mo motor torss ar are e 0a 0ame me p proo rooff$ 3o separate the bi bica calu luta tami mide de fr from om the the li+ li+uid uid
is islla llaon of Acetonitrile and hexane
'ire ha(ard due to st sta acc elec electr tric icit it) ), ope opera rator tor ha( ha(ar ard d if an) an) load loadin ing g > unloading unloa ding acvit) acvit) carried out in a running runni ng cen centrifug trifuge e
?o spe peci ci: :c ha( ha(ard ard
3he centrifuge is earthed b) conducng !ires$ 3he 3he : :lt ltra rao on n is carr carrie ied do out ut th thro roug ugh h a ccen entr trif ifug uge$ e$ % %en entr trif ifug uges es ar are e hig high h speed speed ma machi chines nes and and so sourc urces es of h ha( a(ard ard iin n a ch chemi emical cal pla plant$ nt$ Am Ampl ple e pr precau ecauo ons ns ar are e tak taken en to carr carr) )o out ut the the ccen entr trif ifug ugin ing ga ass ha(a ha(ard rd free free as possi possible$ ble$ ; ;e e are using a 4< inch d dia ia SS SS.1= .1= centri centrifug fuge, e, bo boom om d driv riven en a and nd top top d disc ischar harge$ ge$ 3hi 3hiss is is a four four point point suspe suspension nsion m machin achines es !hich !hich are put on sspecia peciall vibra vibra mount for for smooth vibraon free noiseless operaon$ 3he speed is controlled b) a variable fre+uenc) drive and the feeding of the centrifuge is done b) pneumacall) controlled valves at lo!er *& under nitrogen purging$ 5ven 5ven the bearing housing of the centrifuge is provided !ith a nitrogen purging facilit) facilit)$$ An interlocking s)st s)stem em is provided for ensuring that the lids cannot be opened !hile the centrifuge is running and thereb) prevenng an) operaonal ha(ard b) human error$ All the limits s!itches and the safet) interlocking s!itches are 0ame proof including the "' controls$ All cha chargin ing g is done done b) vacu cuum um suck uckin ing g to avoid oid spi spill lla ages and through the closed SS pipe lines$
into mass r)i r)ing ng operaon
Sepa Separa rao on n of so solv lven ents ts from the product
reacon
r r)i )ing ng of product "acuum r)er
the the ?o spec speci: i:cc ha( ha(ar ard d in tra)
"3 "3 is :ed :ed !i !ith th 0ame 0ame proo prooff mo mottors$ ors$ 7nlo 7nload adin ing g in into to th the e bi bins ns b) actuated valve, 6ence ?o- ess 5xposure 6and gloves # goggles should be used$
To manufacture 'or#zom$b
Sta"e
Proce
Stage 2
eacon of .- phen)l -Ep)ra(ine-carbon)l-aminoF propionic acid !ith Borolex-G-pinanediol tri0uoro acec acid
Hazop Study - Proce ! for 'or#zom$b Po$ble Hazard % fa$lure Addion of eacon of .phen)l -- -Ep)ra(ine-Spillage ou out ssiide tth he carbon)l-aminoF reactor, propionic acid 'ire 'ire ha(ar ha(ard d due tto o sta stac c electricit) 2r 2rri rita tao on n to skin skin # e) e)es es %harging of &% Boom Bo om valve valve ope opened ned,, or eakag ea kage e of Bo Boo om m "a "alv lve e Opera#on
'i 'ire re ha(a ha(ard rd due due tto o sta stac c electricit) 6)drox) ssu uccinamide
Spillage ou out si side tth he reactor,
&emed$al Ac#on 2nstrucon is aid in the SO* , 3o Avoid spillage o ou utside tth he 5 5+ +uipment, a a) d do o!n tth he *ol) Bags to %ollect the spilled &aterial,# 3ransfer to the reactor SS sc scoop oopss to av avoid oid ssta tac c el elect ectric ricit) it)$$ 3he reactor is earthed b) conducng !ires 7sin 7sing gh han and d gl glov oves es # gogg goggle les$ s$ Operaonal control - checkpoint shall be inc includ luded ed in the bat batch ch sheet to indic indicat ate e !he !hethe therr the b bo oom om va valv lve e has b been een cclos losed ed prior to charging &% # is not eaking$ &% addion pipe is kept to the Boom of th the e rrea eact ctor or *ipe lines are all SS and e+uipment motors are 0ame proof$ 2n 2nsstrucon iiss a aid in in tth he S SO O* , 3o Av Avoid spillage outside the 5+uipment, a) do!n the
*ol) Bags to %ollect the spilled &aterial,# 3ransfer to the reactor 'ire 'ire ha(ar ha(ard d due tto o sta stac c electricit) 2r 2rri rita tao on n to skin skin # e) e)es es 'iltraon
Solvent recover)
%harging of & 6a(ardous !aste
Spillage 'ilter %loth Block
a@er ?o speci:c ha(ard
Stage 22
Addion of stage 2 product
Spillage, 'ilter %loth Block
lines$ 3he 'iltraon Operaon Operaon is %arried out in %losed SS ine, 'ilter cloth cleaned for 5ver)
Spillage out side the reactor,
Batch # this %leaning of the 'ilter along !ith %loth is 2ncorporated 2n the B* 2nstrucon is aid in the SO* , 3o Avoid spillage outside the 5+uipment, a) do!n the *ol) Bags to %ollect the spilled &aterial,#
'ire 'ire ha(ar ha(ard d due tto o sta stac c electricit) 2r 2rri rita tao on n to skin skin # e) e)es es 6%l Addion
All charging is done b) vacuum sucking to avoid spillages and through the closed SS pipe
disllaon 'iltraon
