C) CAPITULO II. MUESTREO Y PREPARACIÓN DE MUESTRAS
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CAPÍTULO II. MUESTREO Y , PREP PREPARACIÓN ARACIÓN DE MUESTRAS
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MUESTREO:
Proceso de selección de una porción de material que represente o proporcione información sobre el sistema en estudio (población). (población).
Para que los resultados de una análisis sean acertados, es necesario que la muestra que se va analizar sea representativa, es decir, que contenga la misma proporción de componentes que el total del producto (lote), por lo que el muestreo es de gran importancia.
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El muestreo. Importancia:
Para evaluación metalúrgica de yacimientos.
Para balance metalúrgico.
Para embarque de mineral.
Casi todas las decisiones que se hacen respecto de un Proyecto
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OPERACIONES OPERACION ES MAS MA S IMPORTANTES EN EL MUESTREO MU ESTREO Y TRAT TRATAMIENTO DE LA MUESTRA TIPOS DE MUESTRA
NUMERO DE MUESTRAS
PLAN DE MUESTREO
MUESTRA
TAMAÑO DE MUESTRA
ERRORES DE MUESTREO
SUBMUESTREO
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ETAPAS IMPLICADAS EN UN ANALISIS PROBLEMA
PLANTEAMIENTO DEL PROBLEMA ANALITICO
SELECCIÓN DEL METODO
O E R T S E U M
DISEÑO DEL PLAN DE MUESTREO
TOMA DE MUESTRA
TRATAMIENTO DE
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PLAN DE MUESTREO
Procedimiento para seleccionar, extraer, conservar, transportar y preparar las porciones porciones a separar de la población en en calidad de muestras.
El proceso de muestreo debe ser planificado, detallado y escrito. El plan de muestreo debe incluir:
Dónde realizar la colecta de la muestra.
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REQUISITOS DEL PLAN DE MUESTREO 1.- Debe ser adecuadamente planificado e idealmente efectuado con la frecuencia suficiente para detectar las variaciones que pudieran ocurrir en el transcurso del tiempo.
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REQUISITOS DEL PLAN DE MUESTREO 6.- Debe ser enviada al laboratorio en forma y en un lapso de tiempo tales que no modifiquen sus características originales. 7.- Los detalles del muestreo debe ser adecuadamente descritas con etiquetas
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MUESTRA: Es el material sobre el cual se realiza una determinación. UNIDAD DE MUESTREO: Es una porción del material de volumen suficiente para poder contener con una elevada probabilidad la misma distribución de tamaño de partícula que el material que se somete a muestreo.
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MUESTRA BRUTA:
Se obtiene reuniendo un cierto numero de unidades de muestreo que han sido colectadas en forma sistemática.
Cuando mayor sea el numero de unidades de muestreo, mas representativa será la muestra bruta de totalidad del material.
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MUESTRAS Y MUESTREO
TIPOS DE MUESTRAS:
Representativa: composición y propiedades similares al conjunto de la muestra.
Selectiva: obtenida en el muestreo de determinadas zonas.
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COLECTA COLECTA DE MUESTRAS DE MINERAL, SUELO Y/O
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FACTORES QUE COMPLICAN EL PROCEDIMIENTO DE MUESTREO
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MUESTREO DE SOLIDOS (ROCAS, MINERALES, SUELOS, SEDIMENTOS).
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MUESTREO EN SEDIMENTOS (RÍOS, CANALES)
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CUIDADOS ESPECIALES QUE SE DEBEN TENER TENER DURANTE EL MUESTREO
A) Contaminación de la muestra b) Oxidación atmosférica c) Cambios de humedad d) Pérdida de partículas volátiles
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B) REDUCCIÓN DE LA MUESTRA Consiste en reducirla en tamaño de partícula y en cantidad a través de los siguientes pasos: 1) Trituración y molienda 2) Pulverización 3) Divisiones sucesivas
Cuidados especiales que se deben de tener durante la reducción de la
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MÉTODOS DE MUESTREO Y DISPOSITIVOS DISPOSITIVOS UTILIZADOS UTILIZADOS EN LA REDUCCION DE LA MUESTRA 1) MÉTODOS DE MUESTREO: a) Coneo y Cuarteo b) Rifleado c) Paleo d) Divisores Sectoriales
2) DISPOSITIVOS DE MOLIENDA:
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MOLINO DE RODILLOS
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MOLINO DE CONOS
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PULVERIZADOR PULVERIZADOR DE ANILLOS
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PULVERIZADOR DE DISCOS
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METODO DE CONEO Y CUARTEO Procedimiento del método de Coneo y Cuarteo: 1)
La muestra de mineral se tritura a un tamaño menor de media pulgada, y se extiende en una placa lisa de hierro o en una superficie de concreto que pueda ser limpiada fácilmente.
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MUESTREO POR CONEO Y CUARTEO
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METODO DE RIFLEADO
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PARTIDOR DE RIFLES RIFL ES
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B) PREPARACION DE LAS MUESTRAS PARA EL ANALISIS QUIMICO El tamaño de partícula final de la muestra representativa dependerá del análisis que se pretenda efectuar. efectuar. Existen varios dispositivos para reducir el tamaño de partícula: 1). Pulverizador de discos 2). Pulverizador de anillos 3). Mortero de porcelana 4). Metate y/o plancha de hierro
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La molienda en metate y/o plancha de hierro también se aplica a las muestras que puedan sufrir alteración con el calor producido por el pulverizador como sucede con los minerales de Hg, Se, S. ELEMENTOS Y/O COMPUESTOS
DISPOSITIVO DE MOLIENDA
TAMAÑO DE PARTICULA (MALLAS)
Au, Ag, Cu, Fe, Pb, Zn, Cr, Co, Cd
Pulverizador de disco Pulverizador de anillos
-100 -100
Sn, W, V, Ti, Al
Metate /plancha de hierro
-200
Hg, Se, As, S
Metate/plancha de hierro Mortero de porcelana
-100 -100
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D) CONSERVACIÓN DE LAS MUESTRAS Las muestras deben guardarse de tal forma que queden reducidas al mínimo los cambios que puedan sufrir antes del análisis, como por ejemplo:
a) Perdida de agua de los hidratos b) Adsorción Adsorción de agua de la atmosfera c) Adsorción Adsorción de dióxido de carbono por sustancias alcalinas d) Oxidación atmosférica e) Contaminación
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D) CONSERVACIÓN DE LAS MUESTRAS Es muy importante clasificar las muestras, es decir, darle su identificación, por ejemplo: a) Localización geográfica del área de estudio.
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E) SECADO DE LAS MUESTRAS
La humedad absorbida por la muestra varia con el tamaño de partícula, humedad y naturaleza de la muestra.
La mayor parte de los sólidos se analizan después de secarlos en una estufa u
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ESTUFAS ESTUFAS (a) Y HORNOS (b)
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MUESTREO DE METALES Y ALEACIONES
Las muestras de metales y aleaciones, en general, sistemáticamente porciones por taladrado, limado, o fresado.
se
toman
Las dificultades principalmente radican en las heterogeneidades que resultan como consecuencia de la segregación de impurezas en el
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