Expt 12- 19

LECTURE NOTES: Reduction- Oxidation Titration (Expt. 12- 19) 1. Neutr Neutrali aliza zati tionon- acid acid and base base 2. Redo Redoxx- red reduc ucin ing g agent, agent, oxi oxidi dizi zing ng agent agent Oxidizin aent!: aent!: KMnO4 ; ceric sulfate; odine ; bro!ine; "otassiu! iodate Reducin aent!: Oxalic acid; ferrous sulfate; sodiu! t#iosulfate Note:

#$ no. of electrons gained or lost de"ending on its role in redox

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E"#ER$%ENT 12: #reparation and Standardization o& #ota!!iu' #er'ananate Soution

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E"#ER$%ENT 12: . #reparation o& #ota!!iu' #er'ananate Soution* Ca!!

1. %eig# roug#l& 'g of KMnO4 2. (issol)e it in 1'** !+ distilled ater in a big beaer. . /o)er it# a atc# glass and boil t#e t #e solution for 1' !ins 0"re)ent e)a"oration and accelerate destruction of organic !atters or deco!"osition

4. llo to stand for at least 2 da&s

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E"#ER$%ENT 12: LECTURE NOTES:  sbestos- carcinogenic   for filtration of inorganic !atter    s#ould be lined it# a glass ool as su""ort 0funnel #en used as a filter. 

#ould be as#ed it# distilled ater until ater

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E"#ER$%ENT 12: +. Standardization o& #ota!!iu' #er'ananate Soution 1. %eig# ig# *.1 *.1--*.2g *.2g of Na Na2/2O4 0eig#ing bottle 2. (issol)e it in 2'* !+ distilled ater in a big beaer. . dd 5!+ of conc. sulfuric acid 4. 6ea 6eatt t#e t#e solu solutio tion n to 5*⁰/ 0!aintain ---reaction beteen sodiu! oxalate and KMnO 4 occurs stoic#io!etricall& in a #ot acidic !ediu!

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E"#ER$%ENT 12: LECTURE NOTES tandardization: "ri!ar& standardization 7&"e of 7itration: Redox Met#od of 7itration: 7itration: (irect er!anganate !et#od 1. Na2/2O4 - "ri!ar& standard, reducing agent

2. KMnO4 -strong oxidizing agent

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E"#ER$%ENT 12: Lecture Note! . 62O4 -to ee" t#e acid conc. constant "re)enting t#e for!ation of MnO

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E"#ER$%ENT 12: LECTURE NOTES '. 