SS sc scoop oopss to av avoid oid ssta tac c el elect ectric ricit) it)$$ 3he reactor is earthed b) conducng !ires 7sin 7sing gh han and d gl glov oves es # gogg goggle les$ s$ 3he 'iltraon Operaon Operaon is %arried out in %losed SS ine, 'ilter cloth cleaned for 5ver) Batch # this %leaning of the 'ilter along !ith %loth is 2ncorporated 2n the B*
6)drochoric acid Spillage # 2rritaon
3ransfer reactor SS sc scoop oopsstotothe av avoid oid ssta tac c el elect ectric ricit) it)$$ 3he reactor is earthed b) conducng !ires 7sin 7sing gh han and d gl glov oves es # gogg goggle les$ s$ 3he Addion of 6)drochloric acid is charged through th the % %llosed lliines, !i !ithout an an) Spillage, personnel *rotecve 5+uipments are 7sed to avoid the 5xposure # tackle the irritaon
%harging of ?-6eptane Boom Bo om valve valve ope opened ned,, or eakag ea kage e of Bo Boo om m "a "alv lve e 'ire 'ire ha(a ha(ard rd due due tto o sta stac c electricit)
Saturated sodium bicarbonate
Solvent recover)
%harging of & 6a(ardous ! as aste a @e @er
Operaonal control - checkpoint shall be inc includ luded ed in the bat batch ch sheet to indic indicat ate e !he !hethe therr the b bo oom om va valv lve e has b been een cclos losed ed prior to charging n-heptane # is not eaking$ n-heptane addion pipe is kept to the Boom of th the e rrea eact ctor or *ipe lines are all SS and e+uipment motors are 0ame proof$
'ire 'ire ha(ar ha(ard d due tto o sta stac c electricit) 2r 2rri rita tao on n to skin skin # e) e)es es
2nstrucon is aid in the SO* , 3o Avoid spillage outside the 5+uipment, a) do!n the *ol) Bags to %ollect the spilled &aterial,# 3ransfer to the reactor SS sc scoop oopss to av avoid oid ssta tac c el elect ectric ricit) it)$$ 3he reactor is earthed b) conducng !ires 7sin 7sing gh han and d gl glov oves es # gogg goggle les$ s$
?o speci:c ha(ard
All charging is done b) vacuum sucking to
Spillage out side the reactor,
disllaon
avoid spillages and through the closed SS pipe
%harging 5th)l acetate Boom Bo om valve valve ope opened ned,, or eakage of Boom "alve
'ire 'ire h ha( a(ar ard d du due e tto o sta stac c electricit)
lines$ Operaonal control - checkpoint shall be inc includ luded ed in the bat batch ch sheet to indic indicat ate e !hether the boom valve has been closed prior to charging eth)l acetate # is not eaking$ 5th)l acetate addion pipe is kept to the Boo Boom m of tthe he rrea eact ctor or *ipe lines are all SS and e+uipment motors are 0ame proof$
%harging methanol Boom Bo om valve valve ope opened ned,, or eakag ea kage e of Bo Boo om m "a "alv lve e 'ire 'ire ha(a ha(ard rd due due tto o sta stac c electricit)
'iltraon
Solvent recover)
Spillage, 'ilter %loth Block
Operaonal control - checkpoint shall be inc includ luded ed in the bat batch ch sheet to indic indicat ate e !he !hethe therr the b bo oom om va valv lve e has b been een cclos losed ed prior to charging methanol # is not eaking$ ðanol addion pipe is kept to the Boom of th the e rrea eact ctor or *ipe lines are all SS and e+uipment motors are 0ame proof$
3he 'iltraon Opera on is %arried in %losed SS ine,Operaon 'ilter cloth cleanedout for 5ver) Batch # this %leaning of the 'ilter along !ith %loth is 2ncorporated 2n the B*
%harging of & 6a(ardous !aste a@er ?o speci:c ha(ard
All charging is done b) vacuum sucking to
disllaon
avoid spillages and through the closed SS pipe
Stage 222 Boom Bo om valve valve ope opened ned,, or eakage eakag e of Bo Boo om m "a "alv lve e %harging of methanol 'ire 'ire ha(a ha(ard rd due due tto o sta stac c electricit) Addion product
of stage 22 Spillage out side the reactor,
lines$ Operaonal control - checkpoint shall be inc includ luded ed in the bat batch ch sheet to indic indicat ate e !he !hethe therr the b bo oom om va valv lve e has b been een cclos losed ed prior to charging methanol # is not eaking$ methanol addion pipe is kept to the Boom of th the e rrea eact ctor or *ipe lines are all SS and e+uipment motors are 0ame proof$ 2nstrucon is aid in the SO* , 3o Avoid spillage outside the 5+uipment, a) do!n the
*ol) Bags to %ollect the spilled &aterial,# 3ransfer to the reactor 'ire 'ire ha(ar ha(ard d due tto o sta stac c electricit) 2r 2rri rita tao on n to skin skin # e) e)es es
Solvent recover)
'iltraon
Spillage, 'ilter %loth Block
%harging & 6 a(ardouof s ! as aste a @e @er
?o speci:c ha(ard
All charging is done b) vacuum sucking to
?o sspe pecci: i:cc ha ha(ard
avoid spillages and through the closed SS pipe lines$ %" is :ed !ith 0ame proof motors$ 7nlo 7nloa adi ding ng in intto tthe he bin inss b) b) a act ctua uatted valv lve, e,
disllaon
r)ing
operaon
SS sc scoop oopss to av avoid oid ssta tac c el elect ectric ricit) it)$$ 3he reactor is earthed b) conducng !ires 7sin 7sing gh han and d gl glov oves es # gogg goggle les$ s$ 3he 'iltraon Operaon Operaon is %arried out in %losed SS ine, 'ilter cloth cleaned for 5ver) Batch # this %leaning of the 'ilter along !ith %loth is 2ncorporated 2n the B*
Sepa eparaon of so solven lventts
r)ing )ing of the the p prroduc oductt iin n
from the product
otocone vacuum r)er
6ence ?o- ess 5xposure 6and gloves # goggles should be used$
To manufacture of (apec$tab$ne
Sta"e
Proce
eacon of /-meth)l tetrah)drofuran-,.,4tri)ltriacetate, /-'luoroc)tosine, Stannic chloride, 3&S%, 6&S and Sodium bicarbonate into &% Stag Stage e --1 1 and and ttol olue uene ne$$
Hazop Haz op S Stud tudy y-P Proc roce e ! ffor or (AP (AP,(I ,(IT TA'IN, A'IN, Opera#on Po$ble Hazard % fa$lure &emed$al Ac#on 2nstrucon is aid in the SO* , 3o Avoid spillag spillage e outside %harging / /-Spillage o ou ut ssiide tth he the 5+uipment, a) do!n the *ol) Bags to %ollect the reactor, meth)l spilled &aterial,# 3ransfer to the reactor tetrah)drofuran- 'i 'irre ha( ha(ard ard due tto o stac SS scoop coopss to avoi oid d sta tac el ele ectri ctrici cit) t)$$ 3he rea eact ctor or is ,.,4electricit) earthed b) conducng !ires tri)ltriacetate 2r 2rri rittaon to sski kin n # e) e)es 7si sing ng hand hand glov loves # gog gogg gle les$ s$ 2nstrucon is aid in the SO* , 3o Avoid spillag spillage e outside Spillage out side the the 5+uipment, a) do!n the *ol) Bags to %ollect the %harging of /reactor, spilled &aterial,# 3ransfer to the reactor 'luoroc)tosine 'i 'irre ha ha((ard ard due due to stac SS scoop coopss to avoid oid sta tac el ele ectri ctrici cit) t)$$ 3he rea eact ctor or is electricit) earthed b) conducng !ires 2r 2rri rita tao on n tto o sski kin n # e) e)es es$$ 7sin 7sing gh han and dg glo love vess # gogg oggle les$ s$ 2nstrucon is aid in the SO* , 3o Avoid spillag spillage e outside Spillage out side the the 5+uipment, a) do!n the *ol) Bags to %ollect the reactor, %harging of spilled &aterial,# 3ransfer to the reactor 3&S% 'i 'irre ha ha((ard ard due due to stac SS scoop coopss to avoid oid sta tac el ele ectri ctrici cit) t)$$ 3he rea eact ctor or is electricit) earthed b) conducng !ires 2r 2rri rita tao on n tto o sski kin n # e) e)es es$$ Spillage out side the %harging of 6&S
reactor, 'i 'irre ha ha((ard ard due due to stac electricit) 2r 2rri rita tao on n tto o sski kin n # e) e)es es$$
7sin 7sing gh han and dg glo love vess # gogg oggle les$ s$ 2nstrucon is aid in the SO* , 3o Avoid spillag spillage e outside the 5+uipment, a) do!n the *ol) Bags to %ollect the spilled &aterial,# 3ransfer to the reactor SS scoop coopss to avoid oid sta tac el ele ectri ctrici cit) t)$$ 3he rea eact ctor or is earthed b) conducng !ires 7sin 7sing gh han and dg glo love vess # gogg oggle les$ s$
%harging o off Stannic chloride
%harging of &%
%harging of toluene
Boo Boom mv val alve ve opened, or or eak eakag age e of Boo Boom m "alve 'ire ha(ard due to st sta acc elect electric ricit) it) Boo Boom mv val alve ve open op ened ed,, or or eakage of Boom "alve 'ire ha(a ha(ard rd due tto o st sta acc elect electri rici cit) t) Boo Boom mv val alve ve open op ened ed,, or or eakage of Boom "alve 'ire ha(a ha(ard rd due tto o st sta acc elect electric ricit) it) Spillage, 'ilter %loth Block
'iltraon
'ire ha(ard due to stac electricit)
Solvent recover)
is islla llaon &% 3oluene
of oss oss of and acetate acetonitrile
Op Oper era aon onal al cont contro roll - che check ckpo poin intt sh shal alll be in incl clud uded ed in th the eb bat atch ch sheet to to in indicate ! !h hether th the b bo oom v va alve h ha as be been ccllosed p prrior to char chargi ging ng Stan Stanni nicc chlo chlori ride de # iiss not not eak eakin ing$ g$ Stannic chloride add ion pipe is kept to the Boom of the reactor$ reactor$
*ip *ipe e li lines nes ar are e al alll SS SS and and e e+ui +uipme pment nt mot motors ors are 0ame 0ame p proo rooff$ Op Oper era aon onal al cont contro roll - che check ckpo poin intt sh shal alll be in incl clud uded ed in th the eb bat atch ch shee sheett to to in indi dica catte ! !h het ethe herr the the bo boom valv lve e has has be been en cl clos osed ed pri rior or to charging &% # is not eaking$ &% addio addion n pipe iiss kep keptt to th the e Bo Boom om of th the e reac reactor tor$$ *ipe llines ines ar are e al alll SS a and nd e+ e+ui uipm pmen entt mo moto tors rs a are re 0 0am ame e pr proo ooff$ Op Oper era aon onal al cont contro roll - che check ckpo poin intt sh shal alll be in incl clud uded ed in th the eb bat atch ch shee sheett to to in indi dica catte ! !h het ethe herr the the bo boom valv lve e has has be been en cl clos osed ed pri rior or to charging toluene # is not eaking$ toluene toluene add addion ion p pipe ipe is k kept ept tto o the Bo Boom om of the re reactor actor$ *ipe lin lines es ar are e al alll SS SS and and e e+ui +uipme pment nt mot motors ors ar are e0 0ame ame pro proof of$$ 3he 'iltraon Operaon is %arried out in %losed SS ine, 'ilter cloth cleaned for 5ver) Batch # this %leaning of the 'ilter along !ith %loth is 2ncorporated 2n the B* 3ri meth)lamine and Sodium bicarbonate %harging SS pipe is 'ixed to the Boom of the reactor reactor$$ *ipe lines are all SS and e+uipment motors are 0ame proof$
eth eth)l 3he tem empe perratur ure e is rai aissed b) slo! lo! hea heang ll re0ux ux88 the met etha hano noll and "apour oss is due to 5xcessive heat, 2nstrucon is 9iven in SO*, 3o Open the steam valve to Opmum so as to maintain the re0ux
Boo Boom mv val alve ve opened, or
%harge 2*A into reacon mass$
r)ing operaon
Stage-22
%harging of 2* 2*A A
%entrifuging
3o separat separate e the ocet ocetax axel el 3rih) 3rih)dra drate te sta stage-2 ge-222 from from the li+uid li+uid
Solvent
%harging of &Hs 6a(ard ou ous !aste
recover)
a@er centrifuging
Separaon
eakage of Boom "alve 'ire ha(ard due to
to charging
stac electricit)
are all SS and e+uipment motors are 0ame proof$
2*A # is not eaking$
2*A addion pipe is kept to the Boom of the reactor$ *ipe lines
3he centrifuge is earthed b) conducng !ires$ 3he :ltraon is carried out through a centrifuge$ %entrifuges are high speed machines and sources of ha(ard in a chemical plant$ Ample precauons are taken to carr) out the centrifuging as ha(ard free as possible$ ;e are using a 4< 'ire 'ire ha( ha(ar ard d due to inc inch h di dia a SS.1 SS.1= = ccent entrif rifuge uge,, bo boo om md driv riven en and top top di disc schar harge ge$$ 3his 3his is a ffour our point point stac electricit), suspension machines !hich are put on special vibra mount for smooth vibraon oper operato atorr ha( ha(ar ard d if an) an) free free noise noiseles lesss op oper erao aon$ n$ 3he sp speed eed is co contr ntroll olled ed b) a va varia riable ble fre+u fre+uenc enc) ) drive drive load loading ing > unloading and the feeding of the centrifuge is done b) pneumacall) controlled valves at acvit) ccarried arried out out in a lo!er *& *& under nitrogen purging$ 5ven 5ven the bearing housing housing of the centrif centrifuge uge runnin running g cen centri trifug fuge e is pr prov ovide ided d !ith a nitro nitroge gen n purging purging fac facili ilit) t)$$ An interl interloc ockin king g s) s)st stem em is prov provide ided d for ensuring that the lids cannot be opened !hile the centrifuge is running and thereb) prevenng an) operaonal ha(ard b) human error$ All the limits s!itches and the safet) interlocking s!itches are 0ame proof including the "' controls$ ?o speci:c ha(ard All charging is done b) vacuum sucking to avoid spillages and through the closed
of r)ing of of th the p prroduct iin nv va acuum
solvents from tra) dr)er the product
?o speci:c ha(ard
%harge
Boom valve opened,
capecitabine stage-2, *)riddine and npent)l
or eakage of Boom %harging of * *) )riddine
Op Oper era aon onal al cont contro roll - che check ckpo poin intt sh shal alll be in incl clud uded ed in th the eb bat atch ch sheet to indicate !hether the boom valve has been closed prior
"alve
'ire ha(ard due stac electricit)
SS pipe lines$ "3 is :ed !ith 0ame proof motors$ 7nloading into the bins b) actuated valve, 6ence ?o- ess 5xposure 6and gloves # goggles should be used$ Operaonal Operaon al control - checkpoint shall be included in the batch sheet to indicate !hetherr the boo !hethe boom m val valve ve has has been been close closed d prior prior to char chargin ging g *)r *)ridd iddine ine # is is not eaking$
to *)riddine addion pipe is kept to the Boom of the reactor$ *ipe lines are all SS and e+uipment motors are 0ame proof$
chloroformate into &%$
Boom valve opened, %harging of n-pent)l
or eakage of Boom "alve
chloroformate
'ire ha(ard due st sta acc ele elect ctri rici cit) t)
Boom valve opened, %har hargin ing g of & & %
or eakage of Boom "alve lve 'ire ha(ard due stac electricit)
Operaonal Operaon al control - checkpoint shall be included in the batch sheet to indicate !hether the boom valve has been closed prior to charging n-pent)l chloroformate # is not eaking$
to ?-pe ?-pent)l nt)l chlorof chloroforma ormate te addion addion p pipe ipe is k kept ept to tthe he Boo Boom m of of th the e react reactor or$$ *ipe *ipe line liness a are re all all SS SS a and nd e+ e+uip uipme ment nt moto motors rs ar are e 0am 0ame ep pro roof of$$
Operaonal control - checkpoint shall be included in the batch sheet to indicate !het !hethe herr the the boo boom m va valv lve e has has be been en clo close sed d prio priorr to cha charg rging ing & &% % # is no nott eaking$ to &% addion pipe is kept to the Boom of the reactor$ *ipe lines are all SS and e+uipment motors are 0ame proof$
'il ilte terr %lo loth th 3he 'iltraon Operaon is %arried out in %losed SS ine, 'ilter cloth cleaned for 5ver) Batch # this %leaning of the 'ilter along !ith %loth is 2ncorporated 2n the Block B* 'ir 'ire e ha( ha(ar ard d due to *)r *)ridi idine ne %harg %harging ing SS pip pipe e is 'ixed 'ixed to the Boo Boom mo off tthe he reacto reactorr$ * *ipe ipe lines lines ar are e sta tac c elec electr tric icit it) ) all all SS SS a and nd e+ e+ui uipm pmen entt mot motor orss a are re 0ame 0ame pr proo ooff$ Operaonal control - checkpoint shall be included in the batch sheet to indicate Boom valve opened, !h !het ethe herr the the bo boo om mv val alve ve ha hass b bee een n cclo lose sed d prio priorr tto o cha charg rgin ing g 6e 6ept ptan ane e# or eakage of Boom is not eaking$ "alve Spill pilla age,
'iltraon
%har %harge ge 6ept 6eptan ane e la)er
into in to or orga gani nicc
%har %hargi ging ng o of f 6eptane
'ire ha(ard due stac electricit)$
Solvent recover)
isllaon of &%
%entrifuging
3o separate %apecitabine stage-22 from li+uid
the the
to 6eptane addion pipe is kept to the Boom of the reactor$ *ipe lines are all SS and e+uipment motors are 0ame proof$
3he temperature is raised b) slo! heang ll re0ux8 the methanol "apour oss is due to 5xcessive heat, 2n 2nstrucon is 9iven iin n SO*, 3o Open the steam valve to Opmum so as to maintain the re0ux 3he centrifuge is earthed b) conducng !ires$ 'ir 'ire e ha( ha(ar ard d due to 3he :ltra :ltraon on is ccarr arried ied out thr throug ough h a ce centr ntrifu ifuge ge$$ %en %entri trifug fuges es ar are e high high spe speed ed machines and sources of ha(ard in a chemical plant$ Ample precauons are stac electricit), taken to carr) out the centrifuging as ha(ard free as possible$ ;e are using a 4< operator ha(ard if an) inch dia SS.1= centrifuge, boom driven and top discharge$ 3his is a four point loading > unloading suspension machines !hich are put on special vibra mount for smooth vibraon acvit) carried out in a free noiseless operaon$ 3he speed is controlled b) a variable fre+uenc) drive running centrifuge and the feeding of the centrifuge is done b) pneumacall) controlled valves at lo!er *& under nitrogen purging$ 5ven the bearing housing of t he centrifuge oss of &%
is provided !ith a nitrogen purging facilit)$ An interlocking s)stem is provided for ensuring that the lids cannot be opened !hile the centrifuge is running and thereb) prevenng an) operaonal ha(ard b) human error$ All the limits s!itches and the safet) interlocking s!itches are 0ame proof including the "' controls$
%harging of of Solvent recover) r r)i )ing ng oper perao on n
&Hs
Sepa Separa rao on n of of sol solve vent ntss fro from m tthe he
r)ing of the
pr pro oduc duct
product in "acuum tra) dr)er
%harging o off & &%
%harge
capecitabine stage-22,
&%, &%, so sodi dium um h)dr h)dro oxi xide de and %har %hargi ging ng of h)drochloric acid into methanol methanol$
Stage-222
6%l Addion
Solvent recover) %harge toluene
mass
All charging is done b) vacuum sucking to avoid spillages and through the closed
6a(ardous !aste ?o speci:c ha(ard a@er centrifuging
into reacon
SS pipe lines$
?o speci:c ha(ard
"3 is :ed !ith 0ame proof motors$ 7nloading into the bins b) actuated valve, 6ence ?o- ess 5xposure 6and gloves # goggles should be used$
Boom valve opened, or eakage of Boom "alve
Operaonal Operaon alecontrol checkpoint shall beed included incha therging batch to indicate !he !hethe therr th the b bo oom om- va valve lve has bee been n cclos losed prior prior to charg ing sheet&% & % # is no nott eaking$
'ire 'ire ha ha(a (ard rd du due e to stac elec lectr tric icit it) ) Boom valve opened, or eakage of Boom "alve
&% &% addi addion on pipe pipe is ke kept pt to the the Bo Boom om o off the re react actor or$$ *i *ipe pe lines lines ar are e all SS a and nd e+u +uiipme pment mo motor tors a arre 0 0a ame pro proof$ Operaonal Operaon al control - checkpoint shall be included in the batch sheet to indicate !h !het ethe herr tthe he bo boo om m val valve ve ha hass b bee een n cclo lose sed dp pri rior or to ch char argi ging ng metha methano noll # is not eaking$
'ire 'ire ha ha(a (ard rd du due e to sta tac c elec electr tric icit it) )
ða ðanol nol addi addio on n pip pipe e is kept kept to to the Bo Boom om of of the reacto reactorr$ *ipe *ipe lines lines a are re a all ll SS an and d e+ e+ui uipm pmen entt m mot otor orss ar are e0 0am ame e pr proo ooff$
6)drochoric acid a 3he n) SAddion pillage, pof er6)drochloric sonnel *rotecacid ve is 5+charged uipmentthrough s are 7sethe d to%losed avoid lines, the 5x!ithout posure Spillage # 2rritaon # tackle the irritaon %o %orr rros osiv ive e natu nature re 7s 7se e prop proper erl) l) pe pers rson onne nell prot protec ecv ve e e+ e+ui uipm pmen ent$ t$
%harging of sodium h)droxide isllaon of &%
oss o off
and me methanol$
methanol$
%harging o off
Boom va valve o op pened,
toluene
or eakage of Boom "alve
&%
and 3he temperature is raised b) slo! heang ll re0ux8 the methanol "apour oss is due to 5xcessive heat, 2nstrucon is 9iven in SO*, 3o Open the steam valve to Opmum so as to maintain the re0ux Operaonal Operaon al control - checkpoint shall be included in the batch sheet to indicate !hether the boom valve has been closed prior to charging toluene # is not eaking$
'ire 'ire ha ha(a (ard rd du due e to sta tac c elec electr tric icit it) )
3o separate the
3oluene oluene addi addion on pipe pipe is is k kept ept to to the Bo Boo om m of tthe he rrea eacto ctorr$ *ipe *ipe lines lines a are re a all ll SS an and d e+ e+ui uipm pmen entt moto motors rs ar are e 0ame 0ame pr proo ooff$
3he centrifuge is earthed b) conducng !ires$ 3he :ltraon is carried out through a centrifuge$ %entrifuges are high speed machines and sources of ha(ard in a chemical plant$ Ample precauons are taken to carr) out the centrifuging as 'ire ha(a ha(ard rd due tto o ha(ard ha(ard free free as pos possible sible$$ ;e are are usi using ng a 4< inch d dia ia SS. SS.1= 1= centrifuge, boom driven and top discharge$ 3his is a four point stac electricit), suspension machines !hich are put on special vibra mount for operator ha(ard if
%entrifuging
%apecitabine an) loading > from unloading acvit) stage-222 the li+uid carried out in a running centrifuge
%harging Solvent recover)
r)ing operaon
Separaon of sol solvents from the product
smooth vibraon free noiseless operaon$ 3he speed is controlled b) a variable fre+uenc) drive and the feeding of the centrifuge is done b) pneumacall) controlled valves at lo!er *& under nitrogen purging$ 5ven 5ven the bearing housing of the centrifuge is provided !ith a nitrogen purging facilit) facilit)$$ An interlocking s)st s)stem em is provided for ensuring that the lids cannot be opened !hile the centrifuge is running and thereb) prevenng an) operaonal ha(ard b) human error$ All the limits s!itches and the safet) interlocking s!itches are 0ame proof including the "' controls$
of
&Hs 6a(ardous ?o speci speci:c :c ha ha(a (ard rd !aste a@er centrifuging r)ing of the product in ?o speci:c ha(ard "acuum tra) dr)er
All charging is done b) vacuum sucking to avoid spillages and thr throug ough h the clos closed ed SS p pipe ipe lline ines$ s$
"3 is :ed !ith 0ame proof motors$ 7nloading into the bins b) actuated valve, 6ence ?o- ess 5xposure 6and gloves # goggles should be used$
S$?o
+$cr$p#on
Yearly +ata ./. .// ./ -./0 I .1 . J
./1 -./2 .1 <
-./3
1
?o$of minor incident>accidents from
D
D
D
D
D
D
1
?o$of maKor incident>accidents from ?o$of occupaonal health
D
D
D
D
D
D
D
4/
.con:ned space
/<
H
2( &ri$hnam Nai!u 2* Nara$imhulu
>H >H
2 7.8an!uran"a Nai!u
;
2. N.8ra$a! chanta
;
O+
Normal
Normal
Nil
Nil
Nil
Nil
Nil
Normal
Normal
Normal
Normal Normal
Normal
Normal
Normal
Normal
C le ar
ci !i c
N ilil
N il
Normal
Nil
Normal
B+
Normal
Normal
Nil
Nil
Nil
Nil
Nil
Normal
Normal
Normal
Normal Normal
Normal
Normal
Normal
Normal
C le ar
ci !i c
N ilil
N il
Normal
Nil
Normal
O+
Normal
Normal
Nil
Nil
Nil
Nil
Nil
Normal
Normal
Normal
Normal Normal
Normal
Normal
Normal
Normal
C le ar
ci !i c
N ilil
N il
Normal
Nil
Normal
B+ Normal
Normal
Nil
Nil
Nil
Nil
Nil
Normal
Normal
Normal
Normal Normal
Normal
Normal
Normal
Normal
C le ar
ci !i c
N ilil
N il
Normal
Nil
Normal
Normal
Normal
Nil
Nil
Nil
Nil
Nil
Normal
Normal
Normal
Normal Normal
Normal
Normal
Normal
Normal
C le ar
ci !i c
N ilil
N il
Normal
Nil
Normal
B- Normal
Normal
Nil
Nil
Nil
Nil
Nil
Normal
Normal
Normal
Normal Normal
Normal
Normal
Normal
Normal
C le ar
ci !i c
N ilil
N il
Normal
Nil
Normal
+
2/ &.+athi$h Ba:u
;
B+
Normal
Normal
Nil
Nil
Nil
Nil
Nil
Normal
Normal
Normal
Normal Normal
Normal
Normal
Normal
Normal
C le ar
ci !i c
N ilil
N il
Normal
Nil
Normal
22 B& 7an"a Ra,
;C
O+
Normal
Normal
Nil
Nil
Nil
Nil
Nil
Normal
Normal
Normal
Normal Normal
Normal
Normal
Normal
Normal
C le ar
ci !i c
N ilil
N il
Normal
Nil
Normal
Normal
Normal
Nil
Nil
Nil
Nil
Nil
Normal
Normal
Normal
Normal Normal
Normal
Normal
Normal
Normal
C le ar
ci !i c
N ilil
N il
Normal
Nil
Normal
No rma l
No rma l
Nil
Nil
Nil
Nil
Nil
Normal
Normal
Normal
Normal Normal
Normal
Normal
Normal
Normal
C le ar
ci !i c
N ilil
N il
Normal
Nil
Normal
24 9e#ara, 8atil
;C
B+
46 B.Bharmanna$hi#araya
;C
B+
41 &.+uren!er Re!!y
;C
+
Normal
Normal
Nil
Nil
Nil
Nil
Nil
Normal
Normal
Normal
Normal Normal
Normal
Normal
Normal
Normal
C le ar
ci !i c
N ilil
N il
Normal
Nil
Normal
4% &ri$hna
;C
O+
Normal
Normal
Nil
Nil
Nil
Nil
Nil
Normal
Normal
Normal
Normal Normal
Normal
Normal
Normal
Normal
C le ar
ci !i c
N ilil
N il
Normal
Ni l
N or or ma ma l
Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. & Freefrom Ne"atii#e #e Healthy Conta"iou$ !i$ea$e$.Occupational health & Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & Ne"atii#e #e Conta"iou$ !i$ea$e$. Healthy & Freefrom Occupational health & N e "a titi #e #e
%ontagious diseases$
4( G.+re!har
;C
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
4* +.'aya!e# Goranta
;C
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
4 G.nanatha$ena Re!!y
;C
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health &
4. +ure$h Gou!
;C
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
4/ N.Na"e$h
;C
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
42 B.Ra,e$h
;C
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
44 9.Harnath Re!!y
;C
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
166 8.'alan!har
;C
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
O+
161
a$i$h Be!mutha
;C
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
16%
.&a,an "ou!a
;C
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
16(
&.n0ar :a$ha
;C
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
16*
9r.5.+he$hachalam
R
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
16- 9r.Rafiu!!in
CR&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
16
9r.+an,ay Hirpara
CR&9
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
16/
3.runRe!!y
CR&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
162
N.'a"anmohan Re!!y
CR&9
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
164
Chan!re$h kumar triipati pati
CR&9
B- Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
116
ar#in! mi$hra
CR&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
111
B.Yu#a )e,a
CR&9
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
11%
G.3enkata Re!!y
CR&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
11(
5.+ri!har Ba:u
CR&9
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
11*
N.Ran,ith
CR&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
11- 8.+ati$h
CR&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
11
CR&9
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
11/ ).+rini#a$
CR&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
112
,ith &arpe
CR&9
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
114
Rame$h :a:u
CR&9
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1%6
3i$hnu 3ar!han re!!y
CR&9
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1%1
Ch.Raama )heer!a
CR&9
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1%%
$hok &umar !!anki
CR&9
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1%(
7!.?har Hu$$ain
CR&9
B+ Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1%*
+atya Narayana ayana 9an!a
CR&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1%- G..N.&.Re!!y
CR&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1%
Y.3eera Re!!y
CR&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1%/
Ra,a#ar!han Gou!
CR&9
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1%2
Gan"a!hara Rao
CR&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1%4 G.Ba!raiah
CR&9
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1(6
9r.3ino!&umar +in"h
R&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1(1
Gopal Bo:la!e
R&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1(%
Chan!ra 8raka$h
R&9
B+
No rma l
No rma rmall
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1((
G.3.8a#an &umar
R&9
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1(*
&.Nar$appa Nai!u
R&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1(-
Bala,i ki$anro ka!am
R&9
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1( 9ilip &umar
R&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1(/
+unil +hin!e
R&9
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1(2
8.+rini#a$ +arma
3i,ay &umar H8
8&
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1( 4 & ul !e ep Na "ar
8 ro !
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1* 6 7 uni $h $h 3e rm a
8 ro !
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1*1
B.$0ara Rao
8ro!
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1*%
fta: hme!
8ro!
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
8 ro !
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1* ( + . $ho k&u ma r 1** +an,ay
CR&9
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1*-
karunakar CH
R&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1* &.7an"ala"iri
CR&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
No rma l
No rma rmall
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1*/
N.+rini#a$a Rao
R
1*2 Giri$ha
CR&9
1*4
Bala,i Chan!ra
CR&9
B+
1-6
Nara$imha Rao
CR&9
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1-1
3eera papaiah
CR&9
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
- Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1-% 8uran!har 1-( Na"e$h
=87
=87
1-*
7.8ra$ant 8urohit
CR&9
1--
B.8oorna Chan!er Rao
R
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1-
B.+ati$h &umar
R
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1-/
7.Nare$h &umar
CR&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1-2
9yane$0ar #a"are
CR&9
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
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Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$.. Healthy & Freefrom Occupational health & N e" at i# e C on ta "i ou ou $ ! i$ ea $$ee $$..
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
16 8aramanan!
G-Block
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
11
C.3enkate$0arulu
G-B lock
O-
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1%
Ra"hunan!an Gou!a
G-Block
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
'-Block
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1* Ch.Na"aBa:u
-Block
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1-
-Block
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1 7.8ra#een
-Block
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1/ C.+rini#a$ulu
-Block
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
12
+uka!e# 7ahanti
C-Block
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
14
B.&a$i Nai!u
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1/6
8.+hi#a 8ra$a!a Rao
1-4
Nan!a &umar )he"il
1( C.+u!hakar
R&9
7.3enkata +u::a Rao
1R8
NGG
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1/1 N.Na"a Ra,a
NGG
+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
1/%
NGG
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
=)
O+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
=)
B+
Normal
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
Normal
N il
N il
N il
N il
N il
N or ma l
N or ma l
N or ma l
N or ma l N or ma l
N or ma l
N or ma l
N or ma l
N or ma l
C le ar
ci !i c
N ilil
N il
N or ma l
N il
N or ma l
8.Rama Chan!ra Rao
1/( ?nit at ai&r' for t&e roiet a &eld on 07.0.2005.
9.
%aed
on t&e information =mitted =! !o, t&e Minitr! of "nvironment and
Foret &e &ere= re=! ! a ao ord rd environmental lea learan rane e to t&e a= a=ov ove e ro8e ro8ett nder t&e
roviion of "HA Notifiation dated 14& etem=er 2005 =8et to omliane of t&e folloin> &t of 0 m &a[ =e intafled for dierion of $artilate matter. !lone earator efiiien! &all =e minimm
60L.
l[.
&ere &all =e
no odor nr=ane from rodt E mat"rial ed. odor &afl =e
ontrolled a er t&e t&e Gideline of %. %.
e>lar
monitorin> of and
!
&all =e arried ot
at vario ro=a=le
loation in Kater
t&e am=ient air in and arond t&e lant and in t&e ortB Cone area,
it&draal &all not e*eed l,2 +# &i& &all =e ored from r&e Mniial l!.
&e ate ater >eneration &all not e*eed >00o +# &i& &afi =e treated in t&e "$ to tertiar! treatment and &all =e ed lor >ardenin> and landain>,
after meetin> oa; il
t&e di&ar>e norm. #ometi ater ifi =e ent to eti tan; folloed =!
/
vi
#ediate #edi ated d r= r==er =er and ta ta; ; of aro aroriate riate &ei>&t a er t&e entr"it $olltio $oll tion n ont ontrol rol %oard >ideline &all =e rovided rovided to ontrol t&e emiion
vario vent. &e r==ed ater &all &all =e ent ent to " for frt&er from vario
treatment. vii
All t&e tora>e tan; ill =e =e nder ne>ative ne>ative r re e re re to avoid ari! lea;a>e. %reat&er !tem valve, N, =lan;etin> and eondar! ondener it& =rine &illin> All liDid rovided &all =e for all t&e tora>e tan; to minimiCe vaor loe. ra &andlin> !tem for material &all =e tored in tora>e an; and #rm. loe
ill =e rovided for &emi &e mial al and olvent olvent il rovide ded. d. Ma>neti eal illl =e rovi m/a>itator for reator for redtion of frr>itive emiion. e lea;a>e &all =e it& +ea; #etetion and eair (+#A) !te !tem m and +"+ indiator and !droar=on
detetor. roviion for immediate iolation of & eDiment, in ae
of a lea;a>e ill alo =e made. tie oman! &all rovide
a
ell defined +ea;
#etetion and eair (+#A) ro>ramme for
Dantifiation and ontrol
of f>itive emiion. &e detetor enitivit! ill
=e in m level. ix
&e oman!
&all nderta;e folloin> Kate MinimiCation meare.
Meterin> and ontrol
of
ee of =!-rodt
Dantitie
of ative in>redient to minimiCe ate.
from t&e roe a ra material or a ra material
=titte in ot&er roee.
?e
of atomated ,illin> lo minimiCe illa>e.
?e of loe Feed. !tem into =at& reator.
enlin>
eDiment t&ro>& vaor reover! )rlem. .
rere &oe for eDiment leanin> to rede aleater ?e of &i>& rere &oe
>eneration. x
F>itive emiion in l&e or; Cone environ environmen ment, t, rodt, and ra material tora>e area &all =e re>la re>larl! rl! monitore monitored. d. &e emiion &all onform lo t&e limit olltion imoed =! t=e iderine nder
Manfatre, e and lm lmort of aCa aCard rdo o &emial&le, 16 166 6 a in amended to=er, 1664 and Janar!, 2000 and aCardo Kate
(Mana>ement and andlin>) le, 16>6, a amended from time lo time. Al&oriCation from t&e o=tained for olletion, olletion, treatment,
tora>e, and dioal of
AHH
$roe $ro e ate, efe t>e and r>ani r>ani reide &al &alll +e olleted and a;eo in roof $" $" =a> and tored tored temor temorari aril! l! in a eara earate te lea&at lea&ate e overed overed &ed &ed till dioal into ional xxvi
&e ro8et
at&oritie &rH iTTR
8rrY3@P 1'R33R.[3lPXR,,iQ.m13fi311,,n,r,r[,,,P ,@
r&e rearane, ir imremenration
7.
oJ3 Qff>.3ffi33,,3fi3end
or an! or ,
&e Minitr! reerve
neear!.rR-ii,R1,RXPJ,38.,3,3,3fi
linPR*3.313PrP..,,,o,n.
>PRil9,,QttriR.*RRRitl.iRi@,
-r.,
P,aR1a R-F.-.-n=.
=e ;et ell it&in t&e
(*ii) &e overall noie level in and ardnd t&e lant area &all
aoti &ood'
tandard =! rovidin> noie ontrol meare lnldin>
>eneration'&e am=ient noie level &all ilener, enlore et'on alt ore of noie ($rotetion) onform to t&e tandard reri=ed nder "nvironment
(ni>&t time)' At, 165 le, 166 viC. 79 d%A (da! time) and 70 d%A >reen =elt a er t&e $% (*iii) 29L of t&e total area &all =e develoed a >ideline.
(*iv) ational &ealt& rveillane oft&e or;er
&all =e anied ot on a
re>lar =ai and reord &all =e maintained a er t&e At' t&e Fatorie At' (*v) rainin> &all =e imarted to all emlo!ee on afet! and &ealt& ae-t of eriodiat medial &emial &andlin>. $re-emlo!ment and rotine =ai' e*amination for all emlo!ee &all =e nderta;en on re>lar &all =e enred' (*vi) ?a>e of $$" =! allemlo!ee/or;er xvii
xviii
&e oman! &all tritl! follo all t&e reommendation mentioned in t&e ("$)' &arter on ororate eoni=ilit! for "nvironmental $rotelion from roofto of t&e t&e &e oman! &all &arvet rfa,e a ell a rainater
=ildin>rooedint&ee*anionro8etandtormate =ildin>rooedint&ee*anion ro8etandtormaterdraintore&ar>e rdraintore&ar>e t&e>rondaterandet&eameaterfort&evar t&e>rondaterand et&eameaterfort&evarioativitieoft&eoet ioativitieoft&eoet to onerve fre& ater. .
(*i*) &e ro8et roonent &all alo oml! it& all t&e environmental rotetion t&e meare and afe>ard rooed in t&e "HN"M$ reort' All reommendationmadeinreetofenviron reommendationma deinreetofenvironmentalmana>ementan mentalmana>ementandri; dri; miti>ation meare relatin> to t&e ro8et &all =e imlemented'
(**) &e oman! itt ndeilafe i[ r=liPvant meare, a indiated din> t&e $=li nondin> area'
earin> for imrovin> imrovin> t&e loal villa>e and
(**0 &e oman! &all nderta;e eodevelomental meate inldin> ommnit! t&e elfare meare in t&e ro8et area for t&e overall imrovement of
environment. &e eodeveloment lan &old =e =mitted to t&e ement Mana>ement ell eDied it& fll fled>ed Mana>ement
ta=orator! failitie &all =e et to arr! ot t&e "nvironmental
and
Monitorin> fntion.
o!=. #eartment of Foret, "olo>! E "nvirorment $rinial &e Govemment :amata;a, room No. 404, 4 Floor, ll e, Mlti la, %an>lore- 950 04P :amata;a .
.
arive&
&e &airman, entral $dMion ontrol %oard omle*, "at Ar8n Na>ar, Ne #et&i - 110 02.
%&avan. %#-mfiie
ar!avaran
&e &airman, A.$.$olllion A.$.$olllion ontrol %oard,
%&avan, A-, lndrtrial
"tate, ell, Minitr! d "nvironment and Foret, ar!avaran %&avan, 5 omle*, Ne #el&i. 5. 7.
Gard File.
Monitorin> File eord File.
.i.3
H H (#r.$.+ A&ianil' #iretor
I
AH?
HH,H..l
